Behaviour Of Materials Research Articles

Nondestructive testing techniques for investigating mechanical property and porosity disparities in extrusion 3D printed concrete

ABSTRACT Three Dimensional Concrete printing (3DCP) stands at the forefront of modern construction methodologies, also named additive manufacturing, offering unparalleled time, cost, and labour savings compared to conventional approaches. The evaluation of fresh state parameters like extrudability and buildability through a specialised concrete extruder, combined with a methodical layer-by-layer deposition, ensures structural stability by precisely strengthening each layer. Mechanical strength evaluations highlight the printed material’s anisotropic nature, revealing extreme reductions of Fy = 27.94%, Fx = 19.07%, and Fy = 16.33% in compression, flexural, and split tensile strengths, respectively, compared to cast specimens. This emphasises the importance of direction-specific mechanical testing in understanding material behaviour completely. Non-destructive testing (NDT) methods, like Ultrasonic Pulse Velocity (UPV) testing, are crucial for the qualitative assessment of the integrity and mechanical strength of concrete structures, including both printed and cast specimens, by establishing a strong correlation with compressive strength without causing any damage. Limited research indicates that the microstructure of the material plays a significant role in its mechanical strength, particularly in printed specimens. This claim is reinforced by mercury intrusion porosimetry (MIP) results, which reveal that printed specimens have slightly higher overall porosity, concentrated between 1 µm and 0.1 µm, while cast specimens show higher porosity in pores smaller than 0.1 µm.

Unravelling the mechanics of gastric tissue: A comparison of constitutive models, damage probability and microstructural insights

With the increasing prevalence of obesity worldwide, bariatric surgery is becoming increasingly common. However, the mechanic of the gastric wall related to bariatric surgery complications remains to be investigated. This study aims to understand mechanical behaviour of stomach by developing advanced material laws for gastric tissue incorporating microstructure. A multi-scale characterisation of the porcine stomach wall was performed in the fundus and corpus anatomical regions and in circumferential and longitudinal orientations The protocol included uniaxial tensile testing until damage, survival analysis to provide damage probability, comparison of phenomenological (Fung and Ogden order 1, 2 and 3) and structural (Holzapfel fibre-reinforced) computational models fitted to the experimental data, and quantitative analysis of elastin and collagen fibre structure from histological slides. All constitutive models fitted the experimental data well (r2 > 0.988 and RSME<3.8 kPa). Longitudinal and circumferential elastic modulus in quasi linear phase were respectively 1.75 ± 1.2 MPa, 0.76 ± 0.35 MPa for fundus, and 2.30 ± 0.66 MPa, 1.36 ± 0.89 MPa for corpus, highlighting significant differences between orientations in fundus and corpus, with an overall softer fundus in the circumferential direction. Microstructure analysis illustrated collagen and elastin fibre orientation, dispersion and density. As microstructure appears to play an important role in stomach biomechanics, model incorporating fibre structure such as Holzapfel fibre-reinforced model, seem best suited to describe the material behaviour of the stomach wall. Future research should complement these findings with an expanded sample set in human models.

Bulk and fracture process zone contribution to the rate-dependent adhesion amplification in viscoelastic broad-band materials

The contact between a rigid Hertzian indenter and an adhesive broad-band viscoelastic substrate is considered. The material behavior is described by a modified power law model, which is characterized by only four parameters, the glassy and rubbery elastic moduli, a characteristic exponent n and a timescale τ0. The maximum adherence force that can be reached while unloading the rigid indenter from a relaxed viscoelastic half-space is studied by means of a numerical implementation based on the boundary element method, as a function of the unloading velocity, preload and by varying the broadness of the viscoelastic material spectrum. Through a comprehensive numerical analysis we have determined the minimum contact radius that is needed to achieve the maximum amplification of the pull-off force at a specified unloading rate and for different material exponents n. The numerical results are then compared with the prediction of Persson and Brener viscoelastic crack propagation theory, providing excellent agreement. However, comparison against experimental tests for a glass lens indenting a PDMS substrate shows data can be fitted with the linear theory only up to an unloading rate of about 100μm/s showing the fracture process zone rate-dependent contribution to the energy enhancement is of the same order of the bulk dissipation contribution. Hence, the limitations of the current numerical and theoretical models for viscoelastic adhesion are discussed in light of the most recent literature results.

Evaluation of the Mechanical Properties of PLA Material Used For 3D Printing Solar E-Hub Component

The advent of additive manufacturing (AM) technologies revolutionized design and production processes across various industries. In renewable energy, AM enabled new possibilities for optimizing solar e-hub (solar energy harvesting module) configurations, enhancing efficiency and performance. This study examined critical considerations such as material selection, durability, and cost-effectiveness in solar hub development. This fast-prototyping technique was controlled by computer-aided design (CAD) software like CREO Parametric 7.0 and Creality Slicer 4.8. Experimental results indicated that PLA (Polylactic acid) materials exhibited superior strength, with an impact energy of 4.8 Joules. The deformation study revealed that the maximum load of 22 MPa aligned with the ultimate tensile strength of PLA, and a hardness test result of 83.1 HRF featured its exemplary hardness properties. These findings advanced the understanding of using AM to investigate mechanical behaviours of PLA materials and optimize solar e-hub configurations for portable device applications, promoting sustainable energy solutions and the adoption of renewable energy technologies. In addition, the successful implementation of this approach will enable the renewable energy sectors to minimize the carbon foot-prints towards helping the global net-zero emissions by aligning the circular economy approach.

Analysis of Inherent Frequencies to Mitigate Liquid Sloshing in Overhead Double-Baffle Damper

A disco-rectangular volume-fraction-of-fluid (VOF) model tank of a prismatic size is considered here for investigating the severe effect of overhead baffles made of three different materials, nylon, polyamide, and polylactic acid. In this work, the overdamped, undamped, and nominal damped motion of baffles and their effect are studied. In this research, the behaviour of different material baffles based on the sloshing effect and natural frequency of each baffle excited in damped, undamped, and overdamped cases is studied. VOF modelling is carried out in moving Yeoh model mesh with fluid–structure interaction between the water models for various baffle plates. The results of the water volume distribution and baffle displacement operating between a sloshing time of 0 and 1 s are recorded. Also, a strong investigation is carried out for the water volume suspended on overhead baffles by three different material selections.

Influence of Substrate Location on Mechanical Behaviour of Glass Fibre Composite Materials with Embedded Printed Electronics

Influence of Substrate Location on Mechanical Behaviour of Glass Fibre Composite Materials with Embedded Printed Electronics

Fluid-structure interaction analysis of a healthy aortic valve and its surrounding haemodynamics.

The opening and closing dynamics of the aortic valve (AV) has a strong influence on haemodynamics in the aortic root, and both play a pivotal role in maintaining normal physiological functions of the valve. The aim of this study was to establish a subject-specific fluid-structure interaction (FSI) workflow capable of simulating the motion of a tricuspid healthy valve and the surrounding haemodynamics under physiologically realistic conditions. A subject-specific aortic root was reconstructed from magnetic resonance (MR) images acquired from a healthy volunteer, whilst the valve leaflets were built using a parametric model fitted to the subject-specific aortic root geometry. The material behaviour of the leaflets was described using the isotropic hyperelastic Ogden model, and subject-specific boundary conditions were derived from 4D-flow MR imaging (4D-MRI). Strongly coupled FSI simulations were performed using a finite volume-based boundary conforming method implemented in FlowVision. Our FSI model was able to simulate the opening and closing of the AV throughout the entire cardiac cycle. Comparisons of simulation results with 4D-MRI showed a good agreement in key haemodynamic parameters, with stroke volume differing by 7.5% and the maximum jet velocity differing by less than 1%. Detailed analysis of wall shear stress (WSS) on the leaflets revealed much higher WSS on the ventricular side than the aortic side and different spatial patterns amongst the three leaflets.

Crossing length scales: X-ray approaches to studying the structure of biological materials.

Biological materials have outstanding properties. With ease, challenging mechanical, optical or electrical properties are realised from comparatively `humble' building blocks. The key strategy to realise these properties is through extensive hierarchical structuring of the material from the millimetre to the nanometre scale in 3D. Though hierarchical structuring in biological materials has long been recognized, the 3D characterization of such structures remains a challenge. To understand the behaviour of materials, multimodal and multi-scale characterization approaches are needed. In this review, we outline current X-ray analysis approaches using the structures of bone and shells as examples. We show how recent advances have aided our understanding of hierarchical structures and their functions, and how these could be exploited for future research directions. We also discuss current roadblocks including radiation damage, data quantity and sample preparation, as well as strategies to address them.

A Precise Prediction of the Chemical and Thermal Shrinkage during Curing of an Epoxy Resin.

A precise prediction of the cure-induced shrinkage of an epoxy resin is performed using a finite element simulation procedure for the material behaviour. A series of experiments investigating the cure shrinkage of the resin system has shown a variation in the measured cure-induced strains. The observed variation results from the thermal history during the pre-cure. A proposed complex thermal expansion model and a conventional chemical shrinkage model are utilised to predict the cure shrinkage observed with finite element simulations. The thermal expansion model is fitted to measured data and considers material effects such as the glass transition temperature and the evolution of the expansion with the degree of cure. The simulations accurately capture the exothermal heat release from the resin and the cure-induced strains across various temperature profiles. The simulations follow the experimentally observed behaviour. The simulation predictions achieve good accuracy with 2-6% discrepancy compared with the experimentally measured shrinkage over a wide range of cure profiles. Demonstrating that the proposed complex thermal expansion model affects the potential to minimise the shrinkage of the studied epoxy resin. A recommendation of material parameters necessary to accurately determine cure shrinkage is listed. These parameters are required to predict cure shrinkage, allow for possible minimisation, and optimise cure profiles for the investigated resin system. Furthermore, in a study where the resin movement is restrained and therefore able to build up residual stresses, these parameters can describe the cure contribution of the residual stresses in a component.

On-line and in-line quality assessment across all scale levels of 3D concrete printing

3D Concrete printing requires much more elaborate quality control procedures compared to conventional concrete processing. Due to the various process steps, and the corresponding variation in material behaviour, time-, and length-scales, a single quality indicator and measurement technique (similar to the ‘slump test’ for traditional construction) cannot be selected. Instead, three families of quality indicators have been established: homogeneity during material production and deposition (quality variations), material evolution during printing (transient material behaviour), and macroscopic features and geometric conformity during printing and of the final object (geometry). For each family, quality assessment techniques which have been proven in other fields or for different applications, have been successfully transferred and adapted to the 3DCP process. In some cases, completely new methods have been developed. This paper aims to provide the state-of-the-art in such quality assessment methods, indicating high potential methods and research gaps across all scale levels of 3D concrete printing processes.

Fretting fatigue life of galvanized bridge support cable wire: Experimental study and strain-based fracture mechanics analysis

The galvanized wires used in cable bridges can fail due to fretting fatigue. Experimental results have shown that defects resulting from the galvanization process are a possible source of initiation for fatigue cracks and make the life shorter than that of a wire without a galvanized layer. The investigation presented in this paper uses strain-based fracture mechanics to analyze the influence of these defects on the fatigue life of galvanized wire. The presented analysis considers nonlinear material behaviour. A 3D finite element model is used to compute the required stress field. Stress intensity factors are obtained by a proposed numerical point load weight function, and shape factors are found for the surface and deepest points of the semielliptical crack. Plain fatigue tests of galvanized wires are performed to calibrate key model parameters. The calibrated model is then shown to provide reasonably accurate but systematically conservative estimates of the fatigue life under fretting conditions typical of bridge stay cable saddle supports.

Evaluation of the fatigue life of AISI 347 specimens with small notches based on local strain considerations

The use of materials data for cyclic loading determined on unnotched specimens to predict the fatigue life of notched components has a long tradition, specifically when it comes to nuclear engineering. The basic principle is that the material behaviour of the unnotched specimens can be transferred to what the material is exposed to be in a notch root. This principle has been proven for large notches. However, what happens when the notch is relatively small? Can the fatigue life still be predicted on the grounds of what has been considered as the local strain or Neuber approach? A key reference in that regard is the Neuber equation or generally the load versus notch stress, notch strain – or any combination of those – relationship. In a larger study, unnotched and notched specimens from the metastable austenitic steel AISI 347 have been tested and characterized providing a database that may give some answers to the question raised above.The unnotched specimens considered here had a cross-section diameter of 10 mm while the notch radii of the notched components were only 0.5 and 0.35 mm, respectively. Notch radii of such dimensions will easily reach a fully plastic condition once the material has exceeded the yield limit, because the difference in load between yield start in the notch and full plastification is relatively small. This fully plastic state exceeds the validity of the Neuber equation and requires respective corrections. In this paper it is shown how such corrections can be obtained through a finite element analysis and how this applies to the cases mentioned above.

Modelling insertion behaviour of PVP (Polyvinylpyrrolidone) and PVA (Polyvinyl Alcohol) microneedles

A comprehensive investigation into the effects of nonlinear material behaviour of polymeric (MN) and skin on the dynamics of the MN insertion in skin was undertaken in this study using experiments and numerical simulations. The nonlinearity of the material behaviour was incorporated by employing the Ramberg–Osgood and neo-Hookean equations for stress–strain relationships for the MN materials and skin, respectively. For this purpose, a characteristic type of dissolving MN array was selected. This type of MN is made by a combination of poly(vinyl alcohol) and poly(vinyl pyrrolidone). The numerical simulations were validated using experimental investigations where the MNs were fabricated using laser-engineered silicone micromould templates technology. Young’s modulus, Poisson’s ratio, and compression breaking force for the MN polymers were determined using a texture analyser. The alignment between experimental findings and simulation data underscores the accuracy of the parameters determined through mechanical testing and mathematical calculations for both MN materials (PVP/PVA) and skin behaviour during the MN insertion. This study has demonstrated a strong alignment between the experimental findings and computational simulations, confirming the accuracy of the established parameters for MNs and skin interactions for modelling MN insertion behaviour in skin, providing a solid foundation for future research in this area.

Numerical Modelling of Corrugated Paperboard Boxes

Numerical modelling of corrugated paperboard is quite challenging due to its waved geometry and material non-linearity which is affected by the material properties of the individual paper sheets. Because of the complex geometry and material behaviour of the board, there is still scope to enhance the accuracy of current modelling techniques as well as gain a better understanding of the structural performance of corrugated paperboard packaging for improved packaging design. In this study, four-point bending tests were carried out to determine the bending stiffness of un-creased samples in the machine direction (MD) and cross direction (CD). Bending tests were also carried out on creased samples with the fluting oriented in the CD with the crease at the centre. Inverse analysis was applied using the results from the bending tests to determine the material properties that accurately predict the bending stiffness of the horizontal creases, vertical creases, and panels of a box under compression loading. The finite element model of the box was divided into three sections, the horizontal creases, vertical creases, and the box panels. Each of these sections is described using different material properties. The box edges/corners are described using the optimal material properties from bending and compression tests conducted on creased samples, while the box panels are described using the optimal material properties obtained from four-point bending tests conducted on samples without creases. A homogenised finite element (FE) model of a box was simulated using the obtained material properties and validated using experimental results. The developed FE model accurately predicted the failure load of a corrugated paperboard box under compression with a variation of 0.1% when compared to the experimental results.

Data-driven methods for computational mechanics: A fair comparison between neural networks based and model-free approaches

We present a comparison between two approaches to modelling hyperelastic material behaviour using data. The first approach is a novel approach based on Data-driven Computational Mechanics (DDCM) that completely bypasses the definition of a material model by using only data from simulations or real-life experiments to perform computations. The second is a neural network (NN) based approach, where a neural network is used as a constitutive model. It is trained on data to learn the underlying material behaviour and is implemented in the same way as conventional models. The DDCM approach has been extended to include strategies for recovering isotropic behaviour and local smoothing of data. These have proven to be critical in certain cases and increase accuracy in most cases. The NN approach contains certain elements to enforce principles such as material symmetry, thermodynamic consistency, and convexity. In order to provide a fair comparison between the approaches, they use the same data and solve the same numerical problems with a selection of problems highlighting the advantages and disadvantages of each approach. Both the DDCM and the NNs have shown acceptable performance. The DDCM performed better when applied to cases similar to those from which the data is gathered from, albeit at the expense of generality, whereas NN models were more advantageous when applied to wider range of applications.

Mechanical characterisation and high temperature analysis of hyperelastic adhesives – Modelling and experimental validation

Adhesive bonds are subject to multiple environmental conditions that can affect their mechanical performance during service. Therefore, it is important to evaluate the influence of temperature on adhesive strength, as it can impact joint safety and should be considered during the design phase. This study presents an analysis of the effect of high temperatures on the mechanical behaviour of joints made with highly elastic adhesives, specifically a polyurethane and a silicon-modified polymer. Shear and tensile tests were conducted at temperatures of 23, 50, and 80 °C using dumbbell specimens for tensile tests and single lap specimens (SLJ) for shear tests. The tests were performed with two different substrates, aluminium (Al) and glass fibre reinforced polyester panel (GRP), and with varying adhesive thicknesses. These tests aim to assess the impact of temperature conditions on the mechanical properties of the adhesive and the behaviour of the joints. The analysis of the experimental results reveals that the adhesive degrades when exposed to high temperatures, resulting in reduced strength and stiffness, and less linear behaviour.Furthermore, this work involves the determination of a model able to reproduce the mechanical behaviour of hyperelastic adhesive at high temperatures, considering diverse constitutive modelling approaches. To achieve this, a testing protocol was conducted on basic uniaxial and planar specimens. The results indicate that the Ogden N=2 model is the most suitable for representing the non-linear behaviour of the hyperelastic adhesive at high temperatures. In contrast, the Mooney Rivlin model is more suitable to represent the material behaviour under ambient conditions. To conclude this work, the law has been satisfactorily validated by comparing the results of tests carried out on SLJ specimens with different adhesive thicknesses.

Comparison of elements and state-variable transfer methods for quasi-incompressible material behaviour in the particle finite element method

AbstractThe Particle Finite Element Method (PFEM) is attractive for the simulation of large deformation problems, e.g. in free-surface fluid flows, fluid–structure interaction and in solid mechanics for geotechnical engineering and production processes. During cutting, forming or melting of metal, quasi-incompressible material behaviour is often considered. To circumvent the associated volumetric locking in finite element simulations, different approaches have been proposed in the literature and a stabilised low-order mixed formulation (P1P1) is state-of-the-art. The present paper compares the established mixed formulation with a higher order pure displacement element (TRI6) under 2d plane strain conditions. The TRI6 element requires specialized handling, involving the deletion and re-addition of edge-mid-nodes during triangulation remeshing. The robustness of both element formulations is analysed along with different state-variable transfer schemes, which are not yet widely discussed in the literature. The influence of the stabilisation factor in the P1P1 element formulation is investigated, and an equation linking this factor to the Poisson ratio for hyperelastic materials is proposed.

Effects of Rubber Core on the Mechanical Behaviour of the Carbon-Aramid Composite Materials Subjected to Low-Velocity Impact Loading Considering Water Absorption.

The large-scale use of composite materials reinforced with carbon-aramid hybrid fabric in various outdoor applications, which ensures increased mechanical resistance including in impact loadings, led to the need to investigate the effects of aggressive environmental factors (moisture absorption, temperature, thermal cycles, ultra-violet rays) on the variation of their mechanical properties. Since the literature is still lacking in research on this topic, this article aims to compare the low-velocity impact behaviour of two carbon-aramid hybrid composite materials (with and without rubber core) and to investigate the effects of water absorption on impact properties. The main objectives of this research were as follows: (i) the investigation of the mechanical behavior in tests for two impact energies of 25 J and 50 J; (ii) comparison of the results obtained in terms of the force, displacement, velocity, and energy related to the time; (iii) analysis of the water absorption data; (iii) low-velocity impact testing of wet specimens after saturation; (iv) comparison between the impact behaviour of the wet specimens with that of the dried ones. One of the main findings was that for the wet specimens without rubber core, absorbed impact energy was 16% less than the one recorded for dried specimens at an impact energy of 50 J. The failure modes of the dried specimens without rubber core are breakage for both carbon and aramid fibres, matrix cracks, and delamination at matrix-fibre interfaces. The degradation for the wet specimens with rubber core is much more pronounced because the decrease in the absorbed impact energy was 53.26% after 10,513 h of immersion in water and all the layers were broken.

Strength and fabric anisotropy of granular materials under true triaxial configurations using DEM

This paper investigates the strength and fabric anisotropy of granular materials under true triaxial configurations using the discrete element method. A clump logic based on the multi-sphere approach was utilized to replicate realistic particle shapes. The evolutions of deviatoric stress and volumetric strains were found to be independent of mean effective stress, and intermediate principal stress parameter (b). From a macroscopic viewpoint, all samples exhibited initial strain hardening followed by softening behaviour, stabilizing at large deviatoric strains due to the dense state of assemblies. The peak state friction angles showed dependency on the b-value, aligning closely with experimental findings. Microscopic parameters such as mechanical coordination number and sliding fraction were found to be approximately independent of b-values. Additionally, non-coaxiality was observed for various b-values except for specific shear modes, aligning with previous findings using spherical particles. These results highlight the capability of clumped particles to simulate the true mechanical behaviour of granular materials and contribute to our understanding of their complex response under different loading conditions.

Frictional strength of siliciclastic sediment mixtures in fault stability assessment

Frictional strength of fault zones is a key parameter for evaluation of fault stability and reactivation. We measure friction using the direct shear test (DST) for (i) sand-clay mixes mimicking fault gouges, and (ii) strength of fault zone interfaces. The sand-clay mixing ratio is linked to the established Shale Gouge Ratio (SGR) used in fault seal analysis, suggesting an approach for linking the measured frictional properties to the established subsurface fault characterization methods and risk assessment. We use powdered caprock material from the Draupne Formation mixed with sand to prepare the fault gouge and discuss application of results for fault zones on the Horda Platform, Norwegian North Sea.Shearing of fault gouge show a systematic decrease in residual friction coefficient with increasing clay content from 0.6 (φ = 31°) in pure sand (SGR 0%) to 0.4 (φ = 22°) for clay rich mixtures (SGR 100%). Interface testing mimicking fault gouge on sand surface is less systematic and shows residual friction coefficients ranging from 0.53 to 0.6 (φ = 28–31°) for SGR 0–50%. Detailed interpretation of the shear testing results shows changes in drainage properties, volumetric changes during shearing and shear responses to normal stresses indicating threshold values for sand versus clay dominated material behaviour. However, the results are non-conclusive on the question if a linear variation of friction with clay content or a threshold between sand dominated versus clay dominated friction provides the best approach for linking friction to fault clay content.