Deposition System Research Articles

Effects of Diethoxymethylsilane/Helium Flow Rate Ratio on Low-k Films Deposited by Plasma-Enhanced Chemical Vapor Deposition

As the semiconductor industry has continuously reduced the integrated circuit (IC) chip size, a resistance-capacitance (RC) delay emerged, causing deterioration of the chip performance. To reduce the RC delay, low dielectric constant (low-k) films with suitable mechanical strengths have been adopted as intermetal dielectrics (IMDs). In this study, low-k plasma-polymerized diethoxymethylsilane (ppDEMS) films were fabricated by plasma-enhanced chemical vapor deposition of the DEMS precursor with a flow rate ratio of the DEMS precursor to helium (He) carrier gas (DEMS/He FRR) as a key parameter. As the DEMS/He FRR increased, the refractive index was reduced from 1.401 to 1.386, and the k value decreased from 2.77 to 2.10. From high-resolution scans of C1s, O1s, and Si2p peaks of X-ray photoelectron spectroscopy, the carbon contents increased, and the oxygen contents decreased, along with a decrease in the film density. With the increased DEMS/He FRR, hardness decreased from 2.5 to 1.8 GPa, and elastic modulus decreased from 17.08 to 11.50 GPa. Leakage current densities for all the ppDEMS films were less than 10−7 A cm−2 at 1 MV cm−1. The ppDEMS films could be suggested as the IMDs according to their electrical and mechanical performance.

Low-temperature epitaxial SiGe:P for gate-all-around n-channel metal-oxide-semiconductor devices

This study investigates the viability of Si1−x Ge x :P (x ≤ 0.3) as a novel source/drain material for n-channel Metal-Oxide-Semiconductor for Gate-All-Around (GAA) transistors, addressing the challenges posed by the evolving semiconductor technology. Utilizing a reduced-pressure chemical vapor deposition system, undoped SiGe with low Ge contents were grown at temperatures of ≤500 °C. The addition and optimization of phosphorous doping using phosphine results in improved surface morphology and increased active carrier concentration. The study compares Si1−x Ge x :P with different silicon precursors and temperatures, emphasizing the potential for maintaining high growth rates at lower temperatures when using Si3H8. Ti/Si1−x Ge x :P stacks reveal a promising reduction in contact resistivity with decreasing the Ge content, particularly when incorporating thin Si:P cap layers at the Ti/Si1−x Ge x :P interface. This comprehensive study highlights the potential of Si1−x Ge x :P as an alternative material for advanced GAA transistor technologies, offering improved mobility and meeting the thermal budget requirements.

Plasma surface treatment of amorphous Ga2O3 thin films for solar-blind ultraviolet photodetectors

Recently, amorphous gallium oxide (a-Ga2O3) thin films are gaining more and more attention due to their advantages of low cost and low temperature growth. However, a-Ga2O3 solar-blind ultraviolet photodetectors are plagued by issues such as slow response speed and high dark current. In this work, radio frequency magnetron sputtering was used for a-Ga2O3 deposition, and a novel approach of plasma treatment (including oxygen, argon and hydrogen plasmas) was employed to tailor the device performance using a plasma-enhanced chemical vapor deposition system. It is demonstrated that: (i) the oxygen atoms and ions in the oxygen plasma effectively reduce the oxygen vacancy concentration and improve the respond speed of a-Ga2O3 photodetectors; (ii) the argon ions in the argon plasma create additional defects (such as dangling bonds and oxygen vacancies) and improve the responsivity of a-Ga2O3 photodetectors; (iii) the hydrogen atoms in the hydrogen plasma may incorporate into the film and form an ultra-thin passivation layer near the surface, which gives rise to a balance between responsivity and response speed. Finally, through the detailed analysis of the optical emission spectra and photoelectric performance, the underlying physical mechanism based on the energy band diagram has been proposed to interpret the obtained experimental results.

Solving East Nile Delta's imaging challenges through new ocean-bottom-node acquisition and advanced imaging

The East Nile Delta, located offshore Egypt, is a challenging area for seismic imaging due to the presence of substantial velocity heterogeneity created by the complex Messinian unconformity and overlaying fault structures. Existing towed-streamer (TS) seismic data have been pushed to their technical limit but remain insufficient for adequate representation of the subsurface. Previous studies have shown that a step change in imaging is possible if advanced acquisition, processing, and velocity model building techniques are employed. Atoll Field is a candidate to benefit from such improvements in seismic data. Results show that ocean-bottom-node acquisition provides improved spatial sampling and higher resolution. Acquiring seismic data with offsets of more than 30 km facilitated the generation of a robust high-frequency velocity model that better captures subsurface complexity. This paper outlines the acquisition and processing, with a focus on the velocity model building process. The generated subsurface model is effectively used for imaging with conventional migration algorithms and full-waveform-inversion-derived reflectivity. Results show a significant step change from previous TS images at the Oligocene target, with channel features clearly imaged. This provides an improved understanding of the depositional systems and reduced depth uncertainty.

Seismic sedimentology analysis of meter-scale thin sand bodies in the Jurassic Qigu Formation, Yongjin area, Junggar Basin

Seismic sedimentology is an interdisciplinary field that integrates sedimentary geology and geophysics to accurately characterize the spatial and temporal distributions of sedimentary systems. This paper focuses on the Qigu Formation in the Yongjin area of the Junggar Basin, China. The objectives are to establish a high-resolution sequence stratigraphic framework and to clarify the types of sedimentary systems present. Various technical methods, including 90° phase adjustment, attribute clustering, red-green-blue attribute fusion, stratal slicing, and seismic phase-controlled waveform indication inversion, are employed to restore the vertical evolution history of the sedimentary system and quantitatively characterize the spatial-temporal distribution of the thin sand bodies in the Qigu Formation. The results revealed that the Qigu Formation is divided into a third-order sequence, consisting of a lowstand systems tract and a lacustrine transgressive systems tract. During the lowstand systems tract, a thick channel sand body developed in the delta front, exhibiting a non-muddy, intermittent normal grading structure. The lacustrine transgressive systems tract features thin, discontinuous channel sand bodies with mud layers, also forming an intermittent normal grading structure. Two distinct types of delta fronts are identified: the first, formed during the lowstand systems tract, is characterized by branching subaqueous distributary channels in a shallow-water environment. The second, associated with the lacustrine transgressive systems tract, displays a network-like distribution of subaqueous distributary channels in a relatively deeper-water environment.

Influence of printing parameters on the mechanical behavior of 3D-printed SS316L parts manufactured using laser hot wire directed energy deposition

Hybrid manufacturing combines the simultaneous benefits of additive manufacturing (complex geometries, part consolidation, and mass customization) with the advantages of subtractive manufacturing (superior surface finish and enhanced dimensional accuracies) by integrating a suite of complementary traditional processes into a base platform of additive manufacturing. The use of hybrid technology has grown in recent years given its capabilities on repairing metallic structures, producing parts with conformal cooling features, and manufacturing functionally graded products. These kinds of capabilities are of great interest to the medical implant, energy, automotive, maritime, and aerospace industry sectors, among many other fields. This work investigated the mechanical properties of stainless steel (SS) 316L as a function of different tool paths strategies using an integrated 5-axis CNC hybrid Mazak system with a laser hot wire deposition system (LHWDS). This study includes the evaluation of different printing parameters and their impact on the quality of the printed bead as well as the incorporation of a structure–property material relationship based on the mechanical performance of the manufactured coupons.

Development of an integrated online deposition and corrosion monitoring system in a full-scale solid waste CFB boiler

Solid waste incineration is a clean and sustainable approach for solid waste management. However, ash deposition and corrosion remain a critical issue due to fuel’s inherent enrichment of alkali chlorine. This study develops an integrated online deposition and corrosion monitoring system to enhance the operational safety and efficiency of solid waste incineration boilers. This system combines linear polarization resistance (LPR) for corrosion rate estimation with heat flux measurements for ash deposition analysis. It can offer a novel approach for real-time monitoring of heat exchangers’ safety during solid waste combustion. It was deployed in a full-scale circulating fluidized bed (CFB) boiler that purely combust solid wastes. Key findings demonstrate the system’s capability to deliver continuous, real-time data, crucial for the dynamic control of combustion processes and the maintenance of heat transfer surfaces. Its robust diagnostic capabilities were evident across various scenarios. Specially, initial corrosion rates sharply increase with deposition rates due to the enrichment of alkali chlorine on inner deposit layer, in which chlorine serves as a catalyst, facilitating the rapid penetration and aggravation of corrosion by other agents. As deposit further buildup, the corrosion rate steadily decreases along with surface temperature, highlighting a dynamic interaction. Moreover, measured corrosion rates can quickly response to temperature variations. Such multi-process online monitoring system provide more possibilities to investigate the inherent interaction between deposition and corrosion. Therefore, this work offers insights that could significantly influence operational strategies, maintenance protocols, and the overall reliability of waste-to-energy technologies.

Hydrodynamic Model of the Area of the Żelazny Most Mining Waste Storage Facility to Reconstruct the Migration of Saline Groundwater

This paper presents the construction of a numerical three-dimensional model of the area of the Żelazny Most Mining Waste Storage Facility (MWSF). In the study area, the difficult geological conditions associated with glaciotectonics are accompanied by a complex hydrotechnical system of sediment deposition and sedimentary water drainage. In order to effectively reflect the water flow paths, a detailed schematization was carried out, using 700,000 boreholes and more than 300 hydrogeological cross-sections. In addition, numerous drainage sections, streams, and ditches were included to reliably assess the amount of saline water entering the underlying aquifers. This research was supported by magnetic resonance sounding (MRS) studies of the reservoir’s sediments. The MWSF is currently being expanded, so the work primarily focuses on illustrating changes in the hydrodynamic field resulting from the inclusion of the new southern section. Models of similar facilities have been implemented before, but in the current one, the combination of meticulous analysis of the hydro-structural system, the water balance, a significant amount of data, the size of the facility, and the use of an unstructured discretization grid in the calculations is undoubtedly innovative and will be an important contribution to the development of analogous solutions around the world.

Utilization of graphene nanoplatelets for friction coefficient reduction in NiCu/WC-12Ni composite materials

Graphene Nanoplates (GNPs), known for their outstanding performance, have found extensive applications in the preparation of metal composite carbon materials. In this investigation, a Directed Energy Deposition system was employed to effectively produce deposition specimens of NiCu/WC-12Ni + x wt% GNPs (x = 0, 0.5, 1.0, 1.5) composite material. The findings suggest that incorporating GNPs improved the microstructure of the NiCu/WC-12Ni deposited specimens, leading to a reduction in grain size with predominantly equiaxed and cellular grains. GNPs transformed into amorphous graphene spheres, uniformly distributed within the deposited structure. When 1 wt% GNPs were added, the average microhardness of the deposited specimens increased by approximately 15 %, the friction coefficient decreased from the original 0.318 to 0.257, and the wear rate decreased by 23.2 %. The primary wear mechanism observed was abrasive wear, demonstrating excellent wear resistance. Moreover, introducing a suitable quantity of graphene improved the electrochemical corrosion resistance of the deposited specimen.

High-Volume SiC Epitaxial Layer Manufacturing-Maintaining High Materials Quality of Lab Results in Production

Typically, research and development (R&D) results of epitaxial layer growth show superior properties of the grown layers compared to high volume results. Layer uniformities are excellent and achieved defect densities are low compared to typical results. In particular, the conversion of basal plane dislocations (BPD) from the silicon carbide (SiC) substrate is in focus to reduce bipolar degradation of p-n-junctions. It is a great challenge to maintain those excellent results in high-volume manufacturing considering all the factors that impact the properties of the epilayer. Thus, quality of the layers, high throughput and low cost have to be assessed to find a compromise between these key factors. In this paper we present results on the growth of epitaxial layers on 150 mm and 200 mm 4° off-oriented 4H-SiC substrates using warm-wall multi-wafer chemical vapor deposition (CVD) systems. Single wafer data of the key epitaxial layer parameters, thickness, doping and defect densities, are compared to batch and lot results, as well as to statistical data of several hundreds of wafers produced. Improvements in wafer-to-wafer (w-t-w) doping uniformity could be achieved for instance by implementation of an on-wafer temperature measurement. Substrate impact on defect levels is shown comparing X-ray topography (XRT) results of bare substrate wafers and defect analysis of epilayers on sister wafers from the same crystal. Statistical defect data and resulting predicted yield loss also show a dependence on substrate suppliers. For the first time we show w-t-w and run-to-run (r-t-r) results of doping and thickness measurements on 200 mm substrates. Also, defect results of epilayers on 200 mm wafers are compared to results on 150 mm.

Investigating relationships between shoreline process regime, shelf-margin architecture, and deep-water sand delivery: Insights from the early post-rift Hammerhead shelf margin (Bight Basin, southern Australia)

Shelf margins represent a crucial area along source-to-sink systems where sediments are partitioned from the shelf to slope and basin-floor areas. Reconstructing the evolution of these depositional systems is key for interpreting the interplay between past accommodation and sediment supply, and sediment dispersal mechanisms into deep water. In the Bight Basin, on the southern margin of Australia, the Hammerhead shelf margin prograded during the Late Cretaceous following break-up between Australia and Antarctica. This understudied interval offers important insights into source-to-sink processes in a post-rift, greenhouse, high sediment supply setting. A dynamic stratigraphic approach using high-resolution 3D seismic data across the Hammerhead shelf margin has been used to quantitatively characterise 28 clinothems developed over ∼ 1.9 Myrs each with an average duration of ∼ 67,000 years. By applying a shallow-marine process-based classification to shorelines, alongside quantitative analysis of the architecture of their coeval deep-water deposits downdip, statistical relationships and clear links between shallow-marine processes, stratigraphic architecture, and deep-water sand delivery are revealed. A statistically significant relationship between fluvial dominated shorelines, high slope gradients, and mass-transport deposit development is demonstrated, as is a requirement for fluvial influence at the shoreline for the initiation of long run-out turbidite systems. These long run-out turbidite systems are interpreted to have been formed by repeated density flows which lead to greater sediment transfer efficiency and increased sediment supply. This research has direct application to improve prediction of reservoir locations within the Bight Basin for resource exploration and/or carbon sequestration and may also be applied to improve deep-water sediment predictability in other basins worldwide developed in similar tectonic and climatic settings.

Mapping Ocean Gateways from 3D Seismic Data Using Color Processing and Analogues from Seismic Data

Mapping sedimentary features to delineate ancient ocean gateways from 3D seismic data has long been a challenge due to their limited vertical resolution. We present the technique of color processing of seismic data which improves the vertical resolution to very few seismic samples corresponding to 5–10 m. The result is a representation of the seismic impedance contrast correlation in Red-Green-Blue (RGB) colors, which creates images similar to satellite images that assist the geological interpretation because the RGB colors can be associated with mud-rich and sand-rich sediments. Using this approach, we have extracted six different sedimentary bedforms from different bottom flow settings and correlated these with the bedform-velocity matrix by Stow et al. (2009). Then we studied bedform assemblies in their regional context for the area covered by the 3D seismic data set. We conclude with comparing a modern and an ancient analogue – both from 3D seismic data – and infer paleo flow direction and velocity using oceanographic measurements available for the modern analogue. The method provides insights into ocean bottom currents and their impact on the formation of contourite depositional systems in modern and ancient ocean gateways which contribute to the reconstruction of the paleoclimate as an input to present day climate change models.

Occurrence and Favorable Enrichment Environment of Lithium in Gaoping Coal Measures: Evidence from Mineralogy and Geochemistry

The Carboniferous-Permian coal measure strata in the Qinshui Basin exhibit highly lithium (Li) enrichment, with substantial exploitation potential. To further explore the enrichment mechanism of lithium in coal measure strata, the No. 15 coal of the Taiyuan Formation from the Gaoping mine is taken as the research object, and its mineralogical and geochemistry characteristics are evaluated using optical microscopy, X-ray diffraction, scanning electron microscopy, inductively coupled plasma mass spectrometry, X-ray fluorescence, and infrared spectral. The results show that the No. 15 coal is semi-anthracite coal with low moisture, low ash, low volatility, and high sulfur. Organic macerals are primarily vitrinite, followed by inertinite, and liptinite is rare; the inorganic macerals (ash) are dominated by clay minerals (predominantly kaolinite, cookeite, illite, and NH4-illite), calcite, pyrite, quartz, siderite, gypsum, and zircon. The average Li content in the coal is 66.59 μg/g, with higher content in the coal parting (566.00 μg/g) and floor (396.00 μg/g). Lithium in coal occurs primarily in kaolinite, illite, cookeite, and is closely related to titanium-bearing minerals. In addition, Li in organic maceral may occur in liptinite. The No. 15 coal was formed in the coastal depositional system, and the deposition palaeoenvironment is primarily a wet–shallow water covered environment in open swamp facies; the plant tissue preservation index is poor, and aquatic or herbaceous plants dominate the plant type. The reducing environment with more terrestrial detritus, an arid climate, and strong hydrodynamic effects is favorable for Li enrichment in coal. The results have important theoretical significance for exploring the enrichment and metallogenic mechanisms of Li in coal.

Geological Conditions of Shale Gas Accumulation in Coal Measures

The shale of different potential layers is studied by using rock pyrolysis analysis, total organic carbon determination (TOC), kerogen microscopic component identification, mineral X-ray diffraction, scanning electron microscopy, and low-temperature nitrogen adsorption experiments. The results are as follows: (1) Shishui Formation of the Lower Carboniferous and Longtan Formation of the Upper Permian are the two most important shale gas reservoirs in the Chenlei Depression. The sedimentary environment of the target shale is a marine land interaction facies coastal bay lagoon swamp sedimentary system. Two sedimentary facies of tidal flat facies, subtidal zone, and lagoon swamp facies are developed. (2) The organic matter types of shale are Type III and II2, with TOC content greater than 1%. The maturity of shale samples is relatively higher (Ro,max is above 2%), which means they have entered the stage of large-scale gas generation. The overall brittle mineral content of the target shale sample is relatively higher (above 40%), which is conducive to artificial fracturing and fracture formation in the later stage, while an appropriate amount of clay minerals (generally stable at 40%) is conducive to gas adsorption. (3) The overall pore structure of the water measurement group and Longtan group is good, with a higher specific surface area and total pore volume (average specific surface area is 12.21 and 8.36 m2/g, respectively), which is conducive to the occurrence of shale gas and has good adsorption and storage potential. The gas content of the water measurement group and the Longtan Formation varies from 0.42 to 5 cm3/g, with an average of 2.1 cm3/g. It indicates that the water measurement group and the Longtan Formation shale gas in the study area have good resource potential.

Long-term stability of sediment routing on an active continental margin: Insights from detrital zircon U-Pb ages and measured stratigraphy of Carboniferous to Miocene strata, Sierra de Narváez, NW Argentina

The complex Phanerozoic tectonic evolution of the western margin of South America, including extensional, neutral, and contractional deformation regimes, provides an opportunity to test how sedimentary systems were affected by variable tectonics on a long-lived active margin. Here, we report new geologic mapping, measured stratigraphic sections, paleocurrent measurements, and detrital zircon U-Pb ages from the Fiambalá area, NW Argentina, that together constrain the evolution of sediment routing and basin systems of the northern Sierras Pampeanas during Carboniferous to Miocene time. Carboniferous to Triassic strata of the Paganzo Group include fluvial, lacustrine, and eolian intervals deposited in an extensional setting with SSW-directed paleocurrent orientations. The Mesozoic El Pedernal Formation consists of a lower, basalt interval and an upper, conglomerate and sandstone interval, which has a new detrital zircon maximum depositional age of ca. 88 Ma. Observed strata of the Miocene Tambería Formation include fluvial to eolian sandstones of the lower member of the formation and alluvial conglomerates of the middle member. Whereas lower member Tambería fluvial strata have SSW-oriented paleocurrents, middle member conglomerates indicate broadly E-directed paleoflow.Detrital zircon age distributions of the Paganzo Group, El Pedernal Formation, and Tambería Formation are remarkably consistent, with dominant age peaks ca. 1.3–0.9 Ga and ca. 660-450 Ma. The ages and relative magnitudes of these peaks are consistent with derivation from igneous sources associated with Choiyoi magmatism (330-215 Ma), the Famatinian (490-450 Ma) and Pampean (540-510 Ma) orogens, basement of the MARA block (ca. 1.3–0.9 Ga), and recycling of Neoproterozoic to Cambrian sedimentary successions derived from central Gondwana (ca. 1.3–0.9 Ga, 650-590 Ma, 540-510 Ma).The consistent paleocurrent orientations and detrital zircon U-Pb ages of the Carboniferous Paganzo Group to the Miocene lower member of the Tambería Formation suggest that a S-directed axial drainage network with a consistent sediment source area persisted in the region for ∼300 Myr. This axial drainage network was succeeded by an E-directed transverse drainage network initiated between 15 Ma and 8 Ma due to growth of the Andean thrust wedge, coeval with tectonic compartmentalization and drainage modification of nearby foreland depocenters. These findings highlight the potential for long-term persistence of drainage networks on continental margins under changing tectonic regimes.

Conveyor CVD to high-quality and productivity of large-area graphene and its potentiality

The mass production of high-quality graphene is required for industrial application as a future electronic material. However, the chemical vapor deposition (CVD) systems previously studied for graphene production face bottlenecks in terms of quality, speed, and reproducibility. Herein, we report a novel conveyor CVD system that enables rapid graphene synthesis using liquid precursors. Pristine and nitrogen-doped graphene samples of a size comparable to a smartphone (15 cm × 5 cm) are successfully synthesized at temperatures of 900, 950, and 1000 °C using butane and pyridine, respectively. Raman spectroscopy allows optimization of the rapid-synthesis conditions to achieve uniformity and high quality. By conducting compositional analysis via X-ray photoelectron spectroscopy as well as electrical characterization, it is confirmed that graphene synthesis and nitrogen doping degree can be adjusted by varying the synthesis conditions. Testing the corresponding graphene samples as gas-sensor channels for NH3 and NO2 and evaluating their response characteristics show that the gas sensors exhibit polar characteristics in terms of gas adsorption and desorption depending on the type of gas, with contrasting characteristics depending on the presence or absence of nitrogen doping; nitrogen-doped graphene exhibits superior gas-sensing sensitivity and response speed compared with pristine graphene.

Facies distribution, paleoenvironment and hydrocarbon potential of Kanawa Member of Pindiga Formation, Gongola Basin, Northern Benue Trough, Nigeria

The Gongola sub-basin is a frontier inland sedimentary basin consisting of Cretaceous to Tertiary sediments, believed to have been deposited in continental to coastal shallow marine complex. The Kanawa Member of Pindiga Formation is a sequence of limestone and shale. Sedimentology, facies analysis, biostratigraphy, thermal maturity assessment and kerogen typing were conducted on these strata to determine the facies, facies associations, facies successions, paleoenvironment, age, and hydrocarbon generation potential. The studied sequences are of Turonian–Santonian age, deposited due to a major transgression of the basal part of the Pindiga Formation. The shale-limestone series of the Kanawa Member is interpreted as lagoon-to-shallow marine deposits of a carbonate ramp depositional system. The sediments consist of mainly wackestone and packstone facies and shallow marine foraminiferal, suggesting that the Kanawa Member was deposited under low-energy condition. The presence of Ammobaculites subcretacea, Haplophragmoides bauchensis, Haplophragmoides pindigensis, Haplophragmoides excavata, Ammobaulites pindigensis, Ammobaculites bauchensis, Ammobaculites gombensis, Ammobaculites benuensis Ammoastuta nigeriana, Reophax guineana and Miliammina pindigensis foraminiferal assemblages, indicating Late Cretaceous age. Hydrocarbon potential is interpreted to be gas prone although, minor oil could be expected. These correspond to temperature range (TAI values) of 60 to 75 indicating thermally matured for both oil and gas generation.

Sedimentology and stratigraphy of lower Cretaceous fluvial to shallow marine deposits on the central Atlantic passive margin: The Aaiun-Tarfaya Basin, Morocco

This paper presents the first integrated regional outcrop-based sedimentological study of the northern Aaiun-Tarfaya Basin located in Morocco (NW Africa). The Lower Cretaceous Tan-Tan Formation has been subdivided into six new members and placed within a sequence stratigraphic framework that includes two incomplete depositional sequences. Strong thickness variations of individual lithostratigraphic units from north to south suggest differential subsidence during sedimentation and/or the existence of major topography on the basal unconformity that the succession onlaps. The results provide valuable insights into the timing of local tectonics in the Western Anti-Atlas and the control on the evolution of the sedimentary system. Deposition of each of these six units is interpreted to be the result of a complex interplay between an overall eustatic sea-level rise during the early Cretaceous, sediment delivery controlled by tectonic movements in the Western Anti-Atlas and Reguibat Shield and periods of differential subsidence in the basin. The results document the style of evolution of a back-stepping wave-dominated system feeding into the Central Atlantic during the passive margin phase. The improved facies and depositional models together with improved understanding of the evolution of the delta have significant implication for exploring the deep-water equivalents offshore.

Development of an advanced in-line multilayer deposition system at Diamond Light Source.

A state-of-the-art multilayer deposition system with a 4200 mm-long linear substrate translator housed within an ultra-high vacuum chamber has been developed. This instrument is engineered to produce single and multilayer coatings, accommodating mirrors up to 2000 mm in length through the utilization of eight rectangular cathodes. To ensure the quality and reliability of the coatings, the system incorporates various diagnostic tools for in situ thickness uniformity and stress measurement. Furthermore, the system features an annealing process capable of heating up to 700°C within the load-lock chamber. The entire operation, including pump down, deposition and venting processes, is automated through user-friendly software. In addition, all essential log data, power of sputtering source, working pressure and motion positions are automatically stored for comprehensive data analysis. Preliminary commissioning results demonstrate excellent lateral film thickness uniformity, achieving 0.26% along the translation direction over 1500 mm in dynamic mode. The multilayer deposition system is poised for use in fabricating periodic, lateral-graded and depth-graded multilayers, specifically catering to the beamlines for diverse scientific applications at Diamond Light Source.

Design and simulation analysis of an extrusion structure based on screw extrusion 3D printing

Abstract In response to the problems of 3D printing, such as uneven wire discharge and easy clogging of printing nozzles in FDM (Fused Deposition Modeling) printing technology, this paper develops a screw extrusion 3D printing melting deposition system based on simulation. The simulation results show that the maximum deformation of the screw occurs at the tail end, with a maximum value of 0.04 mm, while the fluid pressure and the pressure on the surface of the screw gradually increase along the direction of extrusion, and the maximum pressure occurs near the nozzle, with a value of 0.13 MPa. The fluid pressure is positively correlated with the screw speed and negatively correlated with the screw pitch. The fitting formula is obtained by numerical simulation of the screw speed and the flow velocity at the nozzle outlet. Using a self-made screw extrusion 3D printing equipment, relevant experiments are conducted to explore the influence of different layer thicknesses and line spacings on the mechanical properties of printed samples, as well as the influence of printing speed on surface quality. It is found that layer thickness has a significant impact on the bending strength of printed samples, with a maximum value of 24.74 MPa and a minimum of 19.21 MPa. The bending strength decreases by 28.79 % from 0.6 mm to 1.0 mm layer thickness. The line spacing has a significant impact on the tensile strength of printed samples, with a maximum value of 27.22 MPa and a minimum of 21.16 MPa. As the printing speed increases, the surface roughness of the printed piece also gradually increases from Ra = 389.28 μm at v = 30 mm/s to Ra = 535.45 μm at v = 70 mm/s, an increase of 37.55 %.