High Temperature Tensile Tests Research Articles

Bending and Straightening of a Medium Carbon Steel Continuous Casting Slab with Low Temperature End Plastic Groove.

The high temperature brittleness range of medium carbon microalloyed steel under an actual continuous casting process was determined by the high temperature tensile test. The test results revealed that only a third of the brittle temperature range from 650–825 °C was due to intergranular ferrite in the experimental steel. In addition, it was found that the plastic recovery was fast and stable when the temperature was lower than 725 °C (the lowest plastic temperature). Bending/straightening operation in this temperature range was conducive to controlling the generation of corner cracks. In order to keep the corner temperature at the low temperature end of the plastic curve when the slab was bent/straightened, the cooling water scheme of the secondary cooling zone of the continuous caster was formulated by numerical calculation. By appropriately increasing the cooling water flow in the foot roll and the secondary cooling zones 1–5, the corner temperature of slab during bending operation was 600–700 °C, avoiding the brittle temperature range. The industrial test was then carried out. The results showed that after using the optimized water volume, the corner grains of the slab were uniform and the microstructure was mainly pearlite + ferrite. In addition, the abnormally large grain size was reduced, and a large amount of ferrite was generated inside the grain, which avoided stress concentration at the corner of the slab during bending/straightening operation, and basically eliminated the corner crack of the slab.

Experimental study on high-temperature relaxation behavior of carbon fiber reinforced polymer cable

In order to fully investigate the relaxation behavior of carbon fiber reinforced polymer (CFRP) cable exposed to high temperature, both steady state-constant displacement and temperature (ST-CDT), and transient state-constant displacement and temperature (TR-CDT) tests were conducted on specimens. The failure modes, stress loss laws and rupture times of high-temperature relaxation specimens were determined under ST-CDT and TR-CDT conditions. After high-temperature relaxation tests, high-temperature tensile tests were conducted on samples without rupture to obtain its residual mechanical properties. Final stress losses and stress loss rates of CFRP cable specimens determined by ST-CDT tests were compared with these of TR-CDT tests to clarify the effect of temperature-load path. A high-temperature relaxation model was developed to characterize the variation law of stress losses for CFRP cables under ST-CDT and TR-CDT conditions. A correlational model between stress loss and creep strain rates in steady stages of CFRP cables under high temperature was calibrated. The obtained results demonstrated that high-temperature stress losses of CFRP cables were closely correlated with target temperature, initial stress level and relaxation duration. The application of initial pre-tension load before heating accelerated the stress loss rate in transition relaxation stage and final stress loss of CFRP cable under high temperature.

Microstructure, residual stress, and mechanical property evolution of a spray-formed vanadium-modified high-speed steel processed by post-heat treatment

A vanadium-modified high-speed steel (HSS) manufactured by spray forming (SF) process was subjected to different heat treatment processes and the resultant microstructural evolution and mechanical properties were investigated. In-situ high-temperature Vickers indentation associated with high-temperature tensile tests were utilized to evaluate the changes in hardness and residual stress with temperature for samples processed by annealing. Moreover, the effect of quenching temperature on hardness, bending strength and impact toughness was investigated. The secondary carbide precipitation behavior and its strengthening mechanisms were discussed in combination with transmission electron microscopy (TEM) characterization. A possible mechanism was proposed to elucidate the evolution of carbide precipitation behavior during different heat treatment processes. We envision the results gained from the present study would provide useful guidance for understanding the evolution of microstructure and mechanical properties of spray-formed HSSs processed by different heat treatment conditions and optimizing the alloy design and post–thermal mechanical processing of HSS.

Hot Deformation and Constitutive Modeling of TC21 Titanium Alloy.

Titanium alloys are extensively employed in the fabrication of various aviation structural parts, of which the most crucial processing step is hot working. In order to study the high-temperature deformation behavior of the TC21 titanium alloy, high-temperature tensile tests were performed. The results reveal that the flow stress of the material gradually decreases with an increased strain rate, and the stress increases rapidly with an increase in strain during the deformation of the alloy. Following this, flow stress gradually decreases. Flow stress decreases sharply, and the sample fractures when the appearance of necking and microvoids is observed. The Arrhenius and Radial basis function (RBF) neural network constitutive models are established in order to accurately describe the high-temperature deformation behavior of the material. In the modified Arrhenius model, strain rate indexes are expressed as a function of deformation temperature and strain rates; furthermore, the high prediction ability of the model was obtained. For the Radial basis function, the network parameters were obtained using the trial-and-error method. The established models could better forecast the flow stress of materials, and highly accurate results are obtained using the radial basis function model. The relationships between the stress index and the deformation activation energy with strain indicate that the primary deformation mechanism involves grain boundary slip and viscous slip of dislocations. The process of dynamic recrystallization primarily promotes the softening of the material.

High Temperature Mechanical Properties and Microstructure Evolution of Ti-6Al-4V Alloy Linear Friction Welding Joints

The combination of linear friction welding (LFW) and hot forming processes is limited due to a lack of research on the high-temperature flow behavior and microstructure evolution of welded joints. In this paper, an electric-assisted high-temperature uniaxial tensile test platform based on digital image correlation (DIC) is built, and uniaxial tensile tests of Ti-6Al-4V alloy with LFW joints are performed at different temperatures (923–1023 K) and different strain rates (0.001 s−1–0.01 s−1). Then the microstructure of the LFW joints under different hot deformation conditions have been analyzed by scanning electron microscope (SEM), electron backscatter diffraction (EBSD) and transmission electron microscopy (TEM). The results indicate that the high-temperature flow behavior of LFW joints shows an obvious correlation between temperature and strain rate: the yield stress decreases from 203 MPa at 923 K to 105 MPa at 1023 K, and increases from 85 MPa to 130 MPa when the strain rate increases from 0.001 s−1 to 0.01 s−1 at 973 K. The hot deformation mechanisms with deformation conditions have been characterized, which changes from the mechanism of dislocation creep to the mechanism of self-diffusion as the deformation temperature increases from 923 to 1023 K. Especially, the fraction of high angle boundaries (HABs) rapidly rise from 49.2% to 64.1% with the increasing temperatures, the discontinuous dynamic recrystallization (DDRX) become the primary mechanism of nucleation during high-temperature deformation of LFW joints.

Room temperature and high temperature micro-forming analysis of SS304 foil

ABSTRACT The micro-sheet metal forming (MSMF) processes such as microstamping and micro-deep drawing can be used to mass-produce miniature parts. However, to design the tools and the processes, material behavior of workpiece under various deformation conditions is required. This paper analyzes the material behavior of 200-µm thickness Stainless steel-304 foil with room-temperature tensile (RTT) tests and high-temperature tensile (HTT) tests. The effect of strain rate and temperature on flow stress behavior, surface roughness, microstructural evolution and fracture mechanism have been examined. It is observed that the percentage elongation for HTT tests is significantly higher than as compared to RTT tests. However, the percentage elongation and the tensile strength during HTT tests are dependent on the strain rate and decreases with a decrease in the strain rate. Recrystallization followed by grain growth in the material took place during high-temperature deformation, thereby changing the surface roughness and fracture mechanism. All the RTT specimens showed ductile failure with characteristic trans-granular dimpled fracture surfaces. The HTT specimens, in contrast, have intergranular fracture by grain pull out due to crack propagation along the grain boundaries. The present analysis can be used to guide the designing of micro-sheet metal forming processes to obtain the required micro-parts.

Microstructure and Mechanical Properties at Elevated Temperature of Powder Metallurgy Al-Zn-Mg-Cu Alloy Subjected to Hot Extrusion

In this work, Al-Zn-Mg-Cu powders containing 0.15 and 0.33 wt % oxygen were utilized to prepare high-strength aluminum alloys through the process of cold isostatic pressing, sintering, hot extrusion, and heat treatment. Microstructural and mechanical properties at elevated temperatures of 250, 350, and 450 °C were investigated by scanning electron microscopy (SEM), electron backscatter diffraction (EBSD), transmission electron microscopy (TEM), and high-temperature tensile tests. Results showed that the tensile strengths of the obtained Al-Zn-Mg-Cu alloys with 0.15 wt % oxygen were 185, 46, and 18 MPa at 250, 350, and 450 °C, respectively. When the oxygen content of Al-Zn-Mg-Cu alloy rose to 0.33 wt %, the tensile strengths at the corresponding temperature reached up to 205, 68, and 25 MPa, respectively. The excellent high-temperature performance could be attributed to double hindrance to dislocation motion and grain boundary migration by a large amount of nano γ-Al2O3 created by the in-creased oxygen, thereby resulting in fine grains even at high temperatures.

Strengthening mechanism and effect of Al2O3 particle on high-temperature tensile properties and microstructure evolution of W–Al2O3 alloys

The W–Al2O3 alloy rods were successfully fabricated by the powder metallurgy process and hot swaging. Subsequently, the high-temperature tensile tests were conducted to characterize the mechanical properties of the W–Al2O3 alloy. At 800 °C, the ultimate tensile strength of W-0.25 wt% Al2O3 alloy is 611.1 MPa, which is 18% higher than that of pure W. After tension, the microstructure evolution was evaluated using metallographic microscope and transmission electron microscopy. For the pure W undergoing deformation at 1000 °C, dynamic recrystallization occurs, leading to the sharp decrease of the strength. However, the microstructure of the W-0.25 wt% Al2O3 alloy contains a large number of sub-grain and low-angle grain boundaries, which does not significantly change in the temperature range of 800–1200 oC, and the work hardening plays a leading role during the high-temperature deformation process. Due to high hardness, the dispersed Al2O3 particles effectively prevent the dislocation movement, displaying a significant strengthening effect.

Elevated temperature tensile properties of an extruded aluminium alloy reinforced with SiCp

Abstract Elevated temperature tensile properties of AlSi7Mg (Al-7 %Si– 0.7 %Mg) and its composites with 10 and 20 vol.% SiCp in the as-extruded form were investigated. The cast ingots of the matrix alloy and the composites were produced by the permanent die casting technique and extruded at 480 °C using an extrusion ratio of 10 : 1. The high-temperature tensile tests were carried out over the temperature range from 25 to 430 °C. Mechanical properties after extrusion show that the composite samples have strength values superior to that of the matrix alloy at ambient temperature. At elevated temperatures the results indicate that the composites exhibit good strength retention up to 300 °C, above which the strengthening effect of SiCp disappears as the temperature is increased. The strain rate sensitivity “m” was observed to be 0.11 for the matrix alloy, 0.13 and 0.07 for the composites with 10 and 20 vol.% SiCp, respectively, at a test temperature of 430 °C in the strain rate range from 4 × 10 –5 to 4 × 10– 2 s– 1.

Influence of Zr on grain orientation, texture, and mechanical properties in hot- and warm-rolled FeCrAl alloys

Iron–chromium–aluminum (Fe–Cr–Al) alloys have great potential application as an accident-tolerant fuel cladding material in light-water reactors. It has excellent processing ability, resistance to steam oxidation at high temperatures (HTs), and irradiation swelling-resistance. It is necessary to improve the room- and high-temperature mechanical properties and reveal the strengthening mechanism. In this study, we analyzed the effect of Zr on the microstructure and room- and high-temperature tensile properties of hot- and warm-rolled FeCrAl alloys. The results show that the Laves phase could be effectively stabilized by Zr addition, and the proportion of low-angle grain boundaries increased. Moreover, the yield strength at room and high temperatures of the samples after Zr addition were improved, owing to the precipitation and sub-grain boundary strengthening by Zr. In addition, Zr changed the grain orientation, but had no relevance to the number of easier activated slip systems. The movable dislocation cannot slip during high-temperature tensile tests because of the pinning effect of the dynamic precipitated Laves phase, which could be the reason for the decrease in elongation at high temperatures. • Zr addition stabilized the Laves phase effectively in Fe–Cr–Al alloys. • Zr addition increased the proportion of LAGBs in hot and warm rolled Fe–Cr–Al alloys. • Zr addition did not influence the number soft orientation grains in Fe–Cr–Al alloys. • The elongation of Fe–Cr–Al alloys decreased at the high temperature tensile tests.

Evolution of Iron-Rich Intermetallics and its Effect on the Mechanical Properties of Al-Cu-Mn-Fe-Si Alloys after Thermal Exposure and High-Temperature Tensile Testing

Evolution of Iron-Rich Intermetallics and its Effect on the Mechanical Properties of Al-Cu-Mn-Fe-Si Alloys after Thermal Exposure and High-Temperature Tensile Testing

Study on mechanical behavior and microstructure evolution of Al-Mg-Li alloy during electropulsing assisted uniaxial tensile

The mechanical behavior and microstructure evolution of Al-Mg-Li alloys under the effect of electric current was investigated using an electropulsing-assisted uniaxial tensile (EAUT) test combined with microstructure observations. It was found that the localized Joule heating-induced microscale high temperature at the grain boundaries in the necking zone significantly accelerated the grain boundary weakening when necking occurred, which resulted in rapid intergranular fracture and relevant decrease in elongation. Electropulsing induced continuous dynamic recrystallization (CDRX) in the both side layers and the discontinuous dynamic recrystallization (DDRX) in the intermediate layers of the Al-Mg-Li sheet during EAUT testing at 460 °C and higher, promoting the formation of newly near-equiaxed recrystallized grains and weakening of β-fiber texture components. For the conventional high temperature tensile test, only a small amount of recrystallized grains formed along the grain boundaries of the coarse parent grains under the control of DDRX. The occurrence of CDRX during EAUT was substantially attributed to the promoted effect of electropulsing on dislocation glide and climb, which resulted from the combined effect of microscale localized Joule heating around dislocations and the electro-induced enhancement effect on vacancy diffusion.

Hot Deformation Behavior and Strain Rate Sensitivity of 33MnCrB5 Boron Steel Using Material Constitutive Equations

In this paper, the constitutive equation parameters (Johnson–Cook parameters) of the 33MnCrB5 material were determined with the help of tensile tests. Initially, Johnson–Cook (JC) model was used for performing the simulations of the sample with finite element analysis with the help of ANSYS software. For these operations, the sample was first used at a certain temperature (24 °C) and low strain rates (10−1, 10−2, 10−3 s−1) and quasi-static tensile tests were performed. Then, high temperature tensile tests were performed with strain rate values of 10−3 s−1 at temperatures of 300 °C, 600 °C, and 900 °C, respectively. Finally, JC parameters belonging to test materials were found in accordance with the results obtained from the high temperature tensile and quasi-static tests. In the last stage, the results obtained from the simulation software for the yield stress, maximum stress, and elongation values were compared with the experimental results. As a result, deviation values for quasi-static tests are calculated as 5.04% at yield stress, 5.57% at maximum stress, and 5.68% at elongation, while for high temperature, yield stress is 9.42%, maximum stress is 11.49% and the elongation value is 7.63%. The accuracy of JC parameters was verified with the comparison made with the obtained data.

Effects of Stabilizing Heat Treatment on Properties of Simulated Microstructures in the Heat-Affected Zone of 347H Stainless Steel

In this paper, two kinds of heat affected zone (HAZ) simulation structures of 347H stainless steel, which are coarse grain zone (CGZ) and unmixed zone (UZ), were prepared by thermal simulator. The material properties of toughness, reheat crack susceptibility and intergranular corrosion susceptibility of the two kinds of HAZ simulation structures were studied by impact test, high temperature tensile test, electrochemical potentiodynamic reactivation (EPR) test and micro morphology test. The result shows that CGHAZ had better toughness. But after the stabilizing heat treatment, it was weakened while that of the UZ was enhanced. The reheat crack susceptibility of the CGZ and UZ both increases after stabilization heat treatment, and the tendency of the UZ are more obvious. Stabilizing heat treatment has a certain effect on the prevention of sensitization process, which can improve the intergranular corrosion resistance of the material. Stabilizing heat treatment is double-edged to 347H HAZ, and it needs combined with the specific situation to used.

The High-Temperature Tensile Test of Quartz Fiber Fabric- Reinforced Resin Composites

The tensile properties of quartz fiber fabric-reinforced resin composites at high temperature were studied. The effects of specimen type and dimension, temperature loading procedure, holding time and loading rate on the tensile properties of the composites at high temperatures were analyzed through series of comparative experiments, the tensile test parameters were determined. Chinese national standard for high-temperature tensile property testing of the composites was compiled based on the data collected. According to the established standard, the tensile testing at 500°C was carried out. Compared with the tensile properties at room temperature, the tensile strength and tensile modulus of the composite at high temperature decreases significantly, with the tensile strength decreasing by about 42.32% and the tensile modulus decreasing by about 24.18%. This is mainly due to the high temperature which causes part of the resin matrix to pyrolyze and detach from around the fiber, thus losing the integrity of the material. In addition, this national standard for high-temperature tensile properties has some general applicability to different types of fiber-reinforced resin composites.

Numerical and experimental investigations of built orientation dependent Johnson–Cook model for selective laser melting manufactured AlSi10Mg

Powder bed fusion based additive manufacturing techniques involve melting or sintering of powder particles via laser beams to join them in order to attain desired shapes. This study aims to provide basis for material constitutive parameters of widely used aluminum alloy AlSi10Mg alloy. Initially, tensile samples of AlSi10Mg alloy samples were manufactured by using SLM technology. Afterwards, through quasi-static and high temperature tensile tests, an attempt has been made to determine the Johnson–Cook material model of AlSi10Mg. in order to conduct quasi-static tensile tests, strain rates of 10−3 s−1, 10−2 s−1 and 5 × 10−2 s−1 were considered and tests were conducted at ambient temperature. Whereas, for high temperature tensile tests 24, 150, 300 °C temperature values were considered at the reference strain rate value of 10−3 s−1. The numerically simulated tensile results achieved by using the established Johnson–Cook model were then compared with experimental results. It was observed that the maximum error between the test and simulation results was around of 7.5%. The error percentage is well within the acceptable, thus proving the accuracy of the established material model.

Comparison of Mechanical and Microstructural Properties of as-Cast Al-Cu-Mg-Ag Alloys: Room Temperature vs. High Temperature

Unfolding the structure–property linkages between the mechanical performance and microstructural characteristics could be an attractive pathway to develop new single- and polycrystalline Al-based alloys to achieve ambitious high strength and fuel economy goals. A lot of polycrystalline as-cast Al-Cu-Mg-Ag alloy systems fabricated by conventional casting techniques have been reported to date. However, no one has reported a comparison of mechanical and microstructural properties that simultaneously incorporates the effects of both alloy chemistry and mechanical testing environments for the as-cast Al-Cu-Mg-Ag alloy systems. This preliminary prospective paper presents the examined experimental results of two alloys (denoted Alloy 1 and Alloy 2), with constant Cu content of ~3 wt.%, Cu/Mg ratios of 12.60 and 6.30, and a constant Ag of 0.65 wt.%, and correlates the synergistic comparison of mechanical properties at room and elevated temperatures. According to experimental results, the effect of the precipitation state and the mechanical properties showed strong dependence on the composition and testing environments for peak-aged, heat-treated specimens. In the room-temperature mechanical testing scenario, the higher Cu/Mg ratio alloy with Mg content of 0.23 wt.% (Alloy 1) possessed higher ultimate tensile strength when compared to the low Cu/Mg ratio with Mg content of 0.47 wt.% (Alloy 2). From phase constitution analysis, it is inferred that the increase in strength for Alloy 1 under room-temperature tensile testing is mainly ascribable to the small grain size and fine and uniform distribution of θ precipitates, which provided a barrier to slip by deaccelerating the dislocation movement in the room-temperature environment. Meanwhile, Alloy 2 showed significantly less degradation of mechanical strength under high-temperature tensile testing. Indeed, in most cases, low Cu/Mg ratios had a strong influence on the copious precipitation of thermally stable omega phase, which is known to be a major strengthening phase at elevated temperatures in the Al-Cu-Mg-Ag alloying system. Consequently, it is rationally suggested that in the high-temperature testing scenario, the improvement in mechanical and/or thermal stability in the case of the Alloy 2 specimen was mainly due to its compositional design.

Dynamic Softening and Hardening Behavior and the Micro-Mechanism of a TC31 High Temperature Titanium Alloy Sheet within Hot Deformation.

TC31 is a new type of α+β dual phase high temperature titanium alloy, which has a high specific strength and creep resistance at temperatures from 650 °C to 700 °C. It has become one of the competitive candidates for the skin and air inlet components of hypersonic aircraft. However, it is very difficult to obtain the best forming windows for TC31 and to form the corresponding complex thin-walled components. In this paper, high temperature tensile tests were carried out at temperatures ranging from 850 °C to 1000 °C and strain rates ranging from 0.001 s−1 to 0.1 s−1, and the microstructures before and after deformation were characterized by an optical microscope, scanning electron microscope, and electron back-scatter diffraction. The dynamic softening and hardening behaviors and the corresponding micro-mechanisms of a TC31 titanium alloy sheet within hot deformation were systematically studied. The effects of deformation temperature, strain rate, and strain on microstructure evolution were revealed. The results show that the dynamic softening and hardening of the material depended on the deformation temperature and strain rate, and changed dynamically with the strain. Obvious softening occurred during hot tensile deformation at a temperature of 850 °C and a strain rate of 0.001 s−1~0.1 s−1, which was mainly caused by void damage, deformation heat, and dynamic recrystallization. Quasi-steady flowing was observed when it was deformed at a temperature of 950 °C~1000 °C and a strain rate of 0.001 s−1~0.01 s−1 due to the relative balance between the dynamic softening and hardening. Dynamic hardening occurred slightly with a strain rate of 0.001 s−1. Mechanisms of dynamic recrystallization transformed from continuous dynamic recrystallization to discontinuous dynamic recrystallization with the increase in strain when it was deformed at a temperature of 950 °C and a strain rate of 0.01 s−1. The grain size also decreased gradually due to the dynamic recrystallization, which provided an optimal forming condition for manufacturing thin-walled components with the desired microstructure and an excellent performance.

Establishment of Thermal Ductile Fracture Criterion for As-Cast 42CrMo Steel and Its Application in Hot Ring Rolling Process

The casting-rolling compound forming process of ring parts is an advanced plastic forming technology that has been developed due to the merits of high efficiency and energy and material saving. However, cracks often occur during the hot ring rolling process, especially at the edges of the ring parts, which severely affects the forming quality. To predict and try to avoid the occurrence of cracks in the casting-rolling compound forming process of ring parts, the high-temperature fracture behaviors of as-cast 42CrMo steel were investigated by thermodynamic experiment method. The high-temperature tensile tests were carried out using the Gleeble-3500D thermomechanical simulator at various temperatures and strain rates. Stress-strain curves and fracture morphology were examined, through which the sensitivity of stress to temperature and strain rate and the effect of dynamic recrystallization and cavity evolution on fracture were found. The law of critical fracture strains was analyzed, and the model of critical fracture strain as a function of temperature and strain rate was established. Based on Oyane criterion, the thermal ductile fracture criterion was established in conjunction with the model of critical fracture strain. By embedding this thermal damage model into the finite element (FE) model for hot ring rolling of an as-cast 42CrMo ring, the damage prediction for this process was realized, and the thermal ductile fracture criterion was proved to be reliable. From the FE results for hot ring rolling, mechanism of damage and fracture in the hot ring rolling process was analyzed. The damage threshold C f is small, and the damage ratio D is large at the top and bottom edges of the inner surface area of the ring, which have the greatest propensity to cracking in the course of hot ring rolling. This is of great significance in terms of improving the forming quality of ring parts in the casting-rolling compound forming process.

Study on high temperature plasticity of Q390 microalloyed steel

In this paper, the effect of Al and Ti on the high temperature plasticity of Q390 microalloyed steel was studied. The high temperature tensile tests of two Q390 steels with different contents of aluminum and titanium (0.02%Al-0.01%Ti and 0%Al-0.02%Ti) were carried out on Gleeble 3800 thermal simulation test machine. The high temperature plasticity of the two steels was compared and analyzed by calculation of shrinkage ratio, fracture morphology and energy spectrum of the precipitates. The study indicated: The toughness of 0%Al-0.02%Ti steel is 12%-35% higher than that of 0.02%al-0.01%Ti steel in the III brittleness temperature zone. Aluminum has a negative effect on the high temperature plasticity of microalloyed steel, while titanium has a positive effect on the high temperature plasticity of microalloyed steel. Therefore, the surface quality of Q390 microalloyed steel is improved when Q390 is adopted the composition of 0%Al-0.02%Ti steel.