The semiconductor industry has exploited productivity improvements through aggressive feature size reduction for over four decades. While enormous effort has been expended in developing the optical lithography tools to print ever finer features, significant advances have also been required to measure the printed features. In this article we will discuss the current state of the art in the metrology for measuring critical dimensions of printed features for scanning electron microscopy and atomic force microscopy, and describe work at the National Institute of Standards and Technology advancing these tools as well as exploratory work on two new promising techniques, scatterfield microscopy and small angle X-ray scattering. Line width roughness critical dimension and overlay metrology and control are two of the most significant industry needs mentioned in the International Technology Roadmap for Semiconductors (2005). To cite this article: S. Knight et al., C. R. Physique 7 (2006).