Ultrasonic Frequency Research Articles

First applications of ultrasound technology in solid rocket propellant combustion promotion

The regulation of propellant combustion using ultrasonic waves is proposed. Under ultrasonic frequencies of 25–40 kHz, we systematically examined the combustion characteristics of Al particles, ammonium perchlorate (AP)/hydroxyl-terminated polybutadiene (HTPB) propellants, and Al-containing Al/AP/HTPB propellants. Ultrasonic treatment increased the ignition delay time of the Al particles by 48.3 %. However, it increased the burning rate of the AP/HTPB propellants by up to 26.1 % and decreased their ignition delay by 39.3 %. As the ultrasonic frequency increased, the burning rate of the solid Al/AP/HTPB propellants increased by 22.5 %, and the degree of Al agglomeration decreased, resulting in a 24 % decrease in the size of the condensed-phase combustion products. The action mechanism was analyzed in terms of the effects of ultrasonic waves on Al droplets and combustion flames. The introduction of ultrasonic waves split the Al droplets near the burning surface into smaller particles, which affected combustion efficiency. Bringing the diffusion flame closer to the burning surface affected the burning rate. These findings demonstrate that the combustion and agglomeration characteristics of solid propellants can be modified using ultrasonic techniques, providing a new method for controlling the thrust of solid rocket motors.

Receptivity of Rayleigh-Taylor instability to acoustic pulses: Theoretical explanation of pulse propagation

Direct numerical simulation (DNS) of Rayleigh-Taylor instability (RTI) has been reported in “Three-dimensional (3D) DNS of RTI triggered by acoustic excitation - Sengupta, et al. Phys. Fluids 34(5), 054108 (2022)” using more than 4 billion points with initial time steps of 7.69 ×10−8s. The set-up consists of quiescent heavy (cold) fluid atop lighter (hot) fluid initially separated by an insulated partition. Removal of this partition creates acoustic pulses in the directions normal to the interface, which provides the receptivity route of RTI to transient acoustic pulses spread over several mega-Hz frequencies, far in excess of ultrasonic frequencies. The DNS and its analysis reveal the pulses to be severely attenuated, which cannot be explained by the classical wave equation. In the present research, after demonstrating the features of the DNS results, we report in detail, the theoretical development of a wave equation incorporating losses based on the Navier-Stokes equation without Stokes' hypothesis for a quiescent ambience. Apart from the physical properties of this altered wave equation, the numerical solution of the same is obtained. The governing partial differential equation (PDE) for the propagation of disturbances in the spectral plane, provides the dispersion relation between wavenumber and circular frequency in the dissipative medium accounting for viscous losses. The presented analysis provides physical properties using the global spectral analysis (GSA). This shows the far-field perturbation to propagate either as attenuated waves or strictly in a diffusive manner depending upon the wavenumber. The PDE is solved numerically by a high-accuracy compact scheme and the four-stage, Runge-Kutta scheme for time advancement. The computed solution is shown to match not only with the developed theoretical analysis but also explains the DNS results for RTI at early times when the computed flow field truly represents the quiescent ambience.

Modeling of the separation process of a two-phase liquid in a high-temperature gas environment

Obtaining a high-quality highly dispersed salt solution can be realized from a salt solution by the method of ultrasonic exposure. As you know, concentrated salt solutions can be presented in the form of a gas-liquid medium. The influence of ultrasound, in the case of wetting a surface vibrating with an ultrasonic frequency by a thin layer, leads to the formation of a cavitation layer in the liquid layer and capillary waves on its surface, from the ridges of which, at a certain intensity of oscillations, finely dispersed aerosol droplets are detached.The detachment of droplets from the vibrating surface leads to the formation of finely dispersed salt aerosol, which saturates the heated air, which is tangentially fed into the cylindrical working chamber with further separation of hydrodynamic processes. Part of the aerosol wets the heated inner surface of the cylindrical chamber with the formation of a thin film, which gravitationally flows down the vertical solid surface and is subjected to active evaporation with the removal of the salt phase, and the second part is subjected to additional grinding and active evaporation in the central turbulent flow and centrifugal turbulent flow of hot air with additional by removing the salt phase. In order to intensify the salt removal process, the surface on which the film is formed can be profiled. Ultrasonic dispersion of the salt solution to a finely dispersed state allows to significantly increase the surface of contact with the heated air, which allows to intensify the diffusion process.

On the Dynamics of a Novel Liquid-Coupled Piezoelectric Micromachined Ultrasonic Transducer Designed to Have a Reduced Resonant Frequency and Enhanced Ultrasonic Reception Capabilities.

This paper introduces a novel design for a liquid-deployed Piezoelectric Micromachined Ultrasonic Transducer (PMUT). This design was specifically developed to resonate at a lower ultrasonic frequency than a PMUT with a circular, fully clamped diaphragm with the same diameter. Furthermore, the novel design was also optimised to enhance its ultrasonic radiation reception capabilities. These parametric enhancements were necessary to develop a PMUT device that could form part of an eventual microscale sensory device used for the Structural Health Monitoring (SHM) of reinforced concrete (RC) structures. Through these two enhancements, an eventual microscale sensor can be made smaller, thus taking up a smaller die footprint and also be able to be deployed further apart from each other. Eventually, this would reduce the developed distributed sensor system's cost. The innovative design employed a configuration where the diaphragm was only pinned at particular points along its circumference. This paper presents results from Finite Element Modelling (FEM), as well as experimental work that was conducted to develop and test this novel PMUT. The experimental work presented involved both laser vibrometry and ultrasonic radiation lab work. The results show that when compared to a clamped diaphragm design, the novel device managed to achieve the required reduction in resonant frequency and presented an enhanced sensitivity to incoming ultrasonic radiation.

A New Process of Chemical Plating Ni-P Electromagnetic Induction Heating Activation on the Surface of Aluminium Alloy Base Material

Nowadays, there are many surface treatment methods for aluminium alloys; the most commonly used of these is the chemical dip galvanizing process, which is complicated due to its use of large quantities of corrosive drugs. In order to simplify the process, this paper proposes a new electromagnetic induction heating activation method instead of the zinc dipping process. The method works as follows: The substrate is first degreased and then activated. The activation process starts by soaking the degreased substrate in an activation solution, taking it out after ten minutes, and placing it into an induction heating unit. The activation solution is sprayed onto the surface of the substrate while heating, using the energy generated by high temperatures to complete the activation reaction. The surface of the activated substrate forms a nanoscale film of nickel, which is finally utilised as a catalytic centre for ENP (an advanced surface treatment process that deposits a very uniform layer). The optimisation of important parameters of the non-destructive activation process was determined using the L9 Taguchi method. The main parameters ranged from 0.15 L/min to 0.25 L/min for spray rate, 200 °C to 400 °C for heat treatment temperature, and 1:4, 1:5, and 1:6 for Ni2+ and H2PO4− ion concentration ratios. The above data were derived from a single variable and were analysed using Minitab 20 software. Scanning electron microscopy (SEM), X-ray photoelectron spectroscopy (XPS), energy spectrometry (EDS), and ultrasonic experiments were used to characterize and analyse the surface morphology, composition, and bond strength of the coatings. The results show that the nanoscale nickel particles can completely cover the surface of the substrate, forming a layer of nano-film. After activation and ultrasonic cleaning for 30 s at an ultrasonic frequency of 40 KHz and a power of 80 W, the surface nano-film was not destroyed, which proves that it had a high bonding strength. After the application of the plating, the plated surface had a compact microstructure, and the continuity was good. Therefore, compared with the currently commonly used zinc dipping process, this process has the advantages of being a low-cost, simple operation, and non-destructive and environmentally friendly activation process for the substrate.

A Comprehensive Review of Piezoelectric Ultrasonic Motors: Classifications, Characterization, Fabrication, Applications, and Future Challenges.

Piezoelectric ultrasonic motors (USMs) are actuators that use ultrasonic frequency piezoelectric vibration-generated waves to transform electrical energy into rotary or translating motion. USMs receive more attention because they offer distinct qualities over traditional magnet-coil-based motors, such as miniaturization, great accuracy, speed, non-magnetic nature, silent operation, straightforward construction, broad temperature operations, and adaptability. This review study focuses on the principle of USMs and their classifications, characterization, fabrication methods, applications, and future challenges. Firstly, the classifications of USMs, especially, standing-wave, traveling-wave, hybrid-mode, and multi-degree-of-freedom USMs, are summarized, and their respective functioning principles are explained. Secondly, finite element modeling analysis for design and performance predictions, conventional and nano/micro-fabrication methods, and various characterization methods are presented. Thirdly, their advantages, such as high accuracy, small size, and silent operation, and their benefits over conventional motors for the different specific applications are examined. Fourthly, the advantages and disadvantages of USMs are highlighted. In addition, their substantial contributions to a variety of technical fields like surgical robots and industrial, aerospace, and biomedical applications are introduced. Finally, their future prospects and challenges, as well as research directions in USM development, are outlined, with an emphasis on downsizing, increasing efficiency, and new materials.

Feasibility of ultrasonic non-destructive testing of ancient funerary urns: Experimental and analytical parametric model

Non-invasive modalities are being developed as the computer tools and industrial non-destructive testing capabilities become more widespread. Using the same investigation methods as those applied to modern objects, we seek to study ancient funerary urns containing human bones. The exploration of ancient urns is key to increasing our understanding of the practices of burial and cremation in archaeo-anthropology. But those urns present at archaeological sites are exposed to diversified environments (wet, temperate or dry environment), and can be subjected to chemical or mechanical destructive actions over time. As ancient funeral urns containers are sometimes made of lead, stone or ceramic, the use of X-ray scanners is difficult or even impossible for in situ control. In this work, we propose an engineering technique based on ultrasonic non-destructive testing and wave propagation in urns. An analytical parametric model is developed using mathematical signal processing tools and validated by means of laboratory experiments under controlled conditions of propagation through reproductions of ancient urns for two ultrasonic frequencies (500 kHz and 1 MHz). The aim is to characterise an ancient urn by creating an analytical model, and to use a parametric identification algorithm to determine the presence or absence of bone fragments. The parametric identification algorithm based on the Levenberg–Marquardt method makes it possible to determine the geometrical (thickness) and physical (wave velocity and attenuation, mass density) parameters when the urn is filled with water, with water and bones, and with water, bones and sand. We show that the model makes it readily (processing time ≈15 sec) possible to find the different times of flight between the transducer and the different walls of the urn and the parameters with an accuracy less than 10%.

Ultrasonic-assisted stripping of single-crystal SiC after laser modification

Laser stripping technology is an advanced processing method with high efficiency and low material loss, which can greatly reduce material loss in the production process of single-crystal SiC wafer, but the single-crystal SiC ingot still have a certain bonding force after laser modification. Ultrasonic vibration can reduce the bonding force and thus strip single-crystal SiC wafer. In order to investigate the effect of ultrasonic vibration on the reduction of the bonding force of single-crystal SiC internal modification layer, through the ultrasonic-assisted stripping of single-crystal SiC orthogonal experiment, the ultrasonic vibration parameters of ultrasonic frequency, vibration time and ultrasonic power of the three indexes of the reduction of the bonding force was analyzed. The results show that the bonding force of the modified layer decreased by 25 %–60 % after ultrasonic vibration. Variance analysis of the experiment results showed that the main factors influencing the bond strength reduction were vibration time and ultrasonic power in turn. When the vibration time is longer and the ultrasonic power is higher, the stripping force decreases more, and the stripping force of single-crystal SiC wafers decreases up to 60 % under the condition of vibration time of 5min and ultrasonic power of 700 W. Through analysis of the single-crystal SiC cross-section, distinct cleavage steps and cleavage channels are evident. The laser-modified region exhibits defect such as nano-pores, micro-cracks, and nano-particles.After the single-crystal SiC laser modification process was upgraded, the distance between the ultrasonic tool head and the single-crystal SiC was 1.5 mm can directly strip off the single-crystal SiC wafer. And eventually stripped 6-inch single-crystal sic wafers. Therefore, ultrasonic vibration can increase the internal defects in the single-crystal SiC modified layer, causing crack expansion to occur and ultimately stripping the single-crystal SiC wafer.

Influences of ultrasonic vibration directions, amplitudes, and frequencies on sapphire polishing studied by molecular dynamics

The sapphire surface morphology, atom removal rate, temperature, polishing force, subsurface damage, dislocation, and stress were explored under different ultrasonic directions, frequencies and amplitudes through molecular dynamics (MD). For both vertical and horizontal vibration, the rising ultrasonic frequency and amplitude will reduce the tangential and normal force, and increase the subsurface temperature and the material removal rate (MRR). Higher frequencies promote the basal dislocation, thus reducing the subsurface damage. Higher amplitudes cause thinner subsurface damage layer under horizontal vibration. However, it is opposite at vertical vibration. The horizontal vibration can obtain a flatter polished surface and a thinner subsurface damage layer due to the longer trajectory and less impact on sapphire surface. This study can provide reference for sapphire high-quality polishing.

Increasing the efficiency of coagulation in resonant gaps due to acoustic flow formation

Relevance. The urgent need to eliminate environmental pollution from industrial emissions of various solid particles. At the same time, maximum attention is paid to cleaning exhaust gases from particles of 2.5 microns in size or less. One of the most promising ways to increase the efficiency of existing gas purification equipment in capturing such particles is their coagulation by exposing the gas flow to high-intensity acoustic vibrations of ultrasonic frequency. However, at low concentrations, even at the maximum permissible sound pressure level, the coagulation efficiency of particles smaller than 2.5 microns is insufficient to increase the recovery rate of gas cleaning equipment. Therefore, there is an urgent need to find new ways to further improve the efficiency of ultrasonic coagulation of particles smaller than 2.5 μm. Aim. To determine the conditions for the formation of vortex flows in ultrasonic fields with the maximum ultrasonic influence in terms of sound pressure level. Conducting comparative studies of the coagulation of particles with a size of 2.5 microns with and without vortex flows. This will make it possible to determine the real values of increasing the efficiency of ultrasonic coagulation during turbulization of a gas-dispersed flow by acoustic flows in comparison with coagulation in a uniform ultrasonic field and without it. Objects. Coagulation of particles under the influence of homogeneous and inhomogeneous ultrasonic fields. Methods. Computer modeling of the formed ultrasonic field by the finite element method using harmonic acoustic analysis. The paper considers the experimental method for studying the process of combining particles under the influence of ultrasonic vibrations. To determine the characteristics of an aerosol during experimental studies, a TIPAS-1 meter based on the small-angle scattering method and the spectral transparency method was used. Results. The paper introduces the results of studies of coagulation of particles with a size of 2.5 microns or less in an ultrasonic field formed in resonant gaps by oscillating disk emitters. The authors proposed to increase the efficiency of coagulation in resonant gaps through the use of ultrasonic disk emitters capable of forming alternating zones of maximum and minimum amplitude oscillations in the resonant gaps. The creation of such zones ensured the formation of vortex-type acoustic flows capable of moving particles within the nodal regions of a standing wave and between them. The involvement of small particles in the formed flows made it possible to increase the probability of their collision. It was established that more effective ultrasonic coagulation provides an increase in the degree of inertial capture for particles of 2.5 microns in size by 6% – from 89 to 95%, for particles of 1.5 microns in size by 7% – from 85 to 92%, and for particles of 0.5 microns by 9% – from 76 to 85%.

Using gardenia pigment for ultrasonic natural dyeing of hemp fiber: A step towards sustainable dyeing

In recent years, with the country advocating the establishment of a resource-saving and environmentally friendly society, people have been pursuing a green and healthy quality of life. The non-toxic, harmless, and biodegradable characteristics of grass and wood dyeing have brought this method back to people's lives. Despite the presence of antibacterial substances such as tetrahydrocannabinol in cannabis fibers, they are still susceptible to microbial attacks. In recent years, scholars have conducted more research on the separation and purification of gardenia flower pigments, but there has been less analysis on the dyeing fibers and performance testing of gardenia flowers. The renewable characteristics, fewer side effects, and low cost increase the use of natural drugs as antibacterial agents in plant extracts or their active ingredients. This experiment used gardenia flowers as the raw material for dyeing experiments, and the dyeing percentage was used as the inspection index. Ultrasonic dyeing was carried out on hemp fibers after degumming treatment. It also aims to endow these dyed fabrics with natural antibacterial properties. During the sorting process, a liquid bath ratio of 1:20 was selected and experiments were conducted under different parameter variations. During the dyeing process, potassium aluminum sulfate (alum) is used as a mordant, and ultrasound is used as an auxiliary dyeing method. After dyeing, evaluate the fibers based on the percentage of exhaustion of obtained fiber and antibacterial activity against Staphylococcus aureus and Escherichia coli. At the same time, the FT-IR analysis, strength, and color fastness of the sorted samples were also checked. Single factor experiments were conducted by controlling the ultrasonic frequency, dyeing temperature, time, and mordant concentration to analyze the effect of gardenia pigment on the dyeing percentage. Response surface design experiments were used to optimize the dyeing process parameters. The research results indicate that the optimal process conditions for dyeing gardenia flowers are ultrasonic power of 85 %, dyeing temperature of 77 ℃, dyeing time of 60 min, and mordant concentration of 15 g/L. The main and secondary order of factors affecting the dyeing effect of hemp fibers is: mordant concentration>ultrasonic power>dyeing temperature. After optimal dyeing process, the hemp fiber shows a bright yellow color with a dyeing percentage of 57.32 %. The single fiber strength is not affected, and the color fastness to water washing and sun exposure meets the requirements for consumption. The infrared spectrum shows good dyeing effect. It has a certain antibacterial effect on Staphylococcus aureus, but the antibacterial effect on Escherichia coli is not significant. Due to these processes, it has been determined that hemp fiber can obtain antibacterial activity through the use of gardenia flowers and can be effectively colored.

Characterization of ultrasonic vibration and polishing force in sapphire ultrasonic vibration-assisted flexible polishing: Insights from in-situ monitoring systems

Sapphire ultrasonic vibration-assisted flexible polishing (UVAFP) is a promising technique for comprehensively improving the surface integrity of machined parts. The technique was performed on an ultra-precision machine tool with the in-situ monitoring systems in this paper, which aims to provide a new perspective for understanding the material removal mechanisms in the sapphire UVAFP process. A Taguchi L9 (43) orthogonal experiment was conducted to investigate the effects of feed distance, spindle speed, ultrasonic vibration (UV), and polishing time on the surface finish and material removal in the process. In addition, the effect of a polyurethane ball tool is not trivial. A single-factor experiment was conducted for exploring it. Based on a laser displacement measurement system and an acoustic emission sensor system, the characteristics of time-dependent ultrasonic amplitude and ultrasonic frequency for the sapphire UVAFP system were analyzed, with the effectiveness of UV demonstrated. Based on a three-component force measurement system, the characteristics of normal force and its relationship with process parameters and tool deformation were analyzed, with macro- and micro-level examined. In conclusion, this paper presents the characterization of UV and polishing force in the sapphire UVAFP process, providing novel insights into understanding the material removal mechanisms of sapphire and even more manufacturing problems.

High frequency venting of MEMS ultrasonic transducers and sensors: materials solutions.

Abstract This paper introduces the concept of ultrasonic venting. Similar to acoustic vents, ultrasonic vents refer to the aperture in air-coupled MEMS ultrasonic transducers (either PMUT or CMUT) intended to allow the equalization of internal and external pressures, the transfer of heat and the pass of ultrasonic waves, while impeding the penetration of fluids or particles that can affect the transducer membrane. To that end, vents are covered with a porous membrane whose properties are tuned to meet the afore mentioned requirements. The main difficulty in ultrasonic venting, compared with acoustic venting, is that the required “transparency” to ultrasonic waves is much more difficult to achieve. This involves two main problems as both transmission loss and frequency distortion are much larger at ultrasonic frequencies than in the audio range. The objectives of this paper are: to measure the response of acoustic venting materials in the ultrasonic frequency range, to determine the usability of these materials in ultrasonic vents, and to extract useful information for the design of efficient ultrasonic venting materials. Transmission coefficient spectra of different acoustic venting materials is measured in the frequency range 0.2 –2.7 MHz. The origin of the ultrasonic losses and frequency distortion are analysed as well as the role of mode conversion, internal interferences, modes interference, etc. Results reveal that none of the acoustic venting materials analysed can be used in ultrasonic venting applications, but the obtained knowledge about the response of these materials in the ultrasonic frequency range permit to advance in the selection of successful candidate materials for this application.

Optimisation and numerical simulation of ultrasonic reactor in hydrometallurgical process

ABSTRACT In this paper, COMSOL Multiphysics software is used to carry out simulations to visualise the distribution of the acoustic field and sound pressure in the reaction cavity for different ultrasonic frequencies, powers, reaction cavity shapes, ultrasonic horn diameters and ultrasonic horn action depths. The results indicate the ultrasonic frequency affects the uniformity of the acoustic field distribution, and the ultrasonic power affects the magnitude of the sonic pressure. Taking into account that the sonic pressure is not less than the cavitation threshold, the sound field is evenly distributed, and it is energy-saving and environment-friendly. The optimal simulation conditions are obtained. In a 500 mL cylindrical reaction chamber, the ultrasonic frequency and power are 25 kHz and 130 W, respectively. The diameter of the ultrasonic horn is 34 mm, and the depth of action is 30 mm. Under these conditions, the maximum sound pressure reaches 1.08 × 106 Pa.

Battery state characterization based on a contactless electromagnetic ultrasound testing method

Nondestructive ultrasonic detection technology has been increasingly applied to battery diagnostics. However, currently used ultrasonic transducers must be affixed to the tested battery very tightly through coupling agents, thereby lowering the test efficiency and convenience. In this paper, a contactless electromagnetic ultrasonic testing technology is proposed for characterizing the states of lithium-ion batteries. The relationship between the ultrasonic frequency and wave velocity is analyzed via a finite element model. Meanwhile, the influence of battery boundary characteristics on ultrasonic signals is investigated. Based on the propagation characteristics of ultrasonic guided waves in the battery, contactless electromagnetic acoustic transducers (EMATs) are designed and optimized. Three features, including the time of flight, signal amplitude, and energy integration, are extracted from the received signals to indicate the variation in battery state during charging and discharging cycles. Experimental results demonstrate that the ultrasonic guided wave features obtained from EMATs change consistently and regularly with the charging and discharging states of the battery. The proposed method can be used to analyze the aging of batteries and the inconsistency of electrolyte infiltration inside batteries, which is expected to improve the battery safety.

Effect of ultrasonic frequency on mass transfer of acoustic cavitation bubble

Mass transfer of acoustic cavitation bubble is numerically investigated focusing on ultrasonic frequency. In the present simulation, transport of chemical specie from an acoustic cavitation bubble after rapid bubble compression is modeled. The simulation results indicate that the bubble oscillation is more nonlinear, and the oscillation amplitude becomes larger with sound pressure amplitude, ultrasonic frequency, and bubble size. Under the condition of strong nonlinear bubble oscillations, the bubble shape becomes non-spherical. The mass transfer of chemical specie becomes smaller with sound pressure amplitude at 20 kHz ultrasound due to shell effect and area effect, although it becomes larger with pressure amplitude at higher ultrasonic frequency because the concentration of chemical specie in the bubble becomes high near the periphery of bubble due to hysteresis effect, which becomes remarkable especially at higher ultrasonic frequency because time for the bubble compression becomes too short for chemical specie to diffuse at higher ultrasonic frequency.

Machine learning predict the degradation efficiency of aqueous refractory organic pollutants by ultrasound-based advanced oxidation processes

Ultrasound based advanced oxidation processes (AOPs) are effective for removing refractory organic pollutants by generating reactive species. Machine learning (ML) can systematically provide an excellent opportunity to determine the relationship between feature variables and output variables through large amounts of data, thereby reducing the need for experimental measurements. In this study, a ML approach was applied for the first time to predict the degradation efficiency of aqueous refractory organic pollutants by ultrasound-based AOPs. The obtained dataset was normalized and introduced into four ML models. Among them, Random Forest Regressor and XGB Regressor models had the best fit with 0.9546 and 0.9749 for training set R2 and 0.9548 and 0.9740 for test set R2, respectively. Relative importance analysis and SHAP analysis showed that catalyst type, oxidant concentration, reaction time, and catalyst dosage are the important variables affecting the degradation efficiency of refractory organic pollutants. In addition, excessive ultrasonic intensity, ultrasonic frequency, oxidant concentration, and catalyst dosage had little effect on the increase of degradation efficiency. Based on the descriptive data analysis, high degradation efficiency was obtained with ultrasonic intensity of 2 W·mL−1, ultrasonic frequency of 20–40 kHz, reaction time of 60–90 min, pH 3–7, oxidant concentration of ∼7.5 mmol·L−1, and catalyst dosage of >0.4 g·L−1. This work demonstrated a new predictive method to understand the comprehensive influence of operative factors on degradation efficiency in US-based AOPs, guiding parameter and process optimization.

On the notch sensitivity of as‐built Laser Beam Powder Bed–Fused AlSi10Mg specimens subjected to Very High Cycle Fatigue tests at ultrasonic frequency up to 109 cycles

AbstractThe notch effect significantly influences the fatigue response of components and is particularly relevant for parts produced with additive manufacturing (AM) processes, characterized by complex geometries and possible geometric discontinuities inducing local and critical peak stresses. Moreover, the low surface quality, as well as manufacturing defects and residual stresses, interacts with the local peak stress induced by geometric discontinuities, complicating the assessment of the notch effect for AM parts and requiring extensive experimental fatigue investigations. In the present paper, the notch sensitivity of as‐built AlSi10Mg specimens produced with the laser beam powder bed fusion in the Very High Cycle Fatigue regime is investigated. Ultrasonic fatigue tests up to 109 cycles have been carried out on rectangular bars and rectangular bars with a central through‐thickness hole. The notch effect has been found to significantly affect the fatigue response of the investigated AlSi10Mg specimens, with surface defects having a main role and pointing out the influence of the surface quality on the crack formation.

Substantiation of wild plants used as functional ingredients in the technology of crisp grain bread

Research on the nutritional content of wild plant fruits in Kazakhstan, including Hawthorn fruit (Crataegus laevigata), rosehip fruit (Rose canina L. variety), sea buckthorn fruit (Hippophae rhamnoides - Altai variety), and black chokeberry fruit (Aronia melanocarpa), has determined that these fruits possess a combination of properties essential for maintaining human health, attributed to the presence of bioactive substances (BAS) and other components. The technological process for obtaining extracts and concentrates from wild-growing raw material fruit has developed. The following extraction modes were proposed: ultrasonic wave frequency 40 kHz, extraction time 30 minutes, temperature 500С, and concentration of the obtained extracts was carried out by vacuum evaporation method, using IKA RV-10 apparatus at 40-50°С and pressure 800 mbar. Found that extracts and concentrates have a higher concentration of nutritional substances when compared to the fruits themselves. Thus, the vitamin C content in hawthorn fruits was 27.8 mg, while in the extract, it was 47.84 mg, and in the concentrate – 62.19 mg. The vitamin C content in rosehip fruits, extracts, and concentrates was 578.01 mg, 811.8 mg, and 1101.3 mg, respectively. The vitamin C content in sea buckthorn fruits, extracts, and concentrates was 285.05 mg, 518.8 mg, and 640.9 mg, respectively. The vitamin C content in black chokeberry fruits, extracts, and concentrates was 86.2 mg, 128.8 mg, and 160.5 mg, respectively. A similar increase was observed for the content of vitamin E and other components. Furthermore, the obtained concentrates meet the safety parameters required by regulatory documents. A technology for producing grain crispbread using the extrusion method has developed, incorporating whole grains, groats, flavouring additives, and concentrates derived from wild fruits such as hawthorn, rosehip, sea buckthorn, and black chokeberry into the recipe.

The use of non-invasive tomographic imaging to monitor lung condition

The development of ultrasound tomography (UST) aimed to significantly enhance the precision and safety of non-invasive UST imaging, particularly for studying crystallization processes in biological tissues. The initiative sought to address the limitations of previous versions by incorporating advanced technological upgrades and providing a more user-friendly interface. The revised system comprises eight four-channel measurement cards interconnected via a high-speed FD CAN bus capable of 8 MBPS data transfer. Each card features a dedicated square wave generator, band-pass filters tailored to specific ultrasonic transducer frequencies, and a sophisticated signal envelope processing unit. The core processing unit is built around a 32-bit STM32G474RE microcontroller, ensuring robust data handling and image reconstruction capabilities. The UST device presented demonstrates improved image clarity and reduced noise interference. The measurement card redesign has achieved a sampling rate of 4 MBPS per channel and includes a two-stage amplification for dynamic range management. Upgraded power components, comprehensive shielding, and the integration of advanced analog switches have led to an enhanced signal-to-noise ratio, pivotal for high-resolution imaging. The advancements presented in the UST device mark a noteworthy progression in ultrasound imaging technology, extending beyond traditional applications. High-speed data collection, precise signal processing, and user-centered design have all come together to make a system that can image crystallization processes more accurately and accurately over and over again.