This paper reports the findings of experimental studies on combined free and forced convection through a plain square duct in laminar region. The test fluid flows through an inner square duct, hot water at high flow rate circulated through a annular channel formed between square duct and circular tube, in counter current fashion to attain a nearly uniform wall temperature conditions. The importance of mixed convection is judged by the value of the Richardson number (Ri). It was observed that at low Reynolds number, heat transfer was mainly governed by mixed convection. However at higher values of Reynolds number, heat transfer was significantly dominated by forced convection. It was found that Reynolds number higher than 1050 for water and 480 for ethylene glycol resulted in laminar forced convention heat transfer. The empirical correlation developed for Nusselt number in terms of Grashoff number and Graez number, was found to fit with experimental Nusselt number within ±11 and ±12 % for water and ethylene glycol respectively.