Composites based on polystyrene and natural rubber at a ratio of 85/15 were prepared by melt mixing with nylon-6 fibres using an internal mixer. The loading of short nylon-6 fibre, untreated and resorcinol formaldehyde latex (RFL)-treated, was varied from 0 to 3wt.%. Tensile and flexural test samples were punched out from sheets and tested to study the variation of mechanical and dynamic mechanical properties. The tensile behaviour of the composite has been determined at three different strain rates (4.1Ă10â4sâ1, 2Ă10â3sâ1 and 2Ă10â2sâ1). Both the tensile strength and Youngâs modulus of the composite increased with strain rate. The tensile strength, tensile modulus, flexural strength and flexural modulus increased with the increase in fibre content up to 1wt.%, above which there was a significant deterioration in the properties. The RFL-treated fibre composites showed improved mechanical properties compared to the untreated one. Dynamic mechanical analysis (DMA) showed that the storage modulus of the composite with RFL-treated fibre was better compared to the untreated one. The fibreâmatrix morphology of the tensile fractured specimens was studied by scanning electron microscopy (SEM). The results suggested that the RFL treatment of nylon fibre promoted adhesion to the natural rubber phase of the blend, thereby improving the mechanical properties of the composite.