The paper presents the research results on duplex corrosion-resistant chromium–nickel–molybdenum cast steel of the GX2CrNiMoCuN 25-6-3-3 grade. The aim was to determine the effect of the soaking temperature for the hyperquenching process Tp, that is, 950 to 1200 °C, on the microstructure and mechanical properties, that is UTS tensile strength, the yield strength, HB Brinell hardness, the elongation EL and impact strength KV of the steel, cast under industrial conditions with the minimum content of Cr, Ni, Mo and Cu according to the PN-EN 10283 standard. On the basis of the results, it was confirmed that the hyperquenching guarantees the elimination of the brittle intermetallic phase in the steel microstructure. In addition, the most favorable strength-to-ductility ratio of the steel with an almost equal amount of austenite γ and ferrite α in its microstructure was obtained using the soak temperature of 1080 °C, which was considered optimal for the above-mentioned duplex cast steel.