Heating Process Research Articles

Effect of hot air-assisted radio frequency rotation heating system on improving heating uniformity of dried black fungus (Auricularia auricula)

A large-capacity radio frequency (RF) rotation heating system was employed in this study to heat dried black fungus, and hot air was used for assistance treatment. The effects of electrode gap, rotation rate and hot air on the uniformity of RF heating of dried black fungus were explored. The optimal heating process parameters were obtained, and the sterilization effect was validated. The results showed that the rotation system could significantly enhance the RF heating uniformity of black fungus (P > 0.05). The optimal heating process for heating a large-capacity (480 g) black fungus was to utilize RF heating assisted by 70 °C hot air with an electrode gap of 175 mm and a rotation rate of 60 rpm, followed by 30 min of heat preservation at 70 °C hot air with a rotation rate of 40 rpm. After the entire sterilization treatment, the heating uniformity index λ of black fungus was reduced to 0.027 ± 0.004, the total plate count decreased by 3 log CFU/g, and the moisture content dropped to below 13 %. The ideal RF heating uniformity and sterilization effect of black fungus were obtained in this study through the simultaneous use of hot air and rotation, providing a theoretical foundation for the application of RF technology in the processing of black fungus.

A way to control sintering deformation of Al2O3 components by gradient shrinkage

Sintering deformation is a great hindrance to the development of ceramic components with complex shapes. In this work, single-face coating method has been used to prepare the special shaped Al2O3 components by taking advantage of the difference in shrinkage between substrate and coating. By adjusting the content of SiO2 in the coating material which consisted of SiO2 and Al2O3 powder, the sintering deformation of Al2O3 ceramics coated with the above material would be controlled during the sintering process. The sintering behavior of Al2O3 green body with and without single-face coating were studied through visual in-situ tests combined with photographing technology. By comparing the images of specimens under different sintering temperatures (defined this method as the image relative method), the warped deformation and the shrinkage behavior of the above specimens were discussed. Moreover, the relationship between curvature radius and shrinkage rate was deduced. Results indicate that, due to the discrepancy in shrinkage of substrate and coating, the deformation of samples occurred in the heating process. And the shrinkage, the elasticity modulus and the ratio of the sectional coating area to substrate area play a major role in determining the shape of ceramics. The way to fabricate the shape controlled ceramic components by the gradient shrinkage is a novel and effective method, which can be used for the plate and shell products with complex shapes.

The improvement and verification of fluid dynamics simulation on temperature uniformity during heat treatment of ring pieces

The improvement and verification of fluid dynamics simulation on temperature uniformity during the heat treatment of ring pieces are investigated in this study. The accuracy of the temperature field model is validated by comparing the simulation results with the measured temperatures. The findings reveal that the vortex generated near the furnace wall during heat treatment significantly affects the uniformity of the temperature field. To improve this, adjustments are made to the placement of ring pieces based on an experimentally validated fluid dynamics simulation model, and subsequent calculations are performed on this adjusted model. It is observed that these adjustments greatly enhance temperature uniformity in the heating process, with a 39.06 % improvement in medium-temperature zone (732.32–743.69 k) within the furnace compared to the original model. Additionally, surface temperatures of ring pieces in another medium-temperature zone (668.89–691.11 k) show a 34.54 % improvement in comparison to those predicted by the original model.

Nanoporous, Ultrastiff, and Transparent Plastic-like Polymer Hydrogels Enabled by Hydrogen Bonding-Induced Self-Assembly.

Most natural supporting tissues possess both exceptional mechanical strength, a significant amount of water, and the anisotropic structure, as well as nanoscale assembly. These properties are essential for biological processes, but have been challenging to emulate in synthetic materials. In an effort to achieve simultaneous improvement of these trade-off features, a hydrogen bonding-induced self-assembly strategy was introduced to create nanoporous plastic-like polymer hydrogels. Multiple hydrogen bonding-mediated networks and nanoporous orientation structures endow transparent hydrogels with remarkable mechanical robustness. They exhibit Young's modulus of up to 223.7 MPa and a breaking strength of up to 10.3 MPa, which are superior to those of most common polymer hydrogels. The uniform porous nanostructures of hydrogen-bonded hydrogels contribute to a significantly larger specific surface area compared to conventional hydrogels. This allows for the retention of high mechanical properties in environments with a high water content of 70 wt %. A rubbery stage is observed during the heating process, which can reverse and reshape the manufacture of objects with various desired 2D or 3D shapes using techniques such as origami and kirigami. Finally, as a proof-of-concept, the outstanding mechanical properties of poly(MAA-co-AA-co-NVCL) hydrogel, combined with its high water content, make it suitable for applications such as smart temperature monitors, multilevel information anticounterfeiting, and artificial muscles.

Exploring the dual effect of sodium lignosulfonate-modified LDH treatment and heat processing on elevating corrosion and wear resistance of Ni-W composite coatings

The exploration of Ni-W composite coatings with high corrosion and wear resistance is highly important for engineering applications. In this study, LDH-SLS composite nanomaterials were synthesized via hydrothermal synthesis, and Ni-W/SLS composite coatings with excellent wear and corrosion resistance were prepared via pulsed electrodeposition combined with heat treatment. The successful synthesis of LDH-SLS was confirmed by TEM, EDS, FTIR, XPS and XRD analyses. Furthermore, multipoint BET specific surface area analyses demonstrated that pore size and the specific surface area of the LDH materials were enhanced by SLS. Corrosion studies showed that the Ni-W/SLS coatings with the addition of the LDH-SLS nanomaterial had higher impedance compared to the Ni-W coatings. And the Ni-W/SLS coating can show better corrosion resistance after heat treatment at 400°C with an impedance of 2.98 ×104 Ω·cm2, which is 502.2 % higher than that of the Ni-W coating, and a corrosion current of 7.2399 ×10−7 A/cm2, which is two orders of magnitude lower than that of the Ni-W coating. Comparative analyses of coating microhardness, friction curves and average friction coefficients show that heat treatment at appropriate temperatures can significantly improve the wear resistance of Ni-W coatings. The Ni-W/SLS coatings heat treated at 400°C showed the most desirable wear resistance. This study presents a new method for producing Ni-W coatings with high corrosion and wear resistance.

Assessing the impact of Transport phenomena on Modeling and Optimization of Solid-State Fermentation for the Revalorization of Agro-industrial Residues in a Wall-Cooled Packed-Bed Bioreactor

This work assesses the influence of transport phenomena on the growth of Yarrowia lipolytica 2.2ab (Yl2.2ab) and protease production during Solid-State Fermentation (SSF) in a bench-scale wall-cooled tubular bioreactor packed with substrate-based pellets derived from agro-industrial residues. Our engineering methodology, in a novel manner, includes: (i) developing a new pseudo-heterogeneous model, (ii) identifying and quantifying the impact of all transport phenomena on microbial kinetics, (iii) elucidating how fluid dynamics can enhance heat and mass transfer processes, and hence microbial kinetics, and (iv) determining the operational and geometric parameters for optimal bioreactor performance. As main results: (i) all transport phenomena occurring within the bench-scale bioreactor were fundamental for its reliable simulation and will be essential for its scale up, and (ii) the maximum production of proteases, 420 U kgDS-1, was achieved under the following operational conditions: a tube to particle diameter ratio of 5.6, a bath temperature of 45°C, an inlet airflow rate of 1Lmin-1, and inlet fluid temperature (Tg0) of 43 °C. Finally, the pseudo-heterogeneous model was assessed by describing SSF-based observations from the literature, appropriately predicting the performance of Yl2.2ab in a bench-scale bioreactor. These results pave the way for future exploration of Yl2.2ab in SSF within larger-scale packed-bed bioreactors.

Computer simulation of heat and mass transfer processes during water vapor condensation from natural gas combustion products on smooth cylindrical tubes

Computer simulation of heat and mass transfer processes during water vapor condensation from natural gas combustion products on smooth cylindrical tubes

Phase change and fluid transport in porous evaporators

Porous evaporators have become the core component of energy systems such as thermal management of electronic equipment, solar steam power generation, and wet power generation by the advantages of their large specific surface area, high-efficiency heat transfer, and liquid self-transportation. How direct observation of the heat and mass transfer process inside the porous evaporator has always puzzled researchers, resulting in a lack of a theoretical foundation for the optimization of the porous structure. This limitation has significantly hindered improvements in the performance of energy systems. To address this challenge, this study proposes a novel visualization approach that integrates three-dimensional (3D) printing and Indium-Tin Oxide (ITO) glass observation of the phase change region in the evaporator. The key novel findings are that: (1) By controlling the pore size to match the bubble nucleation size, the phase change mode can transition from boiling to thin film evaporation, forming a continuous easy vapor escape channel and enhancing heat transfer. (2) The larger the capillary force of the porous structure, the stronger the locking force at the vapor–liquid interface, which ensured the stability of vapor escape and liquid transport at higher heat flux. (3) An ideal porous evaporator should possess strong liquid locking ability, feature pore structures at the phase change point within the size range of vapor nucleation, and simultaneously exhibit large pore size conducive to vapor escape. This investigation casts a new light on the fluid transport and phase change characteristics of porous evaporators, laying a theoretical foundation for the design of porous evaporators.

Entropy production associated with magnetohydrodynamics (MHD) thermo-solutal natural convection of non-Newtonian MWCNT-SiO2-EG hybrid nano-coolant

This article investigates the convective thermal and solutal exchange from the active walls of a trapezium chamber which is filled with multi-walled carbon nanotubes (MWCNT)-silicon dioxide (SiO2)-ethylene glycol-water hybrid nano-coolant. The hybrid nano-coolant exhibits non-Newtonian shear-thinning rheology and is modeled by the power-law viscosity as per an exploratory report. The convection is generated by both the thermal and solutal buoyancy forces in the presence of a magnetic field. Thermophysical properties of the particular nano-coolants are estimated from the temperature-dependent empirical correlation. An in-house FORTRAN code based on the finite volume method (FVM) has been utilized to simulate the non-dimensional controlling equations representing the physical model. By systematically varying the strength of the magnetic field (Ha=0−50) and its direction (δ1=0−90), the volume fraction of nano-coolant (ϕ=0−0.04) and solutal-to-thermal buoyancy ratio (N=−2 to 2), we thoroughly analyzed their impact on the flow field, thermal, and solutal transmission behavior. Significant impacts arising from the shear-thinning nature (n<1) of the nano-coolant were observed, influencing both thermal and solutal transfer rates as reflected in the Nusselt number (Nu) and Sherwood number (Sh). The impact of Ha on Nu and Sh is more substantial for n<1 than the case n=1. The investigation exposed that when Ha=30,δ1=30∘ the average Nu (Nu‾) for nano-ccolants (ϕ=2%) is maximally enhanced by 80% for n=0.6 compared to the case n=1.0. For the same nano-coolant with Ha=30 and δ1=90∘, there is a 128% elevation in the average Sherwood number (Sh‾) when n=0.6 compared to n=1.0. The entropy generation (S‾) inherent to the heat and mass transfer process and hence a criterion (ξ=S‾/Nu‾) is computed to address the system thermal performance from the thermodynamics second law. S‾ increased as n was reduced, indicating that the shear-thinning effect contributed strongly to the entropy generation.

Improving the performance of a shell and tube latent heat thermal energy storage through modifications of heat transfer pipes: A comprehensive investigation on various configurations

The modification of the geometric configurations of heat transfer pipes in shell and tube Latent Heat Thermal Energy Storage (LHTES) systems not only enhances the melting process of the phase change material (PCM) but also improves the overall performance of these systems. This study aims to investigate ways to enhance the performance of LHTES systems by employing heat transfer pipes with various fin and twisted tape arrangements in a horizontal orientation. The Finite Volume Method and Enthalpy-Porosity method are employed to simulate the melting process. Stearic acid is used as the PCM material, while water serves as the heat transfer fluid. Eight different geometric configurations are modelled in the LHTES system: base case, horizontal fins, vertical fins, helical fins, horizontal tape, vertical tape, twisted tape and helical fins with twisted tape. The results show that within the time range of 0 and 29 min, the combined configuration of helical fins with twisted tape consistently demonstrates the fastest melting process. After 29 min, the configuration with vertical fins exhibits a marginally faster melting process than the combined configuration of helical fins with twisted tape. The configurations involving tapes also contribute to accelerated melting, although to a lesser extent than those with fins. Particularly, twisted tape proves highly effective in facilitating faster melting. The complete melting process times for configurations with vertical fins, helical fins, and combined helical fins with twisted tape are 38.7 %, 23.5 % and 32.7 % faster compared to the base case which is ~69 min. Among the configurations, using tapes results in higher flow resistance and surface area compared to the base case. The attractive features of these configurations make them ideal for creating efficient and space-saving energy storage systems. This study provides crucial insights into essential heat and mass transfer processes, which can be leveraged to develop advanced LHTES systems for enhanced performance and sustainable energy solutions.

Comparative study of hybrid, tri-hybrid and tetra-hybrid nanoparticles in MHD unsteady flow with chemical reaction, activation energy, Soret-Dufour effect and sensitivity analysis over Non-Darcy porous stretching cylinder

Present study investigates influence of Soret-Dufour effects on MHD unsteady flow of a tetra-hybrid nanofluid (Al2O3, Cu, SiO2 and TiO2 with base fluid water) within non-Darcy porous stretching cylinder. Additionally, chemical reaction, activation energy, and heat generation are considered. This research contributes to the understanding of how these nanofluids can optimize heat and mass transfer process in applications such as advanced cooling systems, solar collectors, biomedical devices, and chemical reactors. Tetra-hybrid nanofluids are selected as per novel aspects for their exceptional ability to adapt their properties for diverse applications, including advanced thermal management systems and scenarios requiring high thermal and electrical conductivity. The comparison between hybrid, tri-hybrid, and tetra-hybrid nanofluids serves to evaluate how increasing complexity and diversity in nanoparticle combinations impact thermal and flow characteristics. The prevailing PDE's undergo transformation into nonlinear ODE's through the utilization of similarity variables and numerically solved using fifth order Runge-Kutta Fehlberg method with shooting method. It is established that rising unsteady parameter values result in increasing velocity profile and rising shape factor parameter result in higher heat transfer. Specifically, the Nusselt number increases by 24 % in the tri-hybrid and 11 % in the tetra-hybrid with a higher Soret number, whereas the Sherwood number decreases by 38 % in the tri-hybrid and 26 % in the tetra-hybrid nanofluid. Employing sensitivity analysis, this study also aims to investigate impact of output responses such as local Nusselt number and local Sherwood number on input parameter Dufour number, Soret number and chemical reaction parameter for tri-hybrid and tetra-hybrid nanofluid. It is found out that Dufour number in tetra-hybrid nanofluid has the more significant impact on the Nusselt number, whereas the Soret number predominantly affects the Nusselt number in tri-hybrid nanofluid. These findings underscore the potential of tetra-hybrid nanofluid in enhancing the performance of various industrial and environmental processes.

Effects of standard heat treatment on micro-to nanostructure heterogeneities in a Rene 65 Ni-based superalloy billet

Advancements in the manufacturing of aeroengine components with superior mechanical properties rely on the microstructure homogeneity of industrially forged Ni-based superalloys. Billets often contain microstructural heterogeneities that can persist throughout the process, potentially compromising the integrity of the final product. Rene 65 is a relatively new superalloy with high-temperature mechanical properties superior to those of Alloy 718. However, systematic studies on its microstructure-property relationships are scarce. Here, we correlate the microstructural evolution with the hardness of a Rene 65 billet subjected to industrial processing and standard heat treatments. Multiscale microstructural heterogeneities, including grain size, geometrically necessary dislocations, twin boundary density, and the multimodal distribution of γʹ precipitates, are characterised. Grain growth occurs near the billet centre. Precipitation varies with radial position, showing up to a two-fold change in primary and secondary γʹ fractions. Tertiary γʹ precipitates exhibit variations in morphology and chemical composition, with Cr and Co enrichment near the billet surface. These heterogeneities arise from varying strain distributions and cooling rates during radial forging. Sub-solvus annealing and ageing are shown to mitigate these heterogeneities by promoting recrystallisation, recovery, and homogeneous precipitation of tertiary γʹ. A strengthening model elucidates the active mechanisms in as-received and heat-tread conditions, predicting hardness with a deviation of <8 %. Analyses of grain boundaries and γ/γʹ interfaces reveal strong segregation of Mo, W, Nb, C and B before and after heat treatment, with Mo and B showing the highest interfacial excess values. Insights into the microstructural evolution and its impact on properties could guide the development of next-generation aerospace parts.

Drying kinetics and energy efficiency of Y2O3–CeO2 co-doped ZrO2 powder under microwave heating

Zirconia has important application prospects in the field of ceramics. However, during a high-temperature heating process, pure zirconia will undergo martensite transformation, which seriously affects its service performance. Metal oxides, such as Y2O3–CeO2 doping ZrO2, effectively improve the toughness and fire resistance of the material. Thus, the drying of Y2O3–CeO2 co-doped ZrO2 powder is an essential step before practical application. The study employs contemporary microwave drying techniques. The results of the experiment show that the average microwave drying rate increases with an increase in mass, water content, and microwave heating power. When the initial mass was 30 g, the initial moisture content was 12 %, microwave power was 720 W, and the drying rate was the fastest. We used four dynamic models: Modified Page, Quadratic, Wang and Singh, and Page to fit the experiment data. The best model was Modified Page, which describes the kinetic process most accurately. Fick's second law describes how, in the drying process, when microwave power is 720 W, initial mass is 15 g and initial water content is 8 %, the effective diffusion coefficient is 5.25 × 10−16 m2/s. Fourier Transforms of the infrared spectrum of the samples before and after drying were analyzed, the intensity of the O–H absorption peak located at 3442.03 cm/s, and O–H–O absorption peak located at 1594.48 cm/s. Both decreased significantly after drying. To discuss the relationship between the microwave power and the diffusion coefficient, the activating energy of microwave heating was 32.01 W/g. The experimental results show high heating efficiency and selective heating of the microwave method. This study provides a theoretical basis and research data for microwave drying of Y2O3/CeO2 co-doped ZrO2 powder in industry.

Experimental investigation of mass transfer characteristics in centrifugal humidifier

It is proposed to use humidification-dehumidification technology (HDH) for water recovery in space flight conditions, in conditions of weightlessness, the processes of humidification and drying are realized in centrifugal direct contact devices. The process of heat and mass transfer in a centrifugal direct contact air humidifier is experimentally investigated. The effect of the gravity factor (G=40–650), air velocity (Reair = 5–40), water flow rate (Rew = 28000–94000), geometric parameters of the mesh on the intensity of air humidification was investigated. Experimental studies were carried out on a laboratory stand with an automated system for measuring the main parameters. The parameters of the humidifier will allow the development of a distillation system with a productivity of 1.3 kg per hour, which is enough for a crew of two people. The results of the experimental studies are summarized by new correlations suitable for engineering calculations, which make it possible to calculate the geometric parameters of a centrifugal humidifier for a water recovery system with different productivity.

Confinement and heating promoted RTP of flumequine, oxolinic acid and levofloxacin on papers for their detection and discrimination

Developing simple assays to identify and discriminate quinolones are highly desired for food safety, which remain a great challenge due to the interferences from food matrices and the minor variation on the molecular structure of massive quinolones. We proposed a room-temperature phosphorescence (RTP) assay for the quantitative detection and discrimination of quinolones, aided by a confinement and heating strategy. Quinolones were loaded into the porous framework of paper, which provided confinement effects on the molecular motions of quinolones. The heating process further removed the solvents, eliminating their quenching effects on excitons. These synergistic effects improved the RTP intensity and emission lifetime by 1144-fold and from nanoseconds to seconds, respectively. Three types of quinolones were quantitatively detected and discriminated through pattern recognition methods. The proposed assay showed excellent detection performance in complicated meat samples, aided by the delayed signal collecting of RTP. The reported results provided a clue to modulate the RTP properties of organic molecules, showing great potential for application prospect in food safety analysis, environmental and healthy monitoring.

A sustainable MXene/PVA/CNFs@Fabric roll-based 3D photothermal evaporator integrating efficient evaporation and anti-pollution design

Solar-driven interface evaporation is an effective approach towards achieving clean seawater desalination. The focus of research in this field lies in attaining sustained, stable, and efficient steam generation during the photothermal evaporation process. In this study, the proposed MPFR evaporator featured a 3D spiral conical groove design combined with a hydrophilic MXene/PVA/CNFs functional layer, which effectively enhanced light absorption (>97 %) through multistage reflection and absorption. This facilitated a body-phase absorption/body-phase heating process that effectively reduced the surface temperature of the illuminated area compared to a flat evaporator. Consequently, this was conducive to the absorption of environmental heat to supply water evaporation. Under 1.0 sun illumination, the evaporation rate and evaporation efficiency of MPFR-4 evaporator reached 3.84 kg m−2·h−1 and 156.29 % respectively. The introduction of the hydrophilic functional layer not only enabled water activation but also enhanced the water supply capacity of both yarn and fabric on the evaporator surface, forming a water layer that promoted high-salinity water diffusion and salt crystal dissolution while effectively inhibiting salt crystal pollution. Moreover, this water layer imparted oil-repellent characteristics to the evaporator, enabling it to resist oil-pollution from sea surfaces as well. Thus, this work provided novel insights into designing highly efficient and anti-pollution solar thermal evaporators that drove advancements within green and sustainable water generation.

Sustainable Graphene Production: Flash Joule Heating Utilizing Pencil Graphite Precursors.

The production of graphene from cost-effective and readily available sources remains a significant challenge in materials science. This study investigates the potential of common pencil leads as precursors for graphene synthesis using the Flash Joule Heating (FJH) process. We examined 6H, 4B, and 14B pencil grades, representing different graphite-to-clay ratios, under varying voltages (0 V, 200 V, and 400 V) to elucidate the relationships among initial composition, applied voltage, and resulting graphene quality. Samples were characterized using Raman spectroscopy, electrical resistance measurements, and microscopic analysis. The results revealed grade-specific responses to applied voltages, with all samples showing decreased electrical resistance post-FJH treatment. Raman spectroscopy indicated significant structural changes, particularly in ID/IG and I2D/IG ratios, providing insights into defect density and layer stacking. Notably, the 14B pencil lead exhibited unique behavior at 400 V, with a decrease in the ID/IG ratio from 0.135 to 0.031 and an increase in crystallite size from 143 nm to 612 nm, suggesting potential in situ annealing effects. In contrast, harder grades (6H and 4B) showed increased defect density at higher voltages. This research contributes to the development of more efficient and environmentally friendly methods for graphene production, potentially opening new avenues for sustainable and scalable synthesis.

Quantification of organic and inorganic hydrogen in mudstones: a novel approach using the difference between organic-rich and organic-free mudstones during pyrolysis process

Whether mudstone is rich in or free of organic matter has a great influence on the occurrence of water. Comparing different types of water in organic-rich and organic-free mudstones is helpful for further understanding the role of water in hydrocarbon generation. Thermogravimetric analysis (TGA) and differential thermal analysis (DTA) combined with mass spectrometry (MS) afford the opportunity to identify the mass change, reactions and products of the sample in a real-time monitored heating process. This study compared the pyrolysis characteristics of an organic-rich mudstone (CN1) and an organic-free mudstone (CW1) by using the TGA/DTA-MS method to estimate the content of different types of H2O and CO2 in organic-rich mudstones. The results show that the mass changes in CN1 and CW1 can be divided into the three thermogravimetric (TG) stages of 0°C–200°C, 200°C–650°C, and 650°C–900°C, while the peak temperatures of H2O and CO2 obtained through MS are different for CN1 and CW1. The differences in mineral components and organic matter between CN1 and CW1 suggest that the MS peaks of H2O and CO2 in CW1 are mainly influenced by clay and carbonate minerals, and that those of CN1 are also influenced by organic matter. In addition, quantification equations for CO2 and H2O contents from both the organic and inorganic origin of the organic-rich mudstone can be established by using the MS peak area of CO2 and H2O, mass loss in TGA and the mineral composition of the organic-free mudstone. This work provides useful insights for further understanding the hydrocarbon generation mechanism, as well as quantifying different types of water in organic-rich mudstones.

Tracking protein aggregation behavior and molecular interactions induced by conformational alterations in the formation of myofibrillar protein-Abelmoschus manihot gum mixed gels during heating process

The present study aimed to systematically investigate the effects of different Abelmoschus manihot gum (AMG) concentrations (0–0.5%, w/w) on the formation of myofibrillar protein (MP) gels during heating process (30–80 °C) based on conformational alterations, protein aggregation behavior and molecular interactions. With the increase of temperature, the fluorescence intensity and α-helix content significantly decreased, revealing conformational transition of MP molecular. Dynamic rheological results indicated that MP had completely denatured and formed temporary gel at 50 °C, and completely formed irreversible cross-linked three-dimensional network structure at 80 °C. Moreover, the addition of AMG decreased the fluorescence intensity, as well as induced the transition of MP from α-helix to β-sheet during the whole heating process. Furthermore, AMG addition significantly decreased the turbidity and improved solubility of MP (P < 0.05), especially for at 0.3% AMG concentration, indicating that AMG accelerated the early unfolding and aggregation of MP during heating process. This was verified by the dynamic rheological results. Additionally, hydrophobic interactions and disulfide bonds were the main molecular forces to induce the formation of MP-AMG mixed gel. Therefore, our present results provided the new insights into the formation of MP-AMG mixed thermal-induced gel, and also contributed to the practical application of AMG in meat processing.

Evaluation of the qualitative properties of the oil extracted from the mixture of Helianthus annuus and Nigella sativa seeds during heating

The oil obtained from black cumin (Nigella sativa) seeds has many health-effective properties, which is used in food applications and in traditional medicine. One practical method to extract its oil is mixing with other seeds such as sunflower (Helianthus anuus) seeds before oil extraction by press. The effectiveness of the cold-press oil obtained from the mixture of black cumin seeds (BS) and sunflower seeds (SF) in different proportions 100:0, 95:5, 90:10, 85:15 and 0:100 (w/w) was studied to evaluate their qualitative properties including peroxide value (PV), acid value, p-anisidine value (AnV), pigments (carotenoid and chlorophyll) content, polyphenols, and profile of fatty acids during heating process (30–150 min at 180 °C). The results revealed that the acid and p-anisidine value of the all samples enhanced with the extension of the heating time, and the peroxide value increased at the beginning of the heating and then decreased with the prolongation of the heating time (p < .05). With the increase of temperature and heating time, the peroxide of sunflower oil increased with a higher slope and speed than that of black seed and blends oil. Changes in the PV and AnV were the fastest in sunflower oil. Blending and heating caused considerable changes in the fatty acid composition of oils, especially myristic, palmitic, and stearic acids. Moreover, the levels of certain unsaturated fatty acids, namely linoleic, oleic, and linolenic acids declined after heating. The carotenoids, chlorophyll and total phenol content decreased gradually during heating treatments. Among extracted oils, SF:BS (15%) had the good potential for stability, with total phenol content of 95.92 (Caffeic acid equivalents/100 g), PV of 2.16 (meq O2/kg), AV of 2.59 (mg KOH/g oil), and AnV of 8.08 after the heating. In conclusion, oil extracted from the mixture of SF and BS can be used as salad and cooking oils with a high content of bioactive components and positive nutritional properties.