Low Ductility Research Articles

Effects of cutting conditions on materials properties of austenitic stainless steels

Austenitic stainless steel SUS304 is widely used in various engineering applications, including semiconductor manufacturing equipment and food processing machinery, owing to its exceptional material characteristics such as non-magnetic properties, high corrosion resistance, strength, and ductility. However, concerns have arisen in recent years regarding potential alterations in the material properties of austenitic stainless steel after machining processes. As the cutting process was conducted widely to make various engineering applications with different machining conditions, an examination of the effect of machining conditions on the material properties is important. In the present study, the influence of cutting conditions on the microstructure and mechanical of SUS304 was experimentally and numerically investigated, where three types of ball-end mills with rake angles (- 20°, − 3°, and 5°) and different cutting speeds (50 m･min−1 and 100 m･min−1) were conducted with plane and side machining to investigate the cutting properties. Material properties of SUS304 can be changed by the cutting resistance of the above cutting process, in particular the low rake angles under plane machining, where the high cutting resistance makes high dislocation density and strain-induced martensite formation. This occurrence made the low corrosion resistance as well as low ductility. On the contrary, no significant effect of the cutting speeds on the cutting resistance was detected compared to the condition of the rake angle on the plane machining. The reasons behind this will be discussed in detail systematically in this paper. From this approach, it could be clarified to maintain the high material properties of SUS304 even after the cutting process, which could be useful to make design of the engineering applications.

Enhanced strength and ductility of laser-directed energy deposition repaired IN718 superalloy via a novel tailored heat treatment

High-quality repair of damaged Inconel 718 (IN718) superalloy components can achieve great economic benefits. However, the directly double aging (DA) treatment by industrial standards, yields an inferior ductility on the repaired component than that of the wrought base metal. In this work, wrought IN718 components were repaired by laser-directed energy deposition (LDED), a novel tailored heat treatment (THT) schedule consisting of a short-term low-temperature homogenization, and subsequent DA was subsequently conducted to strengthen the repaired IN718 alloys. The microstructure evolution and mechanical properties of the DA and THT-treated repaired alloys were comparatively investigated. The results indicated that the THT effectively dissolved most of the hard brittle Laves precipitates in the deposition region with only slight coarsening of the grains in the substrate. As compared to the DA sample, the elongation of the THT sample increased remarkably by 88% with only a slight reduction of 19.2 MPa in yield stress. Moreover, the strain distribution of the THT sample was overall more even but then destabilized in a narrow abnormal coarsened grain region caused by the static recrystallization. In general, this study breaks through the limitation of the low ductility of the DA-treated repaired IN718 alloys and provides a promising way to further improve the mechanical properties.

Construction of fluorinated hyperbranched polyaryletherketone-based UV-cured films with low dielectric and enhanced mechanical properties

The incorporation of hyperbranched structure into the polyaryletherketone (PAEK) is a crucial method for achieving a low dielectric constant (Dk), and the inclusion of crosslinked structure effectively reduces the dielectric loss (Df). This approach is of great significance in the development of high-quality communication at high frequencies. However, it is still a significant challenge for maintaining its mechanical properties and reducing Dk and Df due to the poor film-forming properties and low ductility of hyperbranched polymers. In this study, we synthesized a novel acrylate-based fluorinated hyperbranched photosensitive polyaryletherketone (hb-P6FAEK-Ace) as a prepolymer with various bifunctional aliphatic active and 4-acryloyl morpholine as the reactive solvent. Upon UV irradiation, cured films were obtained. This method significantly improved the mechanical properties of the hyperbranched UV-cured resin, with the tensile strength of CF-DCDDA of 83.2 MPa and the elongation at break of 7.61%. Additionally, the five prepared photosensitive resins exhibited excellent rheological properties (from 71.6 mPa s to 134.7 mPa s at 100 °C), rapid curing rates (within tens of seconds), and minimal volume shrinkage (<7%). Meanwhile, the Dk of CF-DCDDA was measured to be 2.87, with a Df of 0.0126 at the frequency of 20 GHz. This low dielectric expression for the crosslinked cured films could be ascribed to the confinement of electronic polarization caused by the crosslinked and hyperbranched structures. This work provides a simple, green, and promising strategy for enhancing the dielectric and mechanical properties of hb-PAEK.

Functional Grading Between Soft-Magnetic Fe-Co/Fe-Ni Alloys and the Effect on Magnetic and Microstructural Properties.

Producing soft magnetic alloys by additive manufacturing has the potential to overcome cracking and brittle fracture issues associated with conventional thermomechanical processing. Fe-Co alloys exhibit high magnetic saturation but low ductility that makes them difficult to process by commercial methods. Ni-Fe alloys have good ductility and high permeability in comparison to Fe-Co, but they suffer from low magnetic saturation. Functional grading between Fe-Co and Ni-Fe alloys through blown powder directed energy deposition can produce soft magnetic materials that combine and enhance properties beyond the strengths of the individual magnetic materials. This work focuses on the microstructure, crystal structure, and magnetic properties of functionally graded Fe49Co49V2/Ni80Fe16Mo4 coupons. The grading between the two materials is found to refine the microstructure, thereby improving the mechanical hardness without the use of a nonmagnetic element. Postbuild thermal treatments are found to recrystallize the microstructure and increase the grain size, leading to improved magnetic properties. Analysis of crystal structures provides an understanding of the solubility limits and phase equilibria between the BCC (Fe-Co) and FCC (Ni-Fe) structures. Success in functional grading of soft magnets may provide a pathway toward improving energy conversion efficiency through strategic combinations of high saturation and high strength materials.

Numerical Investigation on Precipitation Hardening of Mg-Gd Alloys.

The second-phase particles in magnesium alloys could affect the mechanical properties of the material significantly. In this work, 3D finite element models with explicit incorporation of second-phase particles are established. The simulations are calibrated with the experimental results of the Mg-1Gd alloy. The influences of factors, such as the particle distribution, size, and orientation of cylindrical particles, on precipitation hardening are investigated in detail. Three interface conditions between particles and the matrix-perfect bonding and high- and low-strength bonding-are studied at the same time. The interface conditions are shown to exert a stronger influence on precipitation hardening compared to the factors of particle distribution and size. In contrast, the influence of the orientation of cylindrical particles at grain boundaries outweighs the effect of interface property. When second-phase particles are relatively large and all located at grain boundaries, the hardening effect can be improved, and the magnesium alloy shows relatively high flow stress. However, the high hardening effect from the second-phase particles could result in high local stress concentration and possible early failure or low ductility of Mg alloys.

Damage evolution and failure mechanism of masonry walls under in-plane cyclic loading

Masonry structures often exhibit poor seismic performance during earthquakes owing to their low material strength, structural integrity, and ductility. To address the mechanism of in-plane damage and collapse of masonry walls subjected to earthquake ground motion, three full-size brick walls, one with structural columns and two without structural columns, were designed and constructed in this experimental study to quantitatively investigate the effect of structural columns on the seismic performance of masonry walls. Quasi-static tests of masonry walls subjected to cyclic lateral loading were conducted using electrohydraulic servo actuators. The in-plane damage evolution and failure mode of the masonry walls under lateral loading were investigated. A numerical model with a novel plastic damage constitutive model of masonry was established. The accuracy of this model and the calculation results were verified by comparing them with the crack development and mechanical property curves obtained from the experiments. Based on the numerical model, a parametric analysis was conducted to investigate the influence of critical factors, such as mortar strength, vertical load, and height-to-width ratio, on the seismic performance of masonry structures. The test results showed that structural columns can effectively improve the performance of masonry structures. Properly installed structural columns can improve the peak load-bearing capacity, ductility, and energy dissipation of masonry structures. The masonry damage constitutive model used in this study could simulate the damage to masonry wall specimens well and reflect the hysteretic curves of the specimens within an acceptable range of accuracy. Thus, it provides a valuable reference for physical experiments. An appropriate mortar strength and vertical compressive stress can effectively enhance the load-bearing capacity of masonry structures within a certain range. For structural column walls. Walls with mortar strengths (average compressive strength) of 12.5 MPa, 10 MPa, 7.5 MPa, and 5 MPa showed an increase in peak bearing capacity of 26.2 %, 23.9 %, 18.5 %, and 9.4 %, respectively, compared to walls with mortar strengths (average compressive strength) of 2.5 Mpa. The aspect ratio had a significant impact on the shear load-bearing capacity of the masonry walls. An increase in the aspect ratio led to a transition from shear failure to flexural failure and a subsequent decrease in shear load-bearing capacity. For masonry walls with structural columns, increasing the diameter of the longitudinal steel in the structural columns can enhance the load-bearing capacity of the masonry wall, resulting in a significant improvement in its overall performance.

Flexible biopolymer-assisted 3D printed bioceramics scaffold with high shape adaptability

Bioceramics are widely used in bone tissue engineering, yet the inherent high brittleness and low ductility of the ceramics lead to poor machinability, which restricts their clinical applications. Here, a flexible and processable 3D printed bioceramic scaffold with high ceramic content (66.7 %) and shape fidelity (volume shrinkage rate < 5 %) was developed by freeze-thaw cycles, which was assisted by polyvinyl alcohol (PVA) and silk fibroin (SF). The hydrogen bonding between PVA imparted printability to the ceramic ink and enabled the subsequent formation of flexible scaffolds, which can be twisted, bend and cut to match bone defects. After adding SF, the printability of the inks and hydrophilicity of the scaffolds were enhanced, owing to the interactions between PVA and SF. Further, combined with the formation of β-sheet in SF, the scaffolds exhibited superior mechanical strength and excellent thermal stability, and can fully recover at 35 % compressive strain, which was breaking through the brittleness bottleneck of conventional ceramic scaffolds. Moreover, in vitro experiments showed excellent mineralization ability, osteogenic and angiogenic activities of the scaffolds, demonstrating its potential in bone regeneration. This initial study offers a promising personalized material for bone repair that can be used rapidly during surgery.

Damage assessment of concrete beams repaired with basalt fiber-reinforced polymer sheets through digital image correlation and acoustic emission

Basalt fiber-reinforced polymer (BFRP) has high mechanical strengths as a repairing material but exhibits low ductility. This paper investigates the damage process of reinforced concrete beams repaired using BFRP sheets, aimed at understanding the underlying mechanisms of achieving structural ductility when BFRP sheets are used. The damage process was assessed using digital image correlation (DIC) and acoustic emission (AE) techniques applied to monitor surface and internal damages of three full-scale concrete beams subjected to four-point bending. A beam was first loaded to crack, then repaired with BFRP sheets, and finally reloaded to failure. Surface strain fields and cracks were monitored using a DIC method, and cracking events were monitored using AE sensors deployed at different positions of the beams. The AE signals were analyzed to assess the damage process. The test results indicated that (1) tensile cracks predominated throughout the loading process; (2) the BFRP sheets hindered the widening of cracks and promoted the generation of fine cracks; and (3) the development of concrete cracks promoted interfacial debonding at steel-concrete and BFRP-concrete interfaces. A combination of different types of cracks and interfacial debonding helped the repaired beam achieve ductile flexural behaviors.

A low-cost Mg–Al–Mn–Zn alloy for automotive road wheel applications

In this study, a new Mg–Al–Mn–Zn alloy (AMZ211) was designed, aided by thermodynamic modeling, for applications in automotive road wheels using forging and flow-forming processes. The AMZ211 alloy was cast and forged in an industrial scale to obtain a forged blank to evaluate its tensile properties and hot formability under high-strain-rates (simulating flow-forming conditions). Multiple characterization techniques, including optical, scanning electron and scanning transmission electron microscopy as well as electron backscatter diffraction, were applied to investigate the microstructural evolution during the processing route. As expected from the alloy design, nano-sized Mn-containing dispersoids formed in a homogeneous manner during homogenization heat treatment, contributing to the formation of refined dynamically recrystallized (DRXed) grains in as-forged microstructure. The as-forged AMZ211 alloy showed better hot formability than as-forged AZ80 Mg alloy under high-strain-rate condition as well as a comparable strength property in relative to the benchmark and more expensive Mg–Zn–Zr alloys. The lower ductility of as-forged AMZ211 alloy may be due to the high twinning tendency of coarse unDRXed domains which were formed as a result of the original coarse-grained microstructure from solidification. The present study provides a low-cost Mg alloy for high-volume automotive road wheel applications.

Influence of Ni and PWHT on microstructure evolution and mechanical properties of GTA-welded duplex stainless steel and super duplex stainless steel joints: A comparative investigation

In the present investigation, a new endeavor has been made to analyze the impact of the secondary process (post-weld heat treatment (PWHT)) as well as Ni addition on the microstructure and mechanical characteristics of welds. Welds between similar joining materials from duplex stainless steels (DSS), as well as super DSS (SDSS), were made by the gas tungsten arc welding (GTAW) process. For DSS, after PWHT with the addition of Ni element, the amount of austenite rises and becomes more uniformly distributed with curved boundaries, while for SDSS, the microstructure mainly consists of intergranular and Widmanstätten austenite. According to the comparison of phase percentages obtained based on both ASTM E1245 and ASTM E562, a good balance between ferrite and austenite phases of joint materials was achieved. X-ray diffraction analyses on both joints revealed that phases are mainly ferrite and austenite with different lattice parameters without evidence of unwanted intermetallic phases. The addition of Ni increases the hardness values of DSS weld metal compared to the base metal due to an increased amount of Widmanstätten austenite and ferrite in the microstructure. The lowest ductility was obtained for the SDSS weld sample with the addition of Ni and PWHT because of the existence of secondary austenite in the weld metal and the Widmanstätten morphology of the austenite. The effect of PWHT on the development of microstructure and mechanical behaviors was more than the effect of nickel powder on weld samples.

Evaluation of Microstructure and Mechanical Properties of TiAl/HI-TEMP 820/ SCM440H Materials Manufactured through Vacuum Brazing according to Process Temperature

The TiAl alloy is attracting attention as a lightweight and heat-resistant material, because of its high specific strength, excellent high-temperature formability, and fatigue strength. However, its applications are limited by its high unit price and low room temperature ductility. To overcome this issue, dissimilarly bonded materials have been extensively employed. This involves joining a brittle metal to a low-cost metal that possesses excellent plasticity, using various dissimilar bonding techniques. In this study, TiAl/HI-TEMP 820/SCM440H materials were fabricated using a vacuum brazing process under different temperature conditions. After the brazing process, the microstructure of the interfacial area revealed seven distinct layers resulting from chemical reactions between the base metals and the filler metal. These reaction layers consisted of a Ni solid solution, intermetallic compounds (Ti&lt;sub&gt;3&lt;/sub&gt;Al, TiNi&lt;sub&gt;2&lt;/sub&gt;Al, Ti&lt;sub&gt;2&lt;/sub&gt;Ni, FeNi), and borides (CrB, TiB&lt;sub&gt;2&lt;/sub&gt;, FeB). To analyze the effect of brazing temperature on the relationship between the microstructure and mechanical properties at the interface of TiAl/HI-TEMP 820/SCM440H materials, conventional uniaxial tests and nanoindentation tests were performed. The measured nanohardness exhibited a significantly large distribution for each reaction layer, with the highest hardness values observed in the intermetallic compounds and borides layers. Additionally, room temperature tensile tests confirmed that fractures initiated in the highhardness and brittle intermetallic compounds and borides layers.

Effect of sodium gluconate addition on anomalous codeposition of electroplated nickel-iron alloys

Invar nickel-iron alloy has been widely applied in the fields of electronics, sensors, communications and optics, due to its low thermal expansion coefficient, high hardness, high ductility and other characteristics according to product requirements. The application in metal stencil during the manufacturing process of active-matrix organic light-emitting diodes is mainly due to their good electrical conductivity and soft magnetic properties. In this study, sodium gluconate is used as a substitute for boric acid in the acidic electroplating of nickel-iron alloys; the concentration ratio of nickel-iron in the plating bath is 2:1. After adding sodium gluconate, the precipitation of nickel varies significantly. The iron content in the weight percentage of the deposited nickel-iron alloy is obviously larger than nickel, even up to 3 times. The whole deposition process is in the state of anomalous codeposition, and the selectivity ratio reaches 3 or more; the nickel-iron alloy deposited by adding sodium gluconate to the plating bath has a great influence on the material properties of the nickel-iron alloy plating, The nickel-iron alloy deposited at -1.4 V exhibits a hardness of approximately 3.17 GPa and a modulus of elasticity about 37.88 GPa. Notably, the resistance to plastic deformation of the alloy deposited in sodium gluconate plating solution (H3/U2=0.022) is significantly higher than that in boric acid plating solution (H3/U2=0.007). The experimental results also show that it has the best ability to resist plastic deformation.

Sensitivity of reduction rate on the mechanical response of boron-doped Fe50Mn30Co10Cr10 high entropy alloy

Phase transformation induced plasticity (TRIP) effect is an effective technical solution to enhance the strength and ductility of alloys, represented by Fe50Mn30Co10Cr10 high entropy alloy (HEA). Introducing heterostructures into alloys is also an effective synergistic method for enhancing the strength and ductility of alloys. Combining element doping, heterostructures, and the TRIP effect of the alloy itself can enable the alloy to achieve both high strength and high ductility. In this work, the boron doped Fe50Mn30Co10Cr10 HEA were prepared by cold rolling with different reduction rates followed by recrystallization annealing processes. Different reduction rates result in different heterogeneous structures. The large rolling reduction weakens the advantage of heterogeneous structure for introducing large stress concentration, resulting in the low ductility of the alloy. The sample with small rolling reduction shows excellent strength and ductility, which comes from the synergistic effect of large-small grains matching and TRIP effect. In summary, the TRIP effect combined with the appropriate amount of reduction and low recrystallization temperature annealing induced heterostructure is an effective solution to overcome the strength ductility trade-off.

Role of loading direction on high-temperature tensile behavior of Fe-13Cr-4Al-2Mo-0.65Nb alloy

The Fe-13Cr-4Al-2Mo-0.65Nb alloy is being considered as a promising accident-tolerant cladding fuel material for light water reactors design. The present work investigated the mechanical properties and serration behavior of the hot-rolled FeCrAl alloy in the rolling direction (RD) and transverse direction (TD) under various temperatures. The presence of the high-density dislocation bands parallel to RD and the smaller grain size in TD are recognized as leading causes of the lower ductility of the TD specimens. Additionally, both RD and TD specimens show identical serrated flow behaviors at each temperature, suggesting the serration behavior is independent of the loading direction.

Balance of strength and ductility for laser directed energy deposited Ta-containing Ti6Al4V via solution and aging treatment

The tensile properties of laser directed energy deposited (LDEDed) titanium (Ti) alloys are usually characterized by high strength and low ductility, which seriously limits their wide application prospects. In this study, a novel Ti6Al4V4Ta alloy is prepared using LDED technique and achieved excellent strength (UTS ∼ 990 MPa) and ductility (elongation ∼ 16%) through solution treatment at 930 °C and aging at 550 °C. The high strength is mainly attributed to the ultrafine micron-scale α s while the good ductility results from equiaxed α p, the increased β phase and weakened α-variant selection. The combination of appropriate elemental alloying and heat treatments could provide some guidance for LDED Ti alloys of good mechanical performance with potentials for wider applications.

NONLINEAR SIMULATIONS TO EVALUATE THE CODE-BASED RESPONSE MODIFICATION FACTOR FOR SEISMIC DESIGN OF SLAB-ON-PILE STRUCTURE

Slab on Pile (SOP) structure using concrete spun pile (CSP) is frequently constructed for highway or railway infrastructures in Indonesia. However, some previous studies showed that spun piles have low energy dissipation and ductility. Therefore, spun pile application as bridge piers, particularly in high seismic locations such as Indonesia, needs additional consideration. The response modification factor (R) in the SOP elastic seismic design needs to be carefully considered since this parameter reflects the ability of the structure to dissipate energy through inelastic behavior. The work discussed in this paper primarily concerns the evaluation of the R-value based on the Indonesia seismic bridge design code, SNI 2833-2016, which is applied to SOP seismic design. The study provided an alternative reference for engineers in the seismic design of a SOP structure. Preliminary elastic design of SOP structures demonstrated that the number of piles and structural flexibility is significantly affected by the R-values consideration. In addition, the pinching hysteresis captured from the nonlinear dynamic analysis results emphasized the limited capability of an SOP structure in dissipating energy under seismic excitation. Moreover, the spun pile concrete material, especially in the pile-to-pile head connection, was observed to have an earlier failure. This study strongly suggested using an R-value of 1.5 to achieve a high seismic performance SOP structure with little need for aftershock retrofitting, even though this would necessitate much more spun piles. However, some further research could be conducted to develop the high seismic performance but economical design of SOP structures.

In-situ observation of deformation-induced grain reorientation in 718 Ni alloy microlattices

Microlattices pose ample opportunity for constructing light weight structures for the automotive and aerospace industries. Laser powder bed fusion is an appealing technique to fabricate these structures because of its capabilities to process high-resolution complex architectured structures. In this work we explore the use of a 718 oxide dispersion strengthened alloy to create three microlattice structures designed in nTop, a straight bar, honeycomb and body-centered cubic (BCC) microlattice and investigate the effects of architectures on tensile behavior of the microlattices in a scanning electron microscope. The straight bar configurations deliver high strength but low ductility. The BCC lattices are highly deformable but soft. The honeycomb has an attractive combination of high strength and pronounced work hardening. Furthermore, electron backscattered diffraction studies revealed substantial crystallographic reorientation and grain refinement in the honeycomb lattice during deformation, in contrast to little crystal orientation change in the straight bar specimens. This study suggests that architectures play a significant role in the tensile behavior and deformation mechanisms in metallic materials.

In-situ additive manufacturing of high strength yet ductility titanium composites with gradient layered structure using N2

It has always been challenging work to reconcile the contradiction between the strength and plasticity of titanium materials. Laser powder bed fusion (LPBF) is a convenient method to fabricate innovative composites including those inspired by gradient layered materials. In this work, we used LPBF to selectively prepare TiN/Ti gradient layered structure (GLSTi) composites by using different N2–Ar ratios during the LPBF process. We systematically investigated the mechanisms of in-situ synthesis TiN, high strength and ductility of GLSTi composites using microscopic analysis, TEM characterization, and tensile testing with digital image correlation. Besides, a digital correspondence was established between the N2 concentration and the volume fraction of LPBF in-situ synthesized TiN. Our results show that the GLSTi composites exhibit superior mechanical properties compared to pure titanium fabricated by LPBF under pure Ar. Specifically, the tensile strength of GLSTi was more than 1.5 times higher than that of LPBF-formed pure titanium, reaching up to 1100 MPa, while maintaining a high elongation at fracture of 17%. GLSTi breaks the bottleneck of high strength but low ductility exhibited by conventional nanoceramic particle-strengthened titanium matrix composites, and the hetero-deformation induced strengthening effect formed by the TiN/Ti layered structure explained its strength-plasticity balanced principle. The microhardness exhibits a jagged variation of the relatively low hardness of 245 HV0.2 for the pure titanium layer and a high hardness of 408 HV0.2 for the N2 in-situ synthesis layer. Our study provides a new concept for the structure-performance digital customization of 3D-printed Ti-based composites.

A study on the fracture pattern change of high-burnup fuel cladding failed by pellet-cladding mechanical interaction failure under reactivity-initiated accident conditions

ABSTRACT In a part of the historical reactivity-initiated accident (RIA) simulated tests on high-burnup fuels performed at the Nuclear Safety Research Reactor, the fuel failure caused by pellet-cladding mechanical interaction (PCMI) led to splitting into upper- and lower-part pieces or even fragmentation of the cladding tube. A massive release of fuel fragments accompanied this fracture pattern change from previously known axial cracks and thus identified as a potential concern in safety evaluation regarding core coolability. Dedicated out-of-pile mechanical tests were performed with unirradiated Zircaloy-4 cladding specimens to clarify the condition of such fracture pattern change. The specimens were pre-hydrided and subjected to loading with axial-to-hoop strain ratios of ℇz/ℇθ = 0.5–1.25, simulating the effects of hydrogen embrittlement and pellet-cladding mechanical bonding of high-burnup fuels, respectively. The results indicate that higher biaxiality of the loading and lower ductility (failure strain level) assist the fracture pattern change. This study proposes a conservative criterion that a PCMI failure splits the cladding tube into more than two pieces when strain ratio ℇz/ℇθ >0.75 and a concurrent hoop strain < 1.7% at the failure instant.

Microscopic Investigation for Experimental Study on Transverse Cracking of Ti-Nb Containing Micro-Alloyed Steels.

The influence of Ti on the behavior of hot ductility was examined in four different Ti-containing micro-alloyed steels with a constant content of Nb. Thermomechanical investigations using a dilatometer were carried out to simulate the conditions during casting and cooling in the strand of a continuous caster with temperatures in the range of 650-1100 °C, strain rates of 0.01 s-1 and 0.001 s-1, and reheating rates between 60 and 180 Kmin-1. To understand the fracture mechanism, optical (LOM) and scanning electron microscopy (SEM), elemental analysis via energy dispersive X-ray spectroscopy (EDX), MatCalc "Scheil-Guilliver" calculations, and precipitation kinetics calculations were carried out for the critical conditions, showing low hot ductility between Ar3 and Ae3 temperatures and a brittle to ductile transition temperature at 900 °C. The existence of TiNb(CN), thin ferrite formation, and grain boundary sliding (GBs) due to limited dynamic recrystallization (DRX) has been documented and discussed. As a result, the reheating rate has no sufficient effect on the ductility. The existence of Nb-rich TiNb(CN) of sizes below ~1 μm triggers brittle fracture by increasing the frequency of micro-voids around grain boundaries. It can be stated that if the conditions in the hot ductility trough are avoided, the addition of Ti and high strain support minimize the risk of crack formation.