High Displacement Research Articles

Impact Assessment of Hydrate Cuttings Migration and Decomposition on Annular Temperature and Pressure in Deep Water Gas Hydrate Formation Riserless Drilling

The accurate prediction of wellbore temperature and pressure is important for safe drilling. However, annulus temperature and pressure changes are more complicated due to phase transition. To study this problem, a prediction model of temperature and pressure in deep water riserless drilling is established by considering hydrate cuttings decomposition, interphase mass transfer, and phase transition heat. Based on this model, the effects of hydrate cuttings decomposition on the temperature and pressure of drilling in a hydrate reservoir are explored. The results show that the influence of hydrate cuttings decomposition increases significantly with an increase in the inlet temperature. The influence of hydrate cuttings decomposition on temperature and pressure decreases with an increase in displacement. A small range in the variation of density and penetration rates has little impact on the annulus pressure but mainly affects the temperature. The influence of hydrate cuttings decomposition increases with an increase in the penetration rate. In normal drilling conditions, hydrate cuttings decomposition has little impact on annulus temperature and pressure, but under the conditions of a high inlet temperature, high hydrate saturation, low displacement, and high penetration rate, it is necessary to consider the impact of hydrate cuttings decomposition. This study can provide reference for the prediction of temperature and pressure in deep water hydrate reservoir riserless drilling.

In-situ TEM bubble to cavity evolution due to annealing post helium and dual ion irradiation in Cu-10Ta and Cu-3Ta

Materials have been essential to every major invention in the history of mankind, e.g. satellites, nuclear reactors, or space shuttles would not exist without advancements in materials withstanding temperature and radiation environments. In this work, we investigate room-temperature implantations of helium and concurrent He and Au via in-situ transmission electron microscopy (TEM) followed by isochronal annealing up to 450 °C to understand the microstructural stability and bubble to cavity evolution in advanced nanocrystalline (NC) Cu-3 at.%Ta and Cu-10 at.%Ta alloys. The room temperature irradiation to high helium concentration and displacements per atom (dpa) levels did not lead to significant coarsening of grains in both Cu10Ta and Cu3Ta. Overall grain sizes remained <150 nm indicating extraordinary microstructural stability in both alloys. Post-irradiation, incubation for a few days resulted in the observation of ~1 nm diameter bubbles homogenously distributed in both the alloys and both irradiation conditions. Further evolution of these bubbles to cavities with annealing to 450 °C indicated Brownian motion migration and coalescence to be the dominant coarsening mechanism involved. A comparison of bubble to cavities evolution in Cu3Ta and Cu10Ta under similar conditions showed smaller bubble size and density in Cu3Ta indicating an overall enhanced resistance of Cu3Ta to swelling under both helium and dual-beam irradiation at high temperatures. This is primarily attributed to the high fraction of essential coherent/incoherent precipitates that act as effective defect sinks in Cu3Ta.

Emergence of correlations in twisted monolayer–trilayer graphene heterostructures

Twisted bilayer graphene heterostructures have recently emerged as a well-established platform for studying strongly correlated phases, such as correlated insulating, superconducting, and topological states. Extending this notion to twisted multilayer graphene heterostructures has exhibited more diverse correlated phases, as some fundamental properties related to symmetry and band structures are correspondingly modified. Here, we report the observations of correlated states in twisted monolayer–trilayer (Bernal stacked) graphene heterostructures. Correlated phases at integer fillings of the moiré unit cell are revealed at a high displacement field and stabilized with a moderate magnetic field on the electron-doping side at a twist angle of 1.45°, where the lift of degeneracy at the integer fillings is observed in the Landau fan diagram. Our results demonstrate the effectiveness of moiré engineering in an extended structure and provide insights into electric-field tunable correlated phases.

Effect of water saturation on CO2 minimum miscibility pressure and oil displacement performance

The CO2 miscible flooding is an effective technology for development of low permeability reservoirs due to high oil displacement efficiency. However, CO2 miscible flooding for tertiary recovery technology typically occur after water flooding. Water hindered the contact and mass transfer of CO2 and oil, produce water resistance effect. Water can block CO2 and contact and mass transfer of crude oil (ie water blocking effect). The impact of this effect on the miscibility pressure and oil displacement effect is still unclear. In this study, homogeneous artificial cores with the same permeability as the reservoir were designed according to the miscible mechanism. Subsequently, the minimum miscibility pressure(MMP) between CO2 and crude oil at different water saturation was measured by the coreflood test. Based on the MMP, CO2 miscible flooding experiments were conducted by natural cores at different water saturation. The results showed that when the water saturation was 30%, 45%, and 60%, respectively, the corresponding MMP between CO2 and crude oil was 18.56, 19.48, and 21.76 MPa. The higher the water saturation, the longer the gas breakthrough time. But the oil recovery factor did not rise with the increase of water saturation. When the water saturation was 45%, the oil recovery factor in the miscible flooding experiment was the highest. In addition, the higher the water saturation, the weaker the CO2 extraction of various components in the crude oil. And the light components below C5 were most affected by water saturation. The mechanisms underlying these results are discussed. This study contributes to the development of CO2 miscible flooding reservoir plan.

Influences of processing conditions on gradient structures in injection‐molded polyethylene caps and their property correlations

AbstractIn this study, the influences of processing conditions, that is, injection speed and holding pressure, on the gradient crystal structural formation in the injection‐molded cap specimens were investigated. Skin‐, shear‐ and core‐layers across the specimen thickness were investigated in detail by using small‐angle x‐ray scattering, wide‐angle x‐ray diffraction, and atomic force microscopy techniques. The results showed that high holding pressure caused high density and large weight of the cap specimens. This strongly contributed to high displacement resistant on applied pressure (doming resistant), while the lamellar thickness (Lc) of the skin layer also played a role. On the contrary, low holding pressure promoted the formation of the random‐oriented lamellae in the core layer, which contributed to high environmental cracking resistance (ESCR). Moreover, the lower injection speed caused the thicker Lc of the skin layer, and this improved the ESCR of the specimen. The results allowed us to propose its failure mechanism.

O-006 Novel and scalable non-invasive metabolic imaging of early embryos using a lab-on-a-chip approach

Abstract Study question Is it feasible to safely determine metabolic imaging signatures to measure nicotinamide adenine dinucleotide (NADH) associated auto-fluorescence in early embryos using a scalable lab-on-a-chip approach? Summary answer We developed an optofluidic device capable of non-invasively obtain high-resolution 3D images of the metabolic activity of live mouse embryos using a lab-on-a-chip approach. What is known already Selecting the most suitable embryos for implantation and subsequent healthy live birth is crucial to the success rate of assisted reproduction and offspring health. Thus, developing non-invasive methods that are reliable to assess oocyte and embryo quality has been a significant aim for assisted reproduction. Besides morphological evaluation using optical microscopy, a promising alternative is the non-invasive imaging of live embryos to establish metabolic activity performance. However, metabolic imaging has been only achieved using highly complex advanced microscopy such as Fluorescence-lifetime imaging (FLIM) and hyperspectral microscopy, methods that are costly and challenging, limiting the potential for deployment in fertility clinics. Study design, size, duration The non-invasive nature of the system was investigated by assessing the development and viability of live embryos after embryo culture for 67hrs post metabolic imaging at the 2-cell embryo stage (n = 115), including a control for culture conditions and sham controls (system no-illuminated). Embryo quality of developed blastocysts was assessed by immunocytochemistry to quantify trophectoderm and inner mass cells (n = 75). Furthermore, inhibition of metabolic activity (FK866 inhibitor) during embryo culture was also assessed (n = 18). Participants/materials, setting, methods Optofluidic devices were manufactured by cast-moulding using a negative photoresist (SU8-2075; MicroChemicals GmbH, Ulm, Germany) by a standard UV-photolithography process. The microstructures fabricated of polydimethylsiloxane (PDSM) integrated Light Sheet Fluorescence Microscopy into a microfluidic system, including on-chip micro-lenses to generate a light sheet at the center of a microchannel. Super-ovulated F1 (CBA/C57Bl6) mice were used to produce 2-cell embryos and embryo culture experiments. Blastocyst formation rates and embryo quality (immunocytochemistry) were compared between study groups. Main results and the role of chance The optofluidic device was capable of non-invasively obtaining high-resolution 3D images of the metabolic activity in live mouse embryos. The system’s design allowed continuous tracking of the embryo location, including high control displacement through the light-sheet, fast imaging of the embryos (&amp;lt;2 second) and keeping a low dose of light exposure (16 J cm-2 and 8 J cm-2). Optimum settings for keeping sample viability showed that a modest light dosage was capable to obtain 30 times higher signal-noise-ratio images than images obtained with a confocal system (p &amp;lt; 0.00001; t-test). The results showed no significant differences between the control, illuminated and non-illuminated embryos (sham control) for embryo development as well as embryo quality at the blastocyst stage (p &amp;gt; 0.05; Yate’s chi squared test). Additionally, embryos with inhibited metabolic activity showed decreased blastocyst formation rates as well as 47% reduction in metabolic activity measured by non-invasive metabolic imaging (p &amp;lt; 0.0001; t-test). This study reports an optofluidic device capable of non-invasive metabolic imaging of live embryos using a similar concept as previously reported using FLIM technology and hyperspectral microscopy, but allowing a novel, scalable and affordable system with implementation potential in standard IVF laboratory equipment. Limitations, reasons for caution The study was conducted using a mouse model focused on early embryo development. Further safety studies are required to assess embryonic health by investigating the impact of the use of light during embryo development, live birth, embryo gene expression and epigenome stability. Wider implications of the findings This lab-on-a-chip is novel, scalable and has the potential to be used in fertility clinics as a technology platform to enable real-time monitoring of the metabolic function of embryos prior embryo transfer. Future applications include potential integration into existing IVF laboratory equipment such as bench and time-lapse incubators. Trial registration number N/A

Long-Term Changes, Synoptic Behaviors, and Future Projections of Large-Scale Anomalous Precipitation Events in China Detected by a Deep Learning Autoencoder

Abstract The frequency of large-scale anomalous precipitation events over China has increased during 1961–2018. However, it remains challenging to understand the mechanisms associated with these anomalous events showing different spatial patterns. Here, we applied an autoencoder technique to identify large-scale anomalous precipitation events for both observations and model simulations, which were then classified into several patterns through a self-organizing map method. The synoptic behavior and atmospheric circulation background of different anomalous patterns were also analyzed using simultaneous composite analyses. Results show that occurrences of different anomalous precipitation patterns have increased significantly, except those centered in North China, Northeast China, and the Yangtze River basin. The anomalous precipitation patterns manifest various intraseasonal distributions, which are linked to zonal oscillations of the western North Pacific subtropical high (WNPSH) and meridional displacements of East Asia westerly jet (EAJ). Accompanied by the westward movement of WNPSH, anticyclonic systems transport warm moist air from the Indian Ocean and the South China Sea to converge with the cold air caused by anomalous cyclones over the northwest flank of the WNPSH, leading to large-scale anomalous precipitation in these regions. Besides WNPSH, the northward and southward displacements of EAJ also favor the occurrence of anomalous precipitation events in northern and southern China, respectively. Our study also illustrates that the occurrence frequency of anomalous precipitation events is projected to increase remarkably under the Shared Socioeconomic Pathway 5–8.5 (SSP585) scenario by rates of twofold to fourfold.

Pain relief after major ankle and hindfoot surgery with repetitive peripheral nerve blocks: A feasibility study.

Major ankle and hindfoot surgery (e.g., ankle, triple and subtalar arthrodesis) typically causes severe postoperative pain, especially the first two postoperative days. Current modalities of postoperative analgesic treatment often include continuous peripheral nerve blocks of the saphenous and sciatic nerves via catheters in order to extend the duration of pain- and opioid-free nerve blockade to 48 h. Unfortunately, the 48 h-efficacy of continuous infusion via a catheter is reduced by a high displacement rate. We hypothesised that one-time repetition of the single injection peripheral nerve blocks would provide effective analgesia with a low opioid consumption the first 48 postoperative hours. Eleven subjects preoperatively received a popliteal sciatic and a saphenous single injection nerve block with a protracted local anaesthetic mixture. Surgery was performed under general anaesthesia. The one-time repetition of the single injection nerve block was carried out approximately 24 h after the primary nerve block. The main outcomes were pain and cumulative opioid consumption during the first 48 postoperative hours. Nine of the 11 (82%) patients had effective analgesia without opioids during the first 48 postoperative hours. Two patients each required a single dose of 7.5 mg of oral morphine equivalents after 43 h. One-time repetition of single injection saphenous and sciatic nerve blocks consistently provided effective analgesia practically without opioids for 48 h after major elective ankle and hindfoot surgery.

New insights of further enhanced tight oil recovery after hydraulic fracturing by VES fracturing fluid

In the process of fracturing in tight reservoirs, viscoelastic surfactant (VES) fracturing fluid has many advantages that can significantly increase the recovery of tight oil. However, there is a risk of formation blockage due to heavy emulsification in the formation. In this study, a VES microemulsion (VES-M) system with low reservoir damage and high oil displacement efficiency is constructed using VES fracturing fluid and polyhydroxy alcohol. The average particle size in the fluid is only 3%–10% of the average pore size of the tight reservoir, and the formation damage is 16.00%. The new fluid can achieve ultra-low interfacial tension (IFT) with Winsor type III microemulsion. Compared with slickwater fracturing fluid and formation water, the new fluid can filtrate deeper into the matrix and increase the oil recovery by 7.20%–11.32% during the flowback process. This study provides a possibility for the field application of VES fracturing fluid in tight reservoirs and new insights into the effects and rules of employing the VES-M system to enhance tight oil recovery.

Interpretation of Petrophysical Properties in Reservoir Rock Using Capillary Pressure Data of the Mishrif Formation in West Qurna Oilfield, Southern Iraq

In this study, capillary pressure tests for twenty-nine samples acquired from four wells, (Rn-83, WQ-155, WQ286, and WQ-355) were used to estimate pore size distribution, pore-throat sorting, displacement pressure, reservoir grade, oil column, effective porosity, and relative permeability of the Mishrif Formation at West Qurna Oilfield, southern Iraq. Interpretation of capillary pressure data revealed that the formation can be divided into four reservoir facies with different reservoir production performances: very good, good, medium, and poor. The facies with very good performance is characterized by large pore sizes, excellent reservoir grade, low displacement pressure, and high oil saturations. The good facies is characterized by the presence of good pore throat sorting, good reservoir grade, and good porosity. Contrary, Medium-performance reservoir facies are characterized by the presence of medium pore sizes, medium pore throat sorting, and medium reservoir grade. Poorly performing reservoir facies is characterized by small pore size, high displacement pressure, poor throat sorting, and high water saturation levels. Based on the relative permeability calculations some samples are wet with water (water-wet), while others are wet with oil (oil-wet).

Wetting transition and fluid trapping in a microfluidic fracture

Immiscible fluid-fluid displacement in confined geometries is a fundamental process occurring in many natural phenomena and technological applications, from geological CO2 sequestration to microfluidics. Due to the interactions between the fluids and the solid walls, fluid invasion undergoes a wetting transition from complete displacement at low displacement rates to leaving a film of the defending fluid on the confining surfaces at high displacement rates. While most real surfaces are rough, fundamental questions remain about the type of fluid-fluid displacement that can emerge in a confined, rough geometry. Here, we study immiscible displacement in a microfluidic device with a precisely controlled structured surface as an analogue for a rough fracture. We analyze the influence of the degree of surface roughness on the wetting transition and the formation of thin films of the defending liquid. We show experimentally, and rationalize theoretically, that roughness affects both the stability and dewetting dynamics of thin films, leading to distinct late-time morphologies of the undisplaced (trapped) fluid. Finally, we discuss the implications of our observations for geologic and technological applications.

Subsurface impact damage imaging for composite structures using 3D digital image correlation

An integrated system is proposed to visualize subsurface barely visible impact damage (BVID) in composite structures using three-dimensional (3D) digital image correlation (3D DIC). This system uses a pair of digital cameras to record video frames in the field-of-view (FOV) of the structure’s surface, capturing the wavefield generated via chirp excitation in the near-ultrasonic frequency range. Significant pitfalls of previous efforts of damage imaging using two-dimensional DIC have been largely mitigated. First, 3D DIC enables capturing out-of-plane displacements, which are much larger in amplitude versus in-plane displacements that a single camera would be limited to sensing, thus increasing the signal-to-noise ratio. This enhancement in turn increases the sensitivity of the stereo-camera system. Second, a total wave energy (TWE) damage imaging condition is proposed to visualize the local damage region. The monogenic signal obtained via Reisz transform (RT) is employed to compute the instantaneous amplitude, with which the local wave energy can be calculated spatially over time. Since a high displacement amplitude and thus high wave energy will occur in the damage region due to the local resonance, the proposed TWE imaging condition can relax the Nyquist sampling requirement, unlike guided-wave-based structural health monitoring techniques which require fully reconstructing the wavefield and wave modes through sampling that satisfies the Nyquist criterion. As such, a much lower camera frame rate is adequate for the proposed system. Consequently, the maximum spatial resolution of the camera for a given FOV can be achieved at the expense of a reduced frame rate. With the maximized pixel resolution and reduced frame rate for employing the TWE imaging condition, composite structures can be inspected or monitored with a larger FOV. As a result, there is no longer any need to apply signal enhancement techniques, such as sample interleaving, image stitching, or averaging, to increase the effective performance of the camera. Rather than needing thousands of repeated videos for minimizing the incoherent noise, only a single stereo-video with a few seconds of sampling duration is necessary for damage imaging. The use of a powerful piezo-shaker also increases the wave signal amplitude and further enhances sensitivity without permanent adhesion. To demonstrate this stereo-camera concept with the TWE imaging condition, the system was used to image damage in two carbon fiber reinforced polymer composite honeycomb panels, which had been subjected to low-velocity impacts (2 J). For each panel, two excitation configurations were used to verify the robustness of the system. Initial damage maps produced for a 100 × 100-mm FOV using a three-second stereo-video show accurate damage imaging ability that is independent of excitation location and comparable to benchmark damage images computed from laser Doppler vibrometer data and those gathered from ultrasonic and X-ray computerized tomography scans. This efficient and reliable integrated system demonstrated high potential for in-time damage inspection on composite aircraft and other critical structures.

Experimental study on evaluation of conglomerate reservoir support-type fracture conductivity in Xinjiang oilfield

The volume fracturing in the Mahu conglomerate reservoir, double-wing fractures are generated, resulting in inadequate proppant laying effect and low fracture conductivity. Experiments are designed to explore methods for improving the conductivity of conglomerate-supported fractures. Real triaxial indoor experiments are conducted to explore the effects of displacement, stress difference, and weak surfaces. The proppant diversion experiment explores the diversion ability under the conditions of single proppant, mixed proppant, and multiple sand-laying concentrations. Attention is focused on the impact of proppant embedding and fragmentation on conductivity. Research has shown that (1) stepped variable displacement fracturing is beneficial for controlling the generation of fractures. High displacement is beneficial for activating naturally weak surfaces. Small displacements are beneficial for identifying naturally weak surfaces and controlling the speed of crack extension. (2) Embedding of proppants mainly affects the conductivity of mixed base-supported conglomerates. Crushing mainly affects the conductivity of particles supporting conglomerate fractures. (3) Quartz sand or quartz sand-mixed ceramsite is used for conglomerate reservoirs with low effective closure stress and a complex matrix. Ceramic particles can are reduce the impact of fragmentation on the conductivity of particle-supported conglomerate reservoirs. Study aims to provide scientific guidance for the efficient development of the Mahu reservoir.

Three-dimensional core reconstruction and performance evaluation of CO2 displacement in a tight oil reservoir

In this study, a three-dimensional tight sandstone core was reconstructed digitally using serials thin sections cut from a core sample used in laboratory carbon dioxide (CO2) flooding experiments. Based on the digital core, multiphase flow simulations were carried out to evaluate the performance of three prior laboratory-tested injection strategies: CO2 continuous injection, water alternative gas (WAG: CO2) injection, and cyclic CO2 injection. The chosen image-based reconstruction led to a close porosity and permeability match with the sampled core in an economical way. The numerical evaluation closely replicated the laboratory-tested procedures, thus providing realistic fluid distributions before CO2 injection. To determine saturation functions for CO2 injection after water flooding, sensitivities of endpoint relative permeability and capillary pressure to CO2 continuous injection were quantified. Water relative permeability was identified as a key factor. The saturation functions were used in a history match between simulations and laboratory data where close agreements were observed for all three CO2 injection strategies. Then critical enhanced oil recovery (EOR) operational parameters (soaking time, slug ratio, cycle size, and test duration) were optimized to maximize CO2 displacement performance, which led to the following observations: (1) While extended soaking after CO2 continuous injection increased incremental oil recovery, such increase was limited due to concurrent soaking during low-rate CO2 injection. (2) In WAG injection, CO2 and brine slug sizes and ratios were optimized: increasing the cycle size performed better than adjusting the slug ratio for favorable mobility control and efficient CO2 EOR. (3) For cyclic CO2 injection, the total CO2 injection volume was the most important factor, followed by the number of cycles, to allow CO2 diffusion into tight core to maximize the swept pore volumes. The history-matched simulations suggest that both WAG and cyclic CO2 injection can achieve high displacement effectiveness for the tight reservoir, compared with that achieved with slight soaking after CO2 continuous injection. The injected brine slugs in the WAG injection reduced the CO2 needed at the expense of reduced storage capacity. Compared to WAG, cyclic CO2 injection, though realizing the highest oil recovery and gas storage, requires more CO2.

SAR Interferometry Data Exploitation for Infrastructure Monitoring Using GIS Application

Monitoring structural stability in urban areas and infrastructure networks is emerging as one of the dominant socio-economic issues for population security. The problem is accentuated by the age of the infrastructure because of increasing risks due to material deterioration and loss of load capacity. In this case, SAR satellite data are crucial to identify and assess the deteriorating conditions of civil infrastructures. The large amount of data available from SAR satellite sensors leads to the exploitation and development of new GIS-based procedures for rapid responses and decision making. In recent decades, the DInSAR technique has been used efficiently for the monitoring of structures, providing measurement points located on structures with millimeter precision. Our study has analyzed the behavior of structures in settlements, attempting to discuss the interactions of soil and structures, and examining the behavior of different types of structures, such as roads and buildings. The method used is based on long-term SAR interferometry data and a semi-automatic procedure to measure the displacement (mm/year) of structures, through a GIS-based application performed in the “Implemented MOnitoring DIsplacement” I.MODI platform. The analysis provides extensive information on long-term spatial and temporal continuity of up to 25 years of record, using satellite SAR multi-sensors from ERS, Envisat, and COSMO-SkyMed. The interpretation uses time series spatial analysis, supported by orthophotos, and layers of the DBTR (regional topographic database), Digital Surface model (DSM), and hydrogeological map to show anomalous areas with a high displacement rate and to observe the correlation of settlements in the sediments. With the satellite information and Geographic Information System (GIS), we were able to observe relevant parameters, such as the velocity of advance in the direction of the slope (deformation profiles), the cumulative displacement, and the trend changes in structures. The results illustrate an innovative procedure that allows the management of DInSAR data to facilitate the effective management of structures in which a monitoring protocol was developed at different spatial scales, integrating the information into a GIS.

Landslide detection and inventory updating using the time-series InSAR approach along the Karakoram Highway, Northern Pakistan

Karakoram Highway (KKH) is frequently disrupted by geological hazards mainly landslides which pose a serious threat to its normal operation. Using documented inventory, optical imagery interpretation, and frequency-area statistics, the features of slope failure, the spatial distribution, and their link to numerous contributing factors have all been effectively explored along the KKH. An updated inventory for the area was recreated using the interferometric synthetic aperture radar (InSAR) persistent scatterer (PS) technology to further investigate millimetre-accurate measurements of slope deformation (Vslope). Utilizing the PS approach, Sentinel-1 data from Jan 2018 to Jan 2022 were processed by which we obtained a deformation rate (VSlope) that varies between 0 and 364 mm/year. A total number of 234 landslides were cited from the literature and classified while 29 new potential landslides were detected and several pre-existing landslides were redefined by the InSAR approach, which was incorporated to generate an updated landslide susceptibility model with 86.6% of prediction precision in the area under curve method. As previous studies done by applying the InSAR technique incorporated a short span temporally and they missed some highly deforming zones like Budalas and Khanabad landslides, contain mean velocities > 50 mm/yr, which we studied individually in this work. In this study, a comprehensive application of the InSAR technique to assessing its performance in detecting and analysing landslides has been applied. The deformation velocity (Vslope) model shows high displacement in some regions, which needed to be further investigated by geoscientists, and the updated developed landslide inventory and susceptibility map can be used for land use planning and landslide mitigation strategies.

High performance electro-active artificial muscles based on 3D dendritic nickel cobalt sulfide nanorods-graphene electrodes

As the desire for biomimicry that utilizes the advantages of natural organisms, increases, electroactive artificial muscles, an emerging technology, have been phasing-in to bioinspired applications in medicine, electronics, and soft robotics. However, it remains challenging to simultaneously obtain stable response characteristics and high bending displacement, considering the instability of electrode materials in open air environments. Here, 3D dendritic nickel cobalt sulfide nanorods grown on graphene electrodes, exhibiting stable electrochemical reactivity owing to their structural and material advantages, are employed to realize high-performance artificial muscles. Importantly, the significant influence of the phase transition of nickel-cobalt metals and graphene template in the synthesis steps on tuning the electrical and electrochemical properties is reported. The resulting artificial muscles show an almost 98 % enhanced bending performance and stable response to both AC and DC input signals without significant phase delay or distortion. These substantial improvements in the performance of artificial muscles enable the demonstration of bioinspired soft locomotive robots; these artificial muscles will thus expand the soft electronics industry in the field of next-generation human-machine interfaces.

Experimental Investigation of the Vibration-Induced Heating of Polyetheretherketone for High-Frequency Applications

Dynamically loaded structures made of thermoplastic polymers have been extensively exploited in several demanding industries. Due to the viscoelastic and thermal properties of thermoplastic polymers, self-heating is generally inevitable, especially during dynamic deformations at high frequencies. Therefore, the thermoplastic polyether ether ketone (PEEK), with its high temperature resistance and high specific strength, is a particularly ideal candidate for dynamically loaded applications. Using scanning laser Doppler vibrometry and infrared thermography, an experimental study of the vibration characteristics and the vibration-induced heating of flat-sheet PEEK specimens was carried out. The specimens were base-excited by means of a piezoelectric actuator at high frequencies in the range between 1 and 16 kHz. As a result, a maximum temperature rise of approximately 6.4 K was detected for the highest investigated excitation. A high correlation between the spatial distribution of the velocity along the beam’s axial direction and the resulting temperature increase was measured. To summarize, the occurring self-heating of PEEK due to the dissipation of vibrational energy has to be critically considered for dynamically loaded structural applications, especially areas with high displacement amplitudes, such as antinodes, which yield the highest temperature increase.

A Systematic Experimental Study to Understand the Performance and Efficiency of Gas Injection in Carbonate Reservoirs

Summary Gas injection is the most widely applied recovery method in light, condensate, and volatile oil carbonate reservoirs. Gas has high displacement efficiency and usually results in a low residual oil saturation in the part of the reservoir that is contacted with gas. The displacement efficiency increases when the injected gas is near-miscible or miscible with the oil. In addition to nitrogen and hydrocarbon gas projects, carbon dioxide (CO2) enhanced oil recovery (EOR) has been the dominant gas EOR process. Gas-based EOR has been implemented in both mature and waterflooded carbonate reservoirs. In this paper, we present the results of a detailed experimental study aimed at understanding the performance and efficiency of gas injection in carbonate reservoirs. A series of immiscible and miscible gas injection coreflood experiments were performed using limestone reservoir cores under different injection strategies. To minimize laboratory artifacts, long cores were used in the experiments, and to observe the effect of gravity, both 2 in. diameter and 4 in. diameter (whole core) were used. The experiments were performed under reservoir conditions using live crude oil. The core wettability was restored by aging the core in crude oil for several weeks under reservoir temperature. Hydrocarbon gas (methane) was used as the immiscible injectant, and both CO2 and a mixture of 50% C1 and 50% CO2 were used as miscible injectant. All gas injection experiments were performed using vertically oriented cores, and the gas was injected from the top unless it is stated otherwise. The main parameters investigated in this study are as follows: The effect of miscibility on oil recovery for both continuous gas injection and water alternating gas (WAG). The effect of gravity on gas sweep efficiency compared to waterflooding. The effect of gas-oil interfacial tension (IFT) on oil recovery when using the same oil. The effect of oil type on oil recovery using the same injected gas at miscible and immiscible conditions. The effect of immiscible gas injection on subsequent miscible gas injection performance. Impact of CO2 cycle length on ultimate oil recovery. The impact of the order of fluid injection where multiple WAG injection cycles were performed in separate experiments after water or gas injection. The main conclusions of this study are as follows: As expected, miscibility has a significant impact on displacement efficiency and oil recovery where miscible gas recovered more than 20% extra oil compared to immiscible gas. A significant variation in oil recovery is observed for miscible gas injection (i.e., more than 10 saturation units difference) depending on the minimum miscibility pressure (MMP) between the injected gas and crude oil, even when both experiments are performed at miscible conditions using the same injected gas. The performance of tertiary CO2 flood was adversely affected by the slug of immiscible gas injected. Therefore, it is not recommended to have immiscible gas injection before miscible gas injection. Regardless of injected gas type, gas injection with similar IFTs achieved similar oil recovery. During WAG experiments, starting the injection cycles with water or gas did not have any impact on the ultimate oil recovery for both miscible and immiscible cases for one of the reservoirs, while WAG_G (WAG starting with gas injection) recovered more oil for another reservoir. Gravity has a significant impact on oil recovery for both miscible and immiscible gas injections. A significant difference is observed in oil recovery when comparing CO2 injection on 2-in.- and 4-in.-diameter core samples or when comparing horizontal vs. vertical immiscible gas injection and WAG experiment. The longer the CO2 slug size, the higher the oil recovery observed in gas injection experiments. The results of this study provide a rich and rarely available set of experimental data that can help improve and optimize gas and WAG injection in oil-wet carbonates.

Design of Piezoelectric Inertial Actuator with Wedge‐shaped Foot Structure for Cell Manipulation

AbstractAiming at the performance requirements of positioning accuracy and stability of piezoelectric inertial actuators in fields including micro‐operation and biomedical engineering, a piezoelectric inertial actuator with wedge‐shaped friction foot structure using bimorph films is proposed in this paper. The wedge‐shaped friction foot structure can adjust the friction force in different driving stages, which suppresses the backward motion and effectively improves the output performance of the actuator. And the bimorph films are processed by Micro Electromechanical Systems (MEMS) manufacturing process technology. It enables the actuator to move steadily with a small tip mass and facilitates the miniaturization of actuator. The simulation model is constructed based on the dynamic model of actuator and the prototype parameters are optimized from the results of simulation tests. Then a series of output performance experiments are carried out. Experimental results show that the proposed actuator has the advantages of high resolution, stability, and displacement linearity. And the highest resolution of 0.035 µm is achieved. Depending on above results, the cell drug injection simulation experiments are successfully conducted. The success of experiments shows that the prototype has good output performance and great application potential and value in the field of cell manipulation.