Low Ductility Research Articles

Friction and Wear Behavior of Selective Laser Melted Ti6Al4V-Equine Bone Nanocomposites

Ti6Al4V is commonly used in implants because of its excellent mechanical properties, corrosion resistance, and biocompatibility. While Hydroxyapatite (HAp) is typically used for strong biological bonding between Ti6Al4V implants and bone tissue, this study takes a different approach by incorporating Equine Bone (EB), which has a chemical structure similar to human bone tissue, as a substitute for HAp. In this study, to develop implant materials with a low elastic modulus, high strength, and excellent wear resistance, Ti6Al4V used in biomedical applications was combined with natural EB. Subsequently, a Ti6Al4V-0.05EB composite was fabricated using ball milling followed by Selective Laser Melting (SLM). SLM can reproduce even the interior of a 3D structure, so various studies are being conducted to apply it as a biomaterial. However, Ti6Al4V alloys produced by SLM are known to have low ductility due to localized heat gradients, rapid solidification, and cooling rates. This reduced ductility can result in decreased formability of biomaterials, and the high elastic modulus may lead to stress shielding phenomena, potentially reducing the lifespan of the biomaterial. To minimize this, a post-heat treatment was applied to the Ti6Al4V-0.05EB composite material manufactured by SLM. Afterwards, the microstructure, mechanical properties, and wear resistance, which are important in biomaterials, were evaluated.

Study on electric pulse-assisted plastic deformation behavior of 5182-O aluminum alloy

Plastic model-based neural networks are emerging phenomenological models with excellent calibration accuracy and interpretability of parameters, and they do not significantly increase the finite element calculation time of neural network models with a simple structure optimized by the algorithm. Because aluminum and magnesium have low ductility at room temperature, complex components made from these alloys need to be forged at high temperatures. In comparison with traditional thermoforming, advanced current-assisted processing provides energy savings, efficiency and green production. Experimental and constitutive modeling are carried out in this study to investigate the coupling effects of electrical pulse, temperature, strain rate, and strain on flow behavior and ductile fracture. It has been shown that electric pulses induce Joule heating effects and electroplastic effects, which reduce deformation resistance and improve formability. Electrical pulses suppress negative strain rate effects caused by dynamic strain aging, which is the main reason for the non-monotonic relationship between temperature and strain rate. The behavior of plasticity and fracture initiation can be described by simulations based on a neural network-based evolving plasticity model that incorporates stress states, current density, temperature, and strain rates.

Strengthening Fe1.4Co0.8Ni0.8Cr high-entropy alloy composites via in-situ synthesis of TiC: Perspective from experiments and first principles calculations

Achieving a harmonious balance between strength and plasticity is a long-standing problem in single-phase face-centered-cubic (fcc) high-entropy alloys (HEAs). Herein, in-situ TiC ceramic particle reinforced fcc-structured Fe1.4Co0.8Ni0.8Cr HEAs is designed and investigated by combining the experiments and first-principate calculations. The results show that the y (TiC)–Fe1.4Co0.8Ni0.8Cr (y = 0, 2.5, 5.0, 7.5 and 10.0 %, y: volume fraction) composites consist of fcc phase with submicron/micron TiC after the co-addition of Ti and C element, and the formation of TiC facilitates to refine the microstructure of the composites. Such microstructural evolutions significantly enhance the mechanical performances of the composites. Particularly, the 7.5 % (TiC)–Fe1.4Co0.8Ni0.8Cr composite exhibits a high yield strength of ∼562.7 ± 7.7 MPa and tensile strength of ∼971.3 ± 5.4 MPa, which are respectively increased by 169.0 % and 88.3 % as compared with the Fe1.4Co0.8Ni0.8Cr based alloy, yet with the fracture elongation decreases to 35.9 ± 0.3 %. The increment in yield strength is mainly driven from the combined effect of the grain refinement strengthening, dislocation strengthening and precipitation strengthening. Density functional theory (DFT) results reveal that the increase of C–Ti bonds and the formation of covalent bonds in the 7.5 % (TiC)–Fe1.4Co0.8Ni0.8Cr composite lead to relatively higher strength and lower ductility, which are well agreed with the experimental results.

Eliminating cracks in Ti–47Al–2Cr–2Nb/Ti–6Al–4V micro-laminated composites fabricated by dual-material laser powder bed fusion

The low ductility of titanium aluminide at room temperature has been one of the factors that severely limit its applications. In this study, Ti–6Al–4V (Ti64) alloys were combined with Ti–47Al–2Cr–2Nb (TiAl) alloys to make micro-laminated composites with optimal ply configurations to eliminate crack formation in TiAl and improve the ductility. A dual-material laser powder bed fusion (LPBF) system was used to fabricate the TiAl/Ti64 micro-laminate samples. The presence of cracks, elemental composition and mechanical properties were experimentally characterised and analysed to understand the effect of ply configuration and the mechanism of eliminating cracks. It was found that smaller TiAl ply thickness and lower TiAl volume fraction result in fewer cracks formed in the micro-laminates. Elemental composition analysis reveals that the Al content in the first two powder layers (i.e., 200 μm thick in total) of a TiAl ply is reduced to 10%–35% due to the partial mixture of the TiAl ply and the proceeding Ti64 ply in the LPBF. The reduced Al content leads to combined α-Ti, β-Ti and α2-Ti3Al phases instead of γ-TiAl phases, thus eliminating the formation of cracks within the first 200 μm thick region of the TiAl ply. This study demonstrates that crack-free and dense TiAl/Ti6 micro-laminated composites can be produced with the TiAl ply thickness reduced to 200 μm and the TiAl volume fraction reduced to 25% (Ti64 ply thickness 400 μm). Ductility of the crack-free micro-laminates at room temperature is comparable to or even exceeds the properties of TiAl/Ti64-type laminates made by other manufacturing processes, which may imply good machinability. Note that further research is required to investigate the properties and applications of the micro-laminates at elevated temperatures.

Effect of solid-solution treatment on high-temperature properties and creep fracture mechanism of laser powder bed fused Inconel 625 alloy

Laser powder bed fusion (LPBF) has been widely used for fabricating Inconel 625 (IN625) alloy, and it is widely regarded as a promising manufacturing technology. However, during high-temperature service, the γ″ strengthening phase of LPBFed IN625 gradually transforms into the detrimental δ phase. Controlling the morphology and distribution of precipitates is necessary for optimizing high-temperature performance. This study compared the as-built and 1090 °C solution-treated LPBFed IN625 alloy and investigated the microstructure evolution, tensile properties, and creep fracture behavior at a high temperature of 815 °C. The results show that the solid-solution treatment improves the creep ductility of LPBFed IN625 alloys at 815 °C by forming a high percentage of twinned boundaries and eliminating dislocations. The formation of coarsened needle-like δ phases and carbides during creep reduces the strength of the grain boundaries and is responsible for creep fracture failure. During creep of the as-built samples, the irregular Laves phase between the columnar dendrites gradually transforms into plate-like δ phases and M6C carbides uniformly and densely distributed within the columnar grains. The precipitation-strengthening effect of these fine precipitates, combined with the initial high density of dislocations and strong texturing effect, brings favorable high-temperature strength and creep fracture life but consequently leads to low creep ductility.

Controlling splat boundary network evolution towards the development of strong and ductile cold sprayed refractory metals: The role of powder characteristics

Feedstock powder characteristics such as composition (specific alloying elements and concentrations and impurity levels), microstructure, thickness/composition of surface oxide layers, and particle size distribution play a crucial role in determining the overall mechanical properties of cold sprayed deposits. Herein, we report on two deposits consolidated via cold spray processing from differently-sourced batches of nominally identical elemental refractory powders under identical spraying conditions, which exhibit bending strength and ductility values that differ by more than a factor of two – and with the weakest sample displaying negligible effective ductility. Through chemical, microstructural and micromechanical characterization of both the feedstock powders and cold sprayed deposits, we consider the possible influences of feedstock characteristics on the mechanical performance of cold spray consolidated deposits. It is shown that while differences in interstitial oxygen and hydrogen content may result in differences in the intrinsic yield characteristics of the feedstock material, both feedstocks maintain the ductile behavior required to induce good metallurgical bonding upon impact of optimally sized powder particles. We conclude that the deposits formed from the two feedstock powders are indistinguishable and exhibit high ductility when characterized locally within the relatively undeformed bulk of a single particle or splat. However, the two sprayed deposits show low ductility or brittle behavior when loaded in tension across intersplat boundary domains comprising material that has undergone extensive deformation. In addition, one feedstock incorporates a broader particle size distribution, with a long tail of larger-than-optimal particles. These larger particles are accelerated below the critical impact velocity, resulting in observed imperfect metallurgical bonding at splat interfaces and higher porosity at such intersplat boundaries. This result, combined with the overall differences in the morphology of the intersplat boundary network between the two deposits, explains the difference in macroscopic mechanical behavior. We conclude that accurate control of the powder feedstock particle size distribution is essential for optimizing the mechanical integrity of cold sprayed refractory elements and alloys.

Achieving high strength-ductility combination of Al–Mn–Mg-Sc-Zr alloy subjected by laser powder bed fusion and suitable post heat treatment

Post heat treatment is crucial for optimizing the performance of additive manufacturing components, yet it is still challenging to synergistically improve the strength and ductility through simple heat treatment. The present work investigated the microstructure evolution and mechanical properties of laser powder bed fusion (L-PBF) additive manufactured Al–Mn–Mg-Sc-Zr alloy after aging at 300 °C for different durations. All the as-built and aged samples exhibited a typical bi-modal microstructure consisting of coarse columnar and fine equiaxed grain regions. The as-built samples contained a number of primary Al6Mn precipitates distributed along grain boundaries; meanwhile, Mg solutes segregation was visible at grain boundaries, forming “Mg walls”. After aging for 4 h, the Al6Mn and a small content of Al3Sc were precipitated. Two types of Mg-rich precipitates evolved along grain boundaries simultaneously, increasing ultimate tensile strength from 401 MPa to 501 MPa, while the ductility was significantly reduced from 19.6 % to 4.6 %. When increased to 6 h, the Mg-rich precipitates disappeared, and the density of Al6Mn and Al3Sc precipitates reached its peak concurrently, providing a dual-precipitate strengthening effect. As a result, an excellent strength-ductility balance with an ultimate tensile strength of 528 MPa and ductility of 14.5 % was obtained. The Al6Mn precipitates became coarsening with increasing to 7 h, resulting in lower ductility. The strategy of modulating elemental distribution and precipitated phases by simple heat treatment is expected to be further developed for high strength and ductility Al alloys prepared by L-PBF.

Enhancing interface bonding strength of Ti/Al laminated composites via periodic surface nano-crystallization pretreatment

Ti/Al laminated composites have high strength and excellent corrosion resistance, while the relatively low interface bonding strength has still restricted its wide usage. This paper proposes a new method to improve the interface bonding strength of Ti/Al laminated composites through surface nano-crystallization pretreatment using ultrasonic rolling technique. The mechanical property, interface characteristics and interface bonding mechanism are thoroughly studied. The results show that ultrasonic rolling surface pretreatment enables the strong interface bonding of Ti/Al laminated composites and greatly reduces the rolling reduction threshold. It is revealed that ultrasonic rolling surface pretreatment can generate periodic grooves and nanocrystalline layer with low ductility on the Ti surface, which can effectively promote cracking of the Ti hardening layer and increase the contact area of virginal Ti and Al metals during rolling process. Besides, ultrasonic rolling forms nanocrystals and high-density defects on the top surface of the titanium layer, which promote the migration, exchange and rearrangement of atoms under severe plastic deformation and eventually lead to the formation of amorphous structures in the transition layer of the Ti/Al interface. Therefore, the Ti/Al laminated composites pretreated using ultrasonic rolling technique exhibit outstanding interface bonding strength, especially at relatively low rolling reduction conditions.

Polymer based multi-layer Al composite current collector improves battery safety

The safety problem obstructs the large-scale application of high energy batteries. Instantaneous short circuit at millisecond triggers uncontrollable thermal runaway in high energy batteries. Herein, to shut down the short circuit at early stage, we accomplish the safety design using composite current collector that spontaneously breaks due to its heterogeneous ductility. The composite current collector has a core with high ductility (the polyethylene terephthalate base), and a skin with low ductility (multi-layer metal). Controlled oxygen is introduced when evaporating aluminum atoms onto the polyethylene terephthalate base, therefore the skin layer will be composed of aluminum and aluminum-oxide layers in staggered rows. The multi-layer skin is more susceptible to crack under the mesoscopic deformation than the plastic core, thereby preventing short circuit by cutting off the pathway of electrons. The cell assembled by the multi-layer composite current collector can pass the nail penetration test without spark, fire and explosion, while the cell with pure current collector and composite current collector with single layer skin cannot. The assembled cell has comparable electrochemical performance (88% capacity retention after 450 cycles) with the reference cell. This work affords novel ideas for the high safety structural design of high energy batteries.

Surface characteristics of additively manufactured γ-TiAl intermetallic alloys post-processed by electrochemical machining

Electron beam melting (EBM) process is the most preferable powder bed fusion process for high melting point alloys. γ-TiAl alloys are intermetallic chemical compounds, which are lightweight and resistant to oxidation and heat, and have low ductility as well. EBM is the best manufacturing process for such alloys to produce aerospace parts, but poor surface quality is the main drawback of this process. Thus, surface post-processing is needed after the EBM process. This study presents the surface characteristics of EBM γ-TiAl alloy surfaces post-processed by electrochemical machining (ECM). The surfaces were ECM and the surface roughness values (Sa, Sq and Sz) have been reduced significantly. The mean reduction values of the experiments are 98.6 %, 98.5 % and 95.3 % for Sa, Sq and Sz, respectively. Additionally, it is observed that the surface roughness is inversely proportional to the electrolyte conductivity up to a limit value (115 mS/cm), and after that the roughness increases via the stray current transition. Sq values decrease with the increased feed rate via the increased current density. However, an increase in feed rate negatively affects the Sku values, which statistically describe the sharpness or spread of surface roughness. Also, XRD results showed that Ti2AlN layer is formed on the surface via the HIP operation. This layer inhibits the electrochemical dissolution of γ-TiAl alloy and caused surface defects.

Experimental and numerical investigation on out-of-plane ultimate strength of high-strength steel arches

This study presents an experimental investigation on the out-of-plane ultimate strength of high-strength-steel (HSS) I-section arches, which has not been reported previously. Fourteen I-section HSS arches having different yield strengths, cross-sectional dimensions, slendernesses, and rise to span ratios were tested under three-point symmetrical vertical loading. The corresponding out-of-plane deformation modes and strengths are identified. Subsequently, in order to predict the out-of-plane capacities of HSS arches, a finite element analyses is carried out, which takes into consideration residual stresses and initial geometrical imperfections. This analysis demonstrates a strong alignment with the experimental results, confirming the accuracy of finite element model and experimental results. Furthermore, the study comprehensively analyzes the influence of yield strength of steel, rise-span ratio, and slenderness on the ultimate bearing capacity of HSS arches. Through a parametric analysis, design formulas for the out-of-plane bearing capacity of HSS arches subjected to arbitrary compression forces combined with arbitrary bending moments are formulated. It is found that the out-of-plane ultimate strength of HSS arches is significantly influenced by the yield strength of the steel. Compared to a low strength steel (LSS) arch, the out-of-plane ultimate bearing capacity of the HSS arch increases with an increase in yield strength in the plastic stage, and the ultimate lateral displacement of the HSS arch decreases with an increase in yield steel strength due to the lower ductility of HSS. In addition, after reaching the out-of-plane ultimate bearing load of arch, the load-displacement curve of the HSS arch drops faster than the LSS arch. It is also found that the proposed design formulas can effectively predict the out-of-plane bearing capacity of HSS arches.

In-situ study of microstructure and mechanical properties of GH3536 alloy manufactured by selective laser melting at 750 °C

Nickel-based GH3536 alloy exhibits high strength but low ductility when produced by selective laser melting (SLM), which hinders its widespread application in aerospace. This paper employed a ‘two-step’ method of heat treatment to optimize the microstructure of the SLM GH3536 alloy and investigated the mechanical properties. Tensile tests were conducted on SLM GH3536 alloy before and after heat treatment at 750 °C, using an in-situ high-temperature tensile stage. The relationship between the microstructural evolution and deformation behavior of the alloys was investigated by combining the in-situ tensile experiments and crystal plasticity finite element method (CPFEM). The results suggested that the elongation can be increased by 80% without a significant reduction in tensile strength. The improved elongation is attributed to the complete recrystallization, formation of annealed twins and serrated grain boundaries after heat treatment. The study also investigated the deformation behavior and fracture mode of the alloy before and after heat treatment. Discussion was done on the influence of the microstructure, particularly the twin and serrated grain boundaries on the alloy's plastic deformation. This study enhanced the understanding of plastic deformation of SLM GH3536 alloy and provided a valuable reference for the design and post-treatment of superalloy.

Kink bands promote exceptional fracture resistance in a NbTaTiHf refractory medium-entropy alloy.

Single-phase body-centered cubic (bcc) refractory medium- or high-entropy alloys can retain compressive strength at elevated temperatures but suffer from extremely low tensile ductility and fracture toughness. We examined the strength and fracture toughness of a bcc refractory alloy, NbTaTiHf, from 77 to 1473 kelvin. This alloy's behavior differed from that of comparable systems by having fracture toughness over 253 MPa·m1/2, which we attribute to a dynamic competition between screw and edge dislocations in controlling the plasticity at a crack tip. Whereas the glide and intersection of screw and mixed dislocations promotes strain hardening controlling uniform deformation, the coordinated slip of <111> edge dislocations with {110} and {112} glide planes prolongs nonuniform strain through formation of kink bands. These bands suppress strain hardening by reorienting microscale bands of the crystal along directions of higher resolved shear stress and continually nucleate to accommodate localized strain and distribute damage away from a crack tip.

Mechanical behavior of ECC-reinforced coupled shear wall

PurposeBased on the weak seismic performance and low ductility of coupled shear walls, engineered cementitious composites (ECC) is utilized to strengthen it to solve the deformation problem in tall buildings more effectively and study its mechanical properties more deeply.Design/methodology/approachThe properties of reinforced concrete coupled shear wall (RCCSW) and reinforced ECC coupled shear wall (RECSW) have been studied by numerical simulation, which is in good agreement with the experimental results. The reliability of the finite element model is verified. On this basis, a detailed parameter study is carried out, including the strength and reinforcement ratio of longitudinal rebar, the placement height of ECC in the wall limb and the position of ECC connecting beams. The study indexes include failure mode and the skeleton curve.FindingsThe results suggest that the bearing capacity of RECSW is significantly affected by the ratio of longitudinal rebar. When the ratio of longitudinal rebar increases from 0.47% to 3.35%, the bearing capacity of RECSW increases from 250 kN to 303 kN, an increase of 21%. The strength of longitudinal rebar has little influence on the bearing capacity of RECSW. When the strength of the longitudinal rebar increases, the bearing capacity of RECSW increases little. The failure mode of RECSW can be improved by lowering the casting height of the ECC beam in a certain range.Originality/valueIn this paper, ECC is used to strengthen the coupled shear wall, and the accuracy of the finite element model is verified from the failure mode and skeleton curve. On this basis, the casting height of the ECC casting wall limb, the strength and reinforcement ratio of longitudinal rebar and the position of the ECC beam are studied in detail.

Time-dependent seismic reliability analysis of rocking cold-formed steel frame based on improved HOMM

Cold-formed steel structures are particularly sensitive to seismic loads due to their relatively low ductility and limited energy dissipation capacity. Moreover, the small thickness of cold-formed steel structures makes them more susceptible to environmental influences, leading to corrosion and material degradation. Therefore, it is essential to quantitatively assess the seismic reliability of cold-formed steel structures from a lifecycle perspective. Current structural reliability design standards often focus on the ultimate strength at the component level while neglecting the global safety of structures. Additionally, it tends to neglect the time-variant characteristic of structural resistance due to the corrosion and degradation of materials. Therefore, the time-dependent seismic reliability analysis framework was proposed at the global structural level based on an improved high-order moment method (HOMM). It directly addresses the objective failure probabilities at the global structural level and takes into account the resistance degradation of structures in the design reference period. A comparative analysis of the time-dependent seismic reliability between rocking cold-formed steel frames and rigid cold-formed steel frames is conducted, focusing on load-bearing capacity limit states and deformation capacity limit states. The investigation indicates that the differences between time-dependent and time-independent seismic reliability indexes are substantial. For cold-formed steel structures subjected to prolonged exposure to the corrosive environment, it is recommended to consider the time-dependent degradation of structures.

Numerical assessment of using FRP rebars as an alternative passive reinforcement in RC beams

AbstractRecent sustainable building strategies make the right decisions to be environmentally friendly and reduce carbon emissions. In some reinforced concrete (RC) elements, fiber-reinforced polymer (FRP) bars have been proposed as an alternative to conventional steel bars. The demand for using noncorrosive and/or nonmetallic reinforcing bars in various reinforced concrete projects has increased. Although these concrete elements are lightweight, have a long lifespan, and need little maintenance, their non-ductile nature and bond with the surrounding concrete create significant challenges. Several experimental investigations have been conducted to evaluate the behavior of RC elements, even with their high cost. This study aims to assess numerically the viability of using FRP bars instead of traditional steel ones in simply supported reinforced concrete beams (RCBs) as longitudinal reinforcement (passive reinforcement). Utilizing the three-dimensional (3D) nonlinear finite element analysis (FEA) software (ABAQUS), a total of eighteen models were carried out to validate the results available in reference case studies with FRP bars. The verification of the numerical results has been verified by comparing them with the reference experimental data. Next, in order to assess the rigidity of such RCBs with FRP bars, parametric research was carried out. The numerical results proved that RCBs with FRP bars have a positive impact on enhancing load-carrying capacities. But on the other hand, the strain energy of such RCBs with CFRP bars is reduced to about 75% of the strain energy of RCBs with steel bars, which leads to low beam ductility.

Mandrel diameter effect on ring-pull testing of nuclear fuel cladding

Inconsistencies in ring-pull testing methods for thin-walled tubes make it difficult to compare a material's mechanical properties in the hoop direction presented in past publications. The effect of test setup, specifically mandrel diameter, was investigated for nuclear fuel cladding tubes of the iron-chromium-aluminium (FeCrAl) alloy, C26M (Fe-12Cr-6Al-2Mo). Mandrel diameter for ring-pull testing can change how the ring deforms and friction effects, further convoluting the results from testing. To address the impact of mandrel size in relation to ring diameter, gaugeless ring-pull samples were tested across a range of mandrel diameters and compared to uniaxial tensile tests from the same tube of material. Two groups of samples were tested: an as-received, low ductility sample set and an annealed, high ductility sample set, both cut from the same extruded tube. By pairing systematic variation of mandrel geometry with analysis of local strain gradients using digital image correlation, this study investigates the effect of test fixture geometry on apparent mechanical properties and effective strain fields and provides guidance for comparing previously published data. Certain features in uniaxial stress-strain curves (namely the yield strength, ultimate tensile strength, and uniform elongation) appeared to have analogies in the effective stress-strain curves from ring-pull testing. These corresponding features are compared to expose biases in the analysis of material properties using gaugeless ring-pull and to provide novel guidance on test setup during experimental design.

Experiments and investigation of planar high-strength steel joints with Additive Manufacturing

This paper investigates the application of high-strength steel in planar steel joints, specifically X-joints and T-joints, which are crucial connecting components in structural engineering, ensuring structural stability in buildings, bridges, and tower cranes. Conventional steel joints, mainly constructed from low-carbon steel, encounter challenges arising from the low ductility of high-strength steel and its strict welding criteria. The Solid Isotropic Material with Penalization (SIMP) method is employed to perform topology optimization on X-joints with different brace width to chord width ratios and T-joints, enabling the manufacturing of high-strength steel components through the Additive Manufacturing method (AM). The impact of different additive manufacturing orientations on material strength is tested, with results indicating improved mechanical properties when the loading direction is perpendicular to the normal direction of the additive manufacturing layer. Compression tests are conducted using 2D/3D Digital Image Correlation methods (2D/3D-DIC) alongside traditional measurement techniques. The results indicate that the stress distribution of the optimized joint is more rational, and the strength of the optimized joint has improved compared to the tubular joint. The optimized joint exhibits a more distinct load path and apparent failure mode. This optimized joint enables a uniform stress redistribution, enhancing ductility and achieving a strong-joint and weak-component structural mechanism that satisfies the serviceability limit state (SLS). In comparison to non-penetrative tubular joints, no significant cracks are observed under identical loading conditions.

On the fatigue behaviour of epoxy-based nanostructured composite materials

Epoxy composites and nanocomposites enable the creation of high-performance structures and innovative designs. However, there is limited research focused on their fatigue characterization. The purpose of this study is to analyze the fatigue resistance results of nanostructured composite materials made with an epoxy matrix of Diglycidyl Ether of Bisphenol F and 9,9-bis(3-chloro-4-aminophenyl) fluorine (DGEBF-CAF) reinforced with 5%wt of elastomeric nanoparticles with an average diameter of 200 nm. The tests are conducted at variable load and frequency using Rotating Bending (R-B) and Tensile-Tensile (T-T) tests, and the results are compared to those obtained with pure resin. The occurrence of thermal fatigue phenomena during the tests is monitored using a thermal camera. The results confirm that pure epoxy resin exhibits poor crack propagation resistance due to its low ductility and toughness, and the introduction of a second phase leads to an improvement of approximately 3 times in T-T tests and 5 times in R-B tests.

Effects of cutting conditions on materials properties of austenitic stainless steels

Austenitic stainless steel SUS304 is widely used in various engineering applications, including semiconductor manufacturing equipment and food processing machinery, owing to its exceptional material characteristics such as non-magnetic properties, high corrosion resistance, strength, and ductility. However, concerns have arisen in recent years regarding potential alterations in the material properties of austenitic stainless steel after machining processes. As the cutting process was conducted widely to make various engineering applications with different machining conditions, an examination of the effect of machining conditions on the material properties is important. In the present study, the influence of cutting conditions on the microstructure and mechanical of SUS304 was experimentally and numerically investigated, where three types of ball-end mills with rake angles (- 20°, − 3°, and 5°) and different cutting speeds (50 m･min−1 and 100 m･min−1) were conducted with plane and side machining to investigate the cutting properties. Material properties of SUS304 can be changed by the cutting resistance of the above cutting process, in particular the low rake angles under plane machining, where the high cutting resistance makes high dislocation density and strain-induced martensite formation. This occurrence made the low corrosion resistance as well as low ductility. On the contrary, no significant effect of the cutting speeds on the cutting resistance was detected compared to the condition of the rake angle on the plane machining. The reasons behind this will be discussed in detail systematically in this paper. From this approach, it could be clarified to maintain the high material properties of SUS304 even after the cutting process, which could be useful to make design of the engineering applications.