RelyX U200 Research Articles

Medium-term evaluation of the bond strength and dentin penetration of self-adhesive resin cements to root dentin.

Medium-term evaluate the bond strength and tag formation in root dentin using self-adhesive cements Maxcem Elite (MCE), Relyx U200 (RU2), SeT PP (SPP) and Megalink (MGL) compared to conventional cement Relyx ARC (ARC) for glass fibre post cementation. One hundred bovine incisors roots were endodontically treated and divided into 5 groups (n = 20) according to the cementation system: MCE, RU2, SPP, MGL and ARC. All cementation systems were evaluated at 24 h (1) and 12 months (2) after post cementation. Specimens from the cervical, middle and apical thirds of the root were submitted to push-out bond strength test and confocal laser microscopy to verify the dentin penetration. The adhesive failure mode was classified as adhesive, cohesive and mixed. Data were analysed by one-way ANOVA and Tukey tests (α = 5%). ARC-1 and ARC-12 showed the highest bond strength (P < 0.05). ARC showed the greatest tag extension, regardless of the third (P < 0.05). The most frequent failure mode in the 24-h analysis was cohesive, regardless of the cement used. For the 12-month analysis, mixed failure was the most frequent. Conventional cement (ARC) showed the highest bond strength and tag extension, regardless of the evaluation period. In all cementation systems, the bond strength decreased after 12 months. © 2023 Australian Dental Association.

Transdentinal cytotoxicity of resin luting cements using the bovine and human dentin barrier

Based upon ethical questions and because of the difficulty of obtaining intact human teeth, researchers have used bovine teeth to assess the physical and mechanical properties of different dental materials. However, data from transdentinal cytotoxicity tests showing that the bovine dentin barrier is similar to the human dentin barrier is lacking. The purpose of this in vitro study was to evaluate whether the bovine dentin barrier produces similar results to those obtained when the human dentin barrier is used to assess the transdentinal cytotoxicity of resin luting cements. The number and diameter of dentinal tubules present in the human dentin barrier and bovine dentin barrier were evaluated and assessed with a t test (α=.05). After inserting the standardized dentin barriers into artificial pulp chambers, murine dental papilla-derived cells (MDPC-23) were seeded on the pulpal surface of the specimens, and the luting cements were applied to their occlusal surfaces. Then, the following groups were established for both human and bovine dentin barriers: no treatment (negative control); Single Bond Universal; RelyX Luting 2; RelyX U200; and RelyX Ultimate. After 24 hours, the viability (alamarBlue) and morphology (scanning electron microscopy) of the cells were evaluated with a 2-way analysis of variance and the Tukey honest significance test (α=.05). Dentinal tubules with larger diameters were observed in bovine dentin (P<.05), but the number of tubules was similar (P>.05). A reduction in viability and notable changes in the morphology of MDPC-23 cells occurred in the Single Bond Universal and RelyX Luting 2 groups in comparison with the negative control (P<.05). The RelyX U200 and RelyX Ultimate groups were statistically similar to the negative control (P>.05). No difference was found in cytotoxicity when the same luting cement was applied on human or bovine dentin barriers (P>.05). For transdentinal cytotoxicity tests of resin luting cements, the bovine dentin barrier proved similar results to the human dentin barrier.

Fracture resistance of monolithic translucent zirconia crown bonded with different self-adhesive resin cement: influence of MDP-containing zirconia primer after aging

ObjectivesSuccessful ceramic restorations depend on the strong bonding with resin cement and even stress distribution. The aim of this study was to evaluate the impact of adding MDP-containing zirconia primer before self-adhesive resin cements with different functional acidic monomers on fracture resistance of monolithic zirconia crown.Materials and methodsEighty defect-free human maxillary premolars were divided according to the cement type and application of MDP-containing zirconia primer into eight groups (n = 10): Calibra Universal (C), Calibra Universal combined with zirconia primer (CZ), RelyX U200 (R), RelyXU200 combined with zirconia primer (RZ), Panavia SA Cement Plus (P), Panavia SA Cement Plus combined with zirconia primer (PZ), Multilink Speed (M), and Multilink Speed combined with zirconia primer (MZ). After teeth preparation and fabrication of zirconia crowns, each crown was bonded to its corresponding tooth. All specimens were subjected to 10,000 thermocycles between 5 and 55°C, followed by cyclic load (50 N) for 240,000 cycles. Each specimen was subjected to a static axial load until fracture using universal testing machine and the fracture load was recorded. The fracture mode studied and recorded. The fracture load results were analyzed using two-way ANOVA test (α = 0.05).ResultsA significant interaction (P = 0.038) of combining MDP-containing zirconia primer and cement type on fracture resistance of monolithic zirconia crown was detected. The mean fracture load values of zirconia crown were significantly influenced by the combined application of the MDP-containing zirconia primer with Calibra Universal (P = 0.01), RelyX U200 (P < 0.001), and Multilink Speed (P = 0.038), while there was no significant difference with Panavia SA Cement Plus (P = 0.660). There was significant difference (F = 20.69, P < 0.001) between the mean fracture loads of groups with self-adhesive cements (C, R, P, and M groups). The highest fracture load was recorded with RZ group (2446.90 ± 126.72 N) while the lowest fracture load was recorded with C group (1623.18 ± 149.86 N).ConclusionsThe self-adhesive resin cement with different acidic functional monomer affects the fracture resistance of monolithic zirconia crown. Application of MDP-containing primer could improve the fracture resistance of monolithic zirconia crown with most self-adhesive cements. The application of an MDP-containing primer had no impact on the fracture resistance of monolithic translucent zirconia crown bonded by MDP-containing self-adhesive resin cement.

Evaluation of Different Priming Agents with Conventional and Bioactive Self-Adhesive Resin Cements on Shear Bond Strength to Zirconia

The aim of this study was to evaluate the effect of different priming agents on the shear bond strength (SBS) of conventional and bioactive self-adhesive resin cements to zirconia. One hundred and twenty zirconia discs were randomly divided into four main groups according to the priming agents used (n = 30): no priming agent (control), zirconia primer (Z-PRIME Plus), universal adhesive (All-Bond Universal), and universal ceramic primer (Monobond N). Then, each group was subdivided into three subgroups according to the type of self-adhesive resin cement used: TheraCem, Activa BioActive, and RelyX U200 Automix (n = 10). All specimens were subjected to thermocycling. The mean SBS data were analyzed using One-Way ANOVA, followed by multiple comparison Bonferroni test. Without the application of priming agents (control), most of the specimens failed during thermocycling. The priming agent, cement type, and their interaction had a significant effect on the SBS to zirconia (p &lt; 0.001). Only the type of priming agent showed a significant effect on the mode of failure (p &lt; 0.001), resulting in mainly mixed failure with Monobond N and adhesive failure with other primers. Regardless of the type of primer, Bioactive resin cements did not improve the SBS to zirconia compared to conventional cements.

Influence of medium-translucency monolithic zirconia thicknesses and light-curing time on the polymerization of dual-cure resin cements

Aim: To investigate and compare the effects of different thicknesses of medium-translucency monolithic zirconia and light curing times on the polymerization of two types of dual-cured resin cement. Methods: A total of 200 cement specimens were prepared from TheraCem and RelyX U200 cement. The specimens were divided into 5 groups: Group I, without interposing zirconia; Group II, 0.50 mm thickness; Group III, 1.00 mm; Group IV, 1.50 mm; and Group V, 2.00 mm thickness. Each group was subdivided into (1) RelyX U200 and (2) TheraCem. Each subgroup was subdivided according to the light-curing time into (a) 20 s and (b) 40 s (n =5). The polymerization was tested using Fourier-transform infrared (FTIR) spectroscopy and a Vickers microhardness tester. The data were statistically analyzed using ANOVA, an independent sample t-test, and Tukey’s test at a significance level of 0.05. Results: The control group had the highest values of DC and VMH, followed by 0.50, 1.00, and 1.50 mm, respectively, while the 2.00 mm group showed the lowest values. The specimens irradiated for 40 s had greater DC and VMH than those irradiated for 20 s. RelyX U200 revealed higher values for both parameters compared to TheraCem cement. Conclusion: The polymerization of selfadhesive cement depends on the thickness of the monolithic zirconia, the light curing time, and the composition of the cement. The cement should be irradiated for a longer period than recommended to overcome the light attenuation of zirconia. TEGDMA-based self-adhesive cement showed a higher DC and VMH than BISGMA-based cement.

Intraradicular Dentinal Changes Following Fiber Postremoval: Micro-computed Tomography Analysis

Abstract Context: Excessive dentine wear during postremoval can occur due to the adhesion between the cement and the post. Aim: The aim is to evaluate dentine wear and microcrack occurrence following the removal of intraradicular fiberglass posts that were previously cemented with two types of resin cement. Methods: Distal roots (n = 38) of lower molars were instrumented, filled, prepared for intraradicular postinstallation, and divided into two groups according to the cement used for the posts: RelyX ARC or RelyX U200. The posts were removed through abrasion using ultrasonic diamond tips, after which the degrees of dentine wear (volume/mm3) and microcrack formation were assessed using microcomputed tomographic imaging. Statistical Analysis Used: The Mann–Whitney U (P ≤ 0.05) and Chi-squared tests (P ≤ 0.05) were used. Results: After the removal of the posts, no statistically significant difference in root canal volume or microcrack occurrence was observed between the groups (P &gt; 0.05). The procedure produced significant dentine wear regardless of the type of cement used (P &lt; 0.05). Conclusions: The removal of fiberglass posts caused extensive dentine wear but did not influence microcrack occurrence. The type of resin cement used did not affect the dentine loss or microcrack appearance that resulted from fiberglass postremoval.

Analysis of a self-adhesive resin cement using immediate or delayed light curing on adhesive/root dentin interface after fiber post cementation

Aim: To evaluate the performance of new self-adhesive resin cement (Megalink Auto, Odontomega Import) using immediate or delayed light curing on adhesive/root dentin interface after fiber post cementation. Methods: Forty human, canine roots were endodontically treated, and the post space was prepared. Specimens were randomized into four groups based on the cement and light-curing timing used (n = 10): RU-I – RelyX U200 (3M ESPE) resin cement with immediate photoactivation after fiberglass post cementation; MG-I – Megalink Auto (Odontomega Import), resin cement with immediate photoactivation after fiberglass post cementation; RU-5 – RelyX U200 (3M ESPE), resin cement with a 5-min delay light-curing timing; and MG-5 – Megalink Auto (Odontomega Import), resin cement with a 5-min delay light-curing timing. Specimens were cross-sectioned (one slice for each third: cervical, middle, and apical) and subjected to push-out and confocal laser microscopy tests. In addition, the fracture mode was analyzed using a stereomicroscope. Kruskal–Wallis tests followed by Dunn's post-test were used to analyze the data (α = 0.05). Results: There was no statistical difference in the bond strength between the groups (p &lt;0.05), regardless of the third analysis. The most insidious failure pattern was adhesive (type 2). There was a statistical difference in the penetrability of the cementation system between the RU-I and MG-5 groups in the cervical and middle thirds (p &lt;0.05). Conclusions: There was no influence of the light-curing time point on bond strength between the dentin and the cementation system, with greater penetrability with immediate light-curing of the self-adhesive resin cement.

Effect of degree of conversion on the surface properties of polymerized resin cements used for luting glass fiber posts

Statement of problemLack of conversion of resin cements for luting glass fiber posts in deeper levels of the root canal may compromise clinical performance. PurposeThe purpose of this in vitro study was to evaluate the effect of the degree of conversion on the surface properties of dual-polymerized resin cements used for cemented glass fiber posts according to the root level. Material and methodsFifty maxillary central incisor teeth were endodontically treated, and glass fiber posts were cemented using the following systems: self-adhesive dual-polymerized resin luting cement (RelyX U200) and dual-polymerizing flowable core and a post luting system (Rebilda DC) with a self-etching adhesive (Futurabond DC). The degree of conversion was determined via attenuated total reflectance and Fourier transform infrared spectroscopy, and surface microhardness and cement film thickness were measured. The intraradicular fit was evaluated with microscopy. All tests were performed in the coronal, middle, and apical third of the root canal. Statistical analysis was done with ANOVA and the multiple comparison Tukey test (α=.05). ResultsThe degree of conversion was higher in the coronal third using Rebilda DC (65.3 ±4.8%) than RelyX U200 (38.7 ±5.3%) (P<.05); on both resin cements, these values decreased from the coronal to the apical third (30.9 ±3.7%, 61.9 ±8.7%, respectively). The cement film thickness was higher for RelyX U200 in the 3 thirds than for Rebilda DC; significant differences (P<.05) were recorded in both cementing systems in the coronal and apical thirds. In the middle third, no significant differences were observed (P>.05). The mean surface microhardness values increased in the coronal thirds and decreased with increasing root canal depth. The marginal seal in the coronal thirds and the intraradicular fit in the middle thirds showed closer adaptation; however, some tags were observed in the interface resin cement and radicular dentin. Gap and tag formations were observed in the apical third. ConclusionsDepending on the root canal third, the surface properties of dual-polymerized resin cements are influenced by the degree of conversion.

Analysis of the adhesive interface of dentine treated with carbodiimide and chitosan before cementation of fiberglass posts with different resin cements.

The objective of this study is to evaluate the effect of 1-ethyl-3-(3-dimethylaminopropyl)-carbodiimide (EDC) and chitosan (CHI) on the adhesive interface of resin cements to root dentine. Forty-five upper canines were sectioned, endodontically treated, prepared and divided into three groups according to dentine treatment (distilled water-DW, CHI 0.2% and EDC 0.5) and in three subgroups according to resin cement: RelyX ARC, Panavia F 2.0 or RelyX U200. Slices were obtained, with five slices of each third submitted to the analysis of the adaptation of the adhesive interface through scores and the perimeter with gaps in confocal laser scanning microscopy and one slice of each third later evaluated qualitatively in scanning electron microscopy. The results were analyzed using with Kruskal-Wallis and Spearman correlation tests. There was no difference in adaptation for the different resin cements (p = .438). EDC presented better adaptation when compared to the groups treated with DW and CHI (p < .001), while the CHI and DW presented similar adaptation values (p = .365). No difference was observed in the perimeter referring to the gap areas for the different resin cements (p = .510). EDC showed a lower percentage of perimeters with gaps when compared to CHI (p < .001), with the percentage of perimeter with gaps of teeth treated with CHI being lower than DW (p < .001). A positive correlation coefficient equal to 0.763 was obtained between the perimeter with gaps and the adaptation data of the adhesive interface (p < .001). EDC resulted in better adaptation of the adhesive interface and a lower percentage of perimeters with gaps compared to chitosan.

Electric Current as an Alternative Method for Surface Treatment of Acid-Sensitive Ceramics

Objectives: The aim of this study was to evaluate the silane application with electric current as an alternative method for surface treatment of acid-sensitive ceramic. Materials and Methods: IPS E.max Press ceramic discs applied with silane, associated or not with hydrofluoric acid, electric current and storage time in water were divided in the groups (n=10) AE+CF (Acid etching + electric current free); AE+CA (Acid etching + electric current); AF+CF (Acid etching free + electric current free); AF+CA (Acid free + electric current); AE+CF +T (Acid etching + electric current free + thermal cycling); AE+CA+T (Acid etching + electric current + thermal cycling); AF+CF+T (Acid free + electric current free + thermal cycling) and AF+CA-T (Acid etching free + electric current + thermal cycling. In the conditioned groups, 10% hydrofluoric acid was applied for 20s. The silane was applied with microbrush in the AE+CF-T, AE+CA-T, AF+CF-T and AE+CA-T groups and in the other groups it was replaced by a metal tip conductor of electric current. Cylindrical silicone matrices with three holes (12 mm in diameter and 1mm thick) were placed on the ceramic. The resin cement RelyX U200 was inserted into the holes of the matrix, subjected to a static load of 250mg for 2min and photoactivated for 20s. After removing the matrix, the sample with resin cement cylinder adhered to the ceramic was stored in an oven at 37 ºC for 24h. The 24-h samples and those thermocycled with 10,000 cycles in vats with water at temperatures of 5±1 ºC and 55±1 ºC were submitted to microshear resistance test, fracture analysis, SEM analysis and contact angle. Data were submitted to one-way ANOVA and Tukey’s test (α=0.05). Results: At 24h, AE+CA showed the highest value in bond resistance and AF+CF at the lowest, both different from AE+CF while AF+CA was intermediate. After thermocycling, with higher values AE+CA+T and AE+CF-T were similar, as well as AF+CF+T and AF+CA+T with lower values. AE+CF+T and AE+CA+T differed statistically from AF+CF+T and AF+CA+T. Adhesive failure was predominant in all groups with or without thermocycling. At 24h, there was cohesive failures in mixed resin cement in the AE+CA and AF+CF. After thermocycling, there were mixed failures in the AE+CA+T and cohesive failures in resin cement for the AE+CF+T and AF+CA+T. The greater contact angle vas observed in the AE+CF. Conclusions: The association of hydrofluoric acid etching, application of silane with electric current and storage times promoted different values of bond strength, types of failures and contact angles in samples of resin cement bonded to acid-sensitive ceramics. Clinical Relevance: The application of silane with an electric current is a promising method to improve the adhesive bond between resin cement and ceramics, especially when associated with hydrofluoric acid etching.

Effect of calcium hypochlorite as an irrigant alternative in the removal of methylene blue after photodynamic therapy under the post-space adhesive interface

We evaluated the effect of irrigation protocols in removing methylene blue after photodynamic therapy (PDT) in post-space dentin. Bond strength to dentin and failure mode after fiber post cementation was also evaluated. Ninety bovine teeth were endodontically treated. Post-space preparation and PDT mediated by 0.01% methylene blue and diode laser (660 nm) were performed. Three irrigations protocols were tested (n = 10): distilled water (DW), 2.5% sodium hypochlorite (SH), and 6% calcium hypochlorite (CH). Other specimens were used to investigate the bond strength to post-space dentin according to the irrigation protocol and the post cementation system used (RelyX U200 cement (RU) and GC Gold Label 1 glass ionomer cement (GC) in six groups (n = 10): DW-RU, SH-RU, CH-RU, DW-GC, SH-GC e CH-GC. Regardless of the post-space third, DW showed a lower incidence of residues than SH (p < 0.05), but similar to CH. SH showed similar results to CH (p > 0.05). Regarding the bond strength, CH-RU and CH-GC showed higher values compared to the other groups (p< 0.05), but similar to each other. No differences were observed between the other groups (p > 0.05). Cohesive was the most predominant failure. 6% CH to remove methylene blue after PDT favors the bond strength of RelyX U200 and GC Gold Label.

Can Carbodiimide (EDC) and Chitosan Cross-linking Agents Effect the Longevity of Fiberglass Posts Luted with Different Types of Composite Cements to Root Dentin?

To evaluate the effect of carbodiimide (EDC) and chitosan (CHI) on the enzymatic activity (EA) and bond strength (BS) of different composite cements to root dentin. Ninety (90) maxillary canines were sectioned, standardizing the length of the roots. The roots were endodontically treated, prepared, divided into 3 groups according to dentin treatment (distilled water [DW], CHI 0.2 wt%, or EDC 0.5M), and further subdivided into 3 subgroups according to composite cement (RelyX ARC [3M Oral Care], Panavia F 2.0 [Kuraray Noritaki], or RelyX U200 [3M Oral Care]). Of the slices obtained by sectioning, the most cervical of each third were subjected to a push-out test and the most apical were subjected to in-situ zymography. Half of the slices were analyzed immediately, and the other half after 6 months. The results were analyzed with ANOVA or the chi-squared test. RelyX ARC showed higher BS associated with CHI, while RelyX U200 showed higher BS associated with EDC (p = 0.044). For Panavia F 2.0, the treatment did not influence BS (p > 0.05). For the cervical and middle thirds, no differences were observed between the cements, while the apical third revealed higher BS for RelyX U200 (p < 0.001). The highest percentage of adhesive-to-dentin failures was observed for Panavia F 2.0. EDC showed the lowest percentage of adhesive-to-dentin failures. According to zymographic analysis, DW and CHI showed greater fluorescence for RelyX ARC, while EDC exhibited the lowest fluorescence of all cements (p > 0.05). The different mechanisms of action of solutions for pre-treatment of intraradicular dentin yielded different results depending on the adhesive used. EDC resulted in higher bond strength and higher enzyme inhibition for RelyX U200, while the treatment with chitosan resulted in higher bond strength and lower enzymatic activity for RelyX ARC. Although EDC and chitosan treatments did not influence the bond strength for Panavia F 2.0, both resulted in higher enzyme inhibition for this composite cement.

Effect of aging and cementation systems on the bond strength to root dentin after fiber post cementation.

This study evaluated the effect of aging and cementation of fiber posts using glass ionomer and resin cements on push-out bond strength, failure mode, and resin tag formation. One hundred and twenty bovine incisors were used. After post-space preparation, the specimens were randomly allocated into 12 groups (n = 10) according to the cementation system used: GC - GC Gold Label Luting & Lining); RL - RelyX Luting 2; MC - MaxCem Elite; RU - RelyX U200 and the aging periods (24 hours, 6 months, and 12 months). Slices from the cervical, middle, and apical thirds were obtained and analyzed by push-out bond strength test and confocal laser scanning microscopy. One-way ANOVA and Tukey's post-hoc test was used at a significance level of 5%. For the push-out bond strength test, no differences among GC, RU, and MC in the cervical and middle thirds were observed, regardless of the period of storage (P > 0.05). In the apical third, GC and RU showed similar bond strength but higher than other groups (P > 0.05). After 12 months, GC showed the highest bond strength (P < 0.05). Bond strength to post-space dentin decreased over time, regardless of the cementation system used. Cohesive failure was the most frequent, regardless of the period of storage, cementation system, and post-space third. Tag formation was similar among all groups. After 12 months, GC showed the highest bond strength values.

Fracture resistance of CAD/CAM blocks cemented on dentin using different cementation strategies.

To determine whether the fracture resistance of computer-aided design/computer-aided manufacturing (CAD/CAM) resin-based composites and polymer-infiltrated ceramic network materials cemented on dentin is influenced by the restoration thickness and composite cement application strategy. Disc-shaped specimens (Ø = 7 mm) of 0.8 mm and 1.5 mm thicknesses were milled from two CAD/CAM materials: resin-based composite (RBC, Cerasmart 270) and polymer-infiltrated ceramic network (PICN, Vita Enamic). The discs (n = 8 per group) were cemented on flattened dentin using three different cementation strategies: 1) self-adhesive composite cement (RelyX U200) in light-curing mode (LC-SAC), 2) universal adhesive (Single Bond Universal) with composite cement (RelyX Ultimate) in auto-curing mode (AC cement), and 3) adhesive and composite cement as in 2) but in light-curing mode (LC cement). The restorative surface was indented perpendicularly with a compressive load using a universal testing machine until fracture. The fracture resistance (N) of RBC and PICN was separately analyzed using two-way ANOVA and Tukey's post-hoc test (α = 0.05). The fracture resistance of each material was significantly influenced by the material thickness and cementation strategy (P < 0.05). Irrespective of the material type and cementation strategy, thicker materials exhibit higher fracture resistance. For RBC, the fracture resistance of the LC cement group was significantly higher than that of AC cement only at 0.8 mm thickness. For PICN, the LC-cement cementation strategy produced superior fracture resistance, regardless of the restoration thickness. The fracture resistance of Cerasmart 270 was higher for the thicker material; the fracture resistance of LC cement was higher than that of AC cement at 0.8 mm thickness cemented to dentin. In comparison, LC cement showed the highest fracture resistance for Vita Enamic for both material thicknesses.

Influence of different adhesion strategies on glass fiber post retention.

Failures in glass fiber post (GFP) retention may be associated with low adhesion achieved in root dentin. 55 single-rooted premolars were endodontically treated and distributed according to different adhesion strategies (n=11): G1: RelyX ARC (3M ESPE; etch-rinse strategy); G2: Relyx Ultimate (3M ESPE; etch-rinse strategy); G3: AllCem (FGM; etch-rinse strategy); G4: Relyx Ultimate (3M ESPE; self-etching strategy); G5: RelyX U200 (3M ESPE; self-adhesive strategy). For Bonding Strength (BS) analysis, the roots were sectioned in slices (1.0mm thickness) corresponding to each root third and submitted to push-out test. The type of failure was assessed by scanning electron microscopy (SEM). The highest BS averages were found in G2 and G3. However, in the middle and apical root thirds, G3 showed statistically similar results to G4 and G5. In the cervical and middle third, G1 was statistically similar to G4 and G5. The mixed type of failure was the most common in all groups. Self-etching (G4) and self-adhesive resin (G5) cements, showed similar BS results of immediate bonding in the cementation of GFP compared to conventional resin cements (G1, G2, G3). Key words:Dental Cements, Dentin-Bonding Agents, Post and Core Technique, Dental Bonding.

Microleakage in indirect onlay restorations cemented with three different types of adhesives: An in vitro study.

To evaluate the in vitro degree of marginal microleakage in indirect Class II onlay restorations cemented with dual self-adhesive, universal adhesive and dual adhesive. In the present in vitro experimental study, a total of 54 human premolar teeth were prepared and divided into three equal groups (n = 18) for placement of onlay-type restorations cemented with A: Allcem™ dual-cure adhesive cement), B: RelyX™U200 dual-cure self-adhesive cement and C: RelyX™ Ultimate universal adhesive cement. All restorations were subjected to 10,000 thermocycles between 5°C and 55°C and immersed in a 1M silver nitrate solution for 6 hours. The crowns were then sectioned mesiodistally and observed under a stereo microscope to determine the degree of marginal microleakage in the cervical area. The onlay restorations cemented with RelyX Ultimate did not present microleakage in the majority of cases (77.8%). Restorations cemented with RelyX U200 showed predominantly microleakage up to the pulp floor in 83.3% of the total, being this significantly higher microleakage than in restorations cemented with RelyX Ultimate and Allcem Dual (p<0.001 and p<0.001 respectively). There was no significant difference in microleakage between the last two mentioned cements (p=0.255). Allcem dual adhesive cement and RelyX Ultimate universal adhesive showed significantly less microleakage than RelyX U200 dual-curing self-adhesive cement at the cervical level, with predominantly no microleakage and microleakage down to the enamel, respectively. The use of RelyX Ultimate cement in indirect restorations is recommended as it showed better marginal adaptation. Key words:Microleakage, human teeth, adhesion, adhesive cement, thermal cycling, onlay restoration.

Effect of different surface treatments on resin-matrix CAD/CAM ceramics bonding to dentin: in vitro study

BackgroundEvaluating the effect of different surface treatment methods on the micro-tensile bond strength (µTBS) of two different resin-matrix computer-aided design/computer-aided manufacturing (CAD/CAM) ceramics (RMCs).MethodsA standardized inlay preparations were performed on 100 intact maxillary premolars. According to the type of the restorative material, the teeth were randomly divided into two equally sized groups (n = 50): (polymer-infiltrated ceramic (Vita Enamic) and resin-based composites (Lava Ultimate)). The inlays were fabricated using CAD/CAM technology. In each group, the specimens were randomly assigned to five subgroups (n = 10) according to the surface treatment method: group 1 used was the control group (no surface treatment); group 2, was treated with air abrasion with 50 μm Al2O3 (A) and universal adhesive (UA); group 3, was treated with air abrasion with 50 μm Al2O3 (A) and silane coupling agent (S); group 4, was treated with hydrofluoric acid (HF) and universal adhesive (UA) and group 5, was treated with Hydrofluoric acid (HF) + silane coupling agent (S). The inlays were then cemented to their respective preparations using dual-cure self-adhesive resin cement (RelyX U200, 3 M ESPE) according to the manufacturer’s instructions. The µTBS test was conducted in all groups, and stereomicroscope and scanning electron microscope were used to inspect the failure mode. The data were statistically analyzed using a two-way analysis of variance (ANOVA) and Tukey’s post-hoc multiple comparison tests at a significance level of p < 0.05.ResultsSurface treatments significantly increased the µTBS of the materials compared to the control group (p < 0.05). For CAD/CAM RBCs, the µTBS value highest in group 2 whereas, for PICN, the µTBS value was highest in group 3. Cohesive failure of CAD/CAM restorative material was the most predominant mode of failure in all treated groups, whereas adhesive failure at restoration-cement interface was the most predominant failure mode in the control group.ConclusionSurface treatments increase the µTBS of resin-matrix CAD/CAM ceramics to tooth structure. Air abrasion followed by universal adhesive and hydrofluoric acid followed by silane application appears to be the best strategies for optimizing the bond strength of CAD/CAM RBCs and PICN respectively.

EXPERIMENTAL INVESTIGATION AND COMPARATIVE EVALUATION OF PUSH-OUT BOND STRENGTH FIBER POST CEMENTED WITH DIFFERENT ADHESIVE RESIN CEMENTS: AN IN-VITRO STUDY

This article present an experimental investigation of push-out bond strength of fiber post that are cemented with various adhesive resin cements. Various modes of failure are also studied and discussed herein. Three resins namely Fluorocore 2+, Rely-X U200 and G-Cem are used in this study. The study is carried out on forth five single rooted teeth randomly divided into three groups. The teeth specimens were prepared by chemo-mechanical procedure and cemented with various adhesive resin cement. These teeth are further sliced at coronal, middle and apical levels for experimental testing of bond strength. These samples further tested on universal spring testing machine until the post was dislodged. Using Chi square, Mann Whitney U and Kruskal Wallis test, the obtained results were analyzed with significance level of p = 0.05. Bond strength of Fluorocore 2+ showed highest as compared to others. Rely-X U200 and G-Cem showed insignificant variation in bond strength at coronal, middle and apical levels.

Digital image analysis of fluorescence of ceramic veneers with different ceramic materials and resin cements.

The objective of this study was to analyze the effect of the type of ceramics and resin cements on the fluorescence of ceramic veneers under the 405 nm UV-light by digital imaging. One hundred and ninety-two veneers were fabricated using three types of ceramics (IPS e.max CAD, IPS Empress CAD, and Zenostar). Eight pieces of substrates were made of resin-nano-ceramic (Lava Ultimate). The level of fluorescence for each sample cemented with the substrate using three kinds of resin cements (RelyX U200, Variolink N, and Choice 2) was analyzed by using histogram data of luminosity from Adobe Photoshop software. Furthermore, the fluorescence values were evaluated by two-way ANOVA and Tukey's test. The highest fluorescence values were observed for the IPS e.max CAD cemented with Choice 2 cement, followed by IPS Empress CAD, and Zenostar the lowest. The final fluorescence intensity of ceramic veneer is affected by ceramic materials and resin cements.

Marginal discrepancy and fracture load of thermomechanically fatigued crowns fabricated with different CAD-CAM techniques.

To assess the effect of CAD-CAM technique (monolithic, CAD-on, or CAD-on cemented) and thermomechanical fatigue on the marginal discrepancy and fracture load of ceramic crowns. A total of 90 brass master dies were fabricated to investigate marginal adaptation and fracture load. A mandibular first molar crown's median measurements were loaded into CAD software and divided into 2 crown design groups: Monolithic (M)(IPS e.max zirCAD)(n= 30) or CAD-on core (IPS e.max zirCAD) and lithium disilicate veneer (IPS e.max CAD) (n= 60). The crowns and cores were milled, seated on their respective dies, and marginal discrepancy values were measured by using microcomputed tomography. After veneers were milled, the cores in the veneer groups were divided into 2 groups; veneers bonded with fusion glass-ceramic (IPS e.max CAD Crystal) in CAD-on group (CO) and CAD-on cemented group (CO-C) where veneers were cemented (RelyX U200) onto cores (CO-C). The marginal discrepancy measurements were remade and the crowns were subjected to thermomechanical fatigue (TMF) by using a chewing simulator and thermocycling (5-55°C, 1,200,000 cycles). Marginal discrepancy measurements were repeated and the crowns were subjected to fracture load test by using a universal test device. Data were analyzed statistically by analysis of variance (ANOVA) and Tukey's honestly significant difference test (α= 0.05). All crown groups had similar marginal discrepancy before veneering. Veneering and cementation on die increased the marginal discrepancy of crowns in cemented CAD-on group. Thermomechanical fatigue increased the marginal discrepancy of both CAD-on groups. Monolithic crown group had the lowest marginal discrepancy after thermomechanical fatigue (p < 0.001), and the highest fracture load (p < 0.001) CONCLUSIONS: Fabrication technique affected the marginal fit and fracture load of CAD-CAM crowns after thermomechanical fatigue. All crowns survived the thermomechanical fatigue test without dislodgement or fracture. Monolithic crowns had the best fit and highest fracture load after fatigue testing. The CAD-on systems had similar marginal discrepancies, and static loading reproduced veneer chipping.