Biodiesel is considered as alternative green fuels that can be used in Internal Combustion engines as a replacement fuel for conventional diesel. Biodiesel is extracted from vegetable and animal sources which are rich in triglycerides. In this work, an attempt has been made to obtain and characterize the biodiesel from animal wastes such as chicken skin and pig tallow which are available in abundance and at an economical cost within the authors’ geographical location. Initially, the feedstock is decontaminated and subjected to conventional heating to convert it into fatty oil. Heating is carried out at different temperatures and for varying time to find out the optimal combination of time and temperature, which would result in maximum fat yield. The fatty oil is then subjected to the trans-esterification process with methyl alcohol in the presence of a catalyst to extract crude biodiesel. A de-canter funnel is used to separate the glycerine and biodiesel from the crude extract. The extracted biodiesel is mixed in different volume percentages with conventional diesel, and various thermochemical properties were evaluated as per ASTM standards. The test result indicated that the properties of the biodiesel blends were well within the limits as prescribed by ASTM standards.