Area Detector Research Articles

The Simulated Characterization and Suitability of Semiconductor Detectors for Strontium 90 Assay in Groundwater.

This paper examines the potential deployment of a 10 mm × 10 mm × 1 mm cadmium telluride detector for strontium-90 measurement in groundwater boreholes at nuclear decommissioning sites. Geant4 simulation was used to model the deployment of the detector in a borehole monitoring contaminated groundwater. It was found that the detector was sensitive to strontium-90, yttrium-90, caesium-137, and potassium-40 decay, some of the significant beta emitters found at Sellafield. However, the device showed no sensitivity to carbon-14 decay, due to the inability of the weak beta emission to penetrate both the groundwater and the detector shielding. The limit of detection for such a sensor when looking at solely strontium-90 decay was calculated as 323 BqL after a 1-h measurement and 66 BqL after a 24-h measurement. A gallium-arsenide (GaAs) sensor with twice the surface area, but 0.3% of the thickness was modelled for comparison. Using this sensor, sensitivity was increased, such that the limit of detection for strontium-90 was 91 BqL after 1 h and 18 BqL after 24 h. However, this sensor sacrifices the potential to identify the present radionuclides by their end-point energy. Additionally, the feasibility of using flexible detectors based on solar cell designs to maximise the surface area of detectors has been modelled.

Waveform analysis of a large-area superconducting nanowire single photon detector

Superconducting nanowire single photon detectors (SNSPDs) are typically used as single-mode-fiber-coupled single-pixel detectors, but large area detectors are increasingly critical for applications ranging from microscopy to free-space quantum communications. However, the long meander-line length of such large-area SNSPDs results in a proportionately large kinetic inductance that affects the waveform generated by the device. Here, we explore changes in the rising edge of the readout pulse for a single-pixel large-area SNSPD as a function of the optical spot size on the detector and compare to the rising edge of the dark-count waveform. We observe a bimodal distribution of bright-count rise times and show that the probability of a slow rise time increases in the limit of large spot sizes, indicative of a position sensitive response. Additionally, in the limit of low bias currents, the dark-count readout pulse is most similar to the large spot-size bright-count readout pulse, which suggests that dark counts arise from locations spanning the device. These results are consistent with a simple model of traveling microwave modes excited by single photons incident at varying positions along the length of the nanowire.

Orientation-dependent, field-induced phase transitions in soft lead zirconate titanate piezoceramics

In situ high-energy X-ray diffraction (XRD) was performed on lead-zirconate-titanate-based ferroelectric materials with composition near the morphotropic phase boundary (MPB). The utilization of the two-dimensional area detector in in situ field-dependent experiments enables the complete analysis of the material response with respect to all azimuthal angles at each field amplitude. The studies reveal that the field-induced phase transition from tetragonal to rhombohedral is dependent on crystal orientation in Nb-doped PbZr0.53Ti0.47O3 that is in close compositional proximity to the MPB. However, only domain wall motion is activated in Nb-doped PbZr0.50Ti0.50O3, which is further in composition from the MPB. This synchrotron-based XRD characterization approach illustrates the importance in evaluating the orientation-dependence of phase transitions in piezoelectric and ferroelectric polycrystalline materials.

Annular Flow in the Upper Esophageal Sphincter Demonstrated with Dynamic 320-row Area Detector Computed Tomography

Understanding bolus flow patterns in swallowing (rheology, the study of flow) is fundamental to assessment and treatment of dysphagia. These patterns are complex and poorly understood. A liquid swallow is typically biphasic, including air, so the actual bolus has both liquid and gas phases. We report a novel observation of annular two-phase flow (a ring of liquid around a core of air) as thin liquids passed through the upper esophageal sphincter (UES). Dynamic CT was performed on 27 healthy asymptomatic volunteers swallowing liquid barium in a semi-reclining position. Each subject swallowed 3, 10, and 20 ml of either thin (14 subjects) or thick liquid (13 subjects). Sagittal and axial images were analyzed. Flow patterns in the UES were assessed on cross-sectional images. Annular flow was seen in the majority of subjects with thin liquid but few with thick liquid swallows. The percentage of Annular flow during UES opening was 3 ml 58%, 10 ml 58%, 20 ml 56% in thin and 3 ml 0%, 10 ml 4%, 20 ml 1% in thick. Annular flow was usually observed from the second or third frames after onset of UES opening. The other pattern, Plug flow was seldom seen with thin but was typical with thick liquid swallows. Annular flow was the most common pattern for thin liquids (but not thick liquids) passing through the UES. Annular flow has been defined as a liquid continuum adjacent to the channel wall with a gas continuum (core) in the center of the channel. The two regions are demarcated by a gas–liquid interface. Annular flow is typical for two-phase gas–liquid flow in a vertical or inclined channel. It results from the interaction of viscosity with cohesive and adhesive forces in the two phases. We infer that the difference in flow pattern between thin liquid–air and thick liquid–air boluses resulted from the differing magnitudes of viscous forces.

Operation of a novel large area, high gain, single stage gaseous electron multiplier

The operation of a novel large area micro-patterned gaseous electron multiplier, made from a 125 micron thick copper claded kapton foil, the COBRA_125, is presented. The COBRA_125 is equiped with 3 independent electrodes which allow to establish 2 independent multiplication regions in a single micro-patterened gaseous electron mutiplier. We report on the operation of a COBRA_125 with an active area of 100×100 mm2. Charge gains above 104 and energy resolutions in the range 18%–20% were achieved in a mixture of Ar-CH4 (90%–10%) by irradiation with X-rays from 55Fe source. Gain and energy resolutions were stable over the detector area, with maximum deviation from the average values of 8% and 15%, respectively.

Research on the readout noise suppression method for digital correlated double sampling

As the areas of CCD detectors and CCD mosaics have become larger and larger, the number of readout channels in astronomical cameras has increased accordingly to keep the image readout time within an acceptable range. For the large area cameras or the mosaic cameras, the analog Correlated Double Sampling (aCDS) circuit used in traditional astronomical cameras for suppressing readout noise is difficult to integrate into the camera controllers within the constraints of the space and energy consumption. Recently, digital CDS (dCDS) technology has been developed to solve this problem, which also offers novel analysis and noise suppression methods. In this study, a mathematical model is presented to conveniently analyze the frequency characteristic of a dCDS circuit, which is then simulated by a numerical method for investigating the noise suppression capability with different sampling weights. Importantly, using this model, the extreme point with lowest readout noise can be predicted for a certain dCDS model; and for a specific CCD readout frequency, readout noise can be suppressed by selecting the proper dCDS model. A testing system is then constructed for validating the efficiency of the proposed method.

Reciprocal space slicing: A time-efficient approach to femtosecond x-ray diffraction.

An experimental technique that allows faster assessment of out-of-plane strain dynamics of thin film heterostructures via x-ray diffraction is presented. In contrast to conventional high-speed reciprocal space-mapping setups, our approach reduces the measurement time drastically due to a fixed measurement geometry with a position-sensitive detector. This means that neither the incident (ω) nor the exit () diffraction angle is scanned during the strain assessment via x-ray diffraction. Shifts of diffraction peaks on the fixed x-ray area detector originate from an out-of-plane strain within the sample. Quantitative strain assessment requires the determination of a factor relating the observed shift to the change in the reciprocal lattice vector. The factor depends only on the widths of the peak along certain directions in reciprocal space, the diffraction angle of the studied reflection, and the resolution of the instrumental setup. We provide a full theoretical explanation and exemplify the concept with picosecond strain dynamics of a thin layer of NbO2.

Grape Leaf Spot Identification Under Limited Samples by Fine Grained-GAN

In practice, early detection of disease is of high importance to practical value, corresponding measures can be taken at the early stage of plant disease. However, in the early stage of disease or when a rare disease occurs, there are limited training samples in practice, which makes machine learning especially deep learning models hardly work well while the stronger representative ability needs large-scale training data. To solve this problem, a fine grained-GAN based grape leaf spot identification method was proposed for local spot area image data augmentation to the generated local spot area images which were added and fed them into deep learning models for training to further strengthen the generalization ability of the classification models, which can effectively improve the accuracy and robustness of the prediction. Including 500 early-stage grape leaf spot images every category were fed into the proposed fine grained-GAN for local spot area data augmentation, 1000 local spot area sub images every category were generated in this study. The improved faster R-CNN was integrated in fine grained-GAN as local spot area detector. After that, the segmented sub-images and generated sub-images were mixed as training data input into the deep learning models, while the original segmented sub-images were used for testing. Experimental results showed that the proposed method had achieved higher identification accuracy on five state-of-art deep learning models; especially ResNet-50 had got 96.27% accuracy, which obtained significant improvements than other data augmentation methods and verified its satisfactory performance. This is of great practical significance for rare diseases or limited training samples.

Identification of the Ambient Response Relationship in Neutron Counting and Scintillation Measurement Systems

Radiation detection for nuclear security frequently employs neutron counting and scintillation systems simultaneously. One potential issue, particularly when searching a large area, is understanding the ambient (or background) response of these systems throughout the operation. This is easily mitigated for the scintillation system but remains a problem for neutron counting systems. Operational data and previous research have shown that a correlation appears between the neutron count rate and the count rate at high energies in the scintillation system (energies greater than 4 MeV) in background conditions. To understand the cause of the correlation, background measurements were performed using sodium iodide (NaI) and polyvinyl toluene (PVT) scintillation systems. These detectors were calibrated to high energy scales such that their spectra would show energies up to 70 MeV and 85 MeV, respectively. Results show that at least one statistical mode appeared in the spectra on these energy scales (particularly between 5 MeV and 60 MeV). The energy and maximum probability of these modes varied with orientation, and they were dependent upon the detector thickness with respect to the vertical axis and the detector area perpendicular to that axis, respectively. The modes’ energies also matched the expected energy deposition from background muons in the detectors with path lengths equal to one of the detectors’ dimensions. These data matched results from simulations of background muons interacting with these detectors calculated using MCNP, and they similarly matched muon energy spectra calculated from possible path lengths through the detectors using Python. These results indicate that scintillation measurements at energies higher than those employed in typical nuclear security operations are the result of background muons. Since these muons are produced similar processes as background neutrons, the count rate of these particles could potentially be applied to better characterize the background in neutron counting systems.

Detector Tilt Considerations in Bragg Coherent Diffraction Imaging: A Simulation Study

This paper addresses the three-dimensional signal distortion and image reconstruction issues in X-ray Bragg coherent diffraction imaging (BCDI) in the event of a general non-orthogonal orientation of the area detector with respect to the diffracted beam. Growing interest in novel BCDI adaptations at fourth-generation synchrotron light sources has necessitated improvisations in the experimental configuration and the subsequent data analysis. One such possibly unavoidable improvisation that is envisioned in this paper is a photon-counting area detector whose face is tilted away from the perpendicular to the Bragg-diffracted beam during the acquisition of the coherent diffraction signal. We describe a likely circumstance in which one would require such a detector configuration, along with the experimental precedent at third-generation synchrotrons. Using physically accurate diffraction simulations from synthetic scatterers in the presence of such tilted detectors, we analyze the general nature of the observed signal distortion qualitatively and quantitatively and provide a prescription to correct for it during image reconstruction. Our simulations and reconstructions are based on an adaptation of the known theory of BCDI sampling geometry, as well as the recently developed projection-based methods of wavefield propagation. Such configurational modifications and their numerical remedies are potentially valuable in realizing unconventional coherent diffraction measurement geometries, eventually paving the way for the integration of BCDI into new material characterization experiments at next-generation light sources.

Simulation of Monolithically Integrated Meta-Lens with Colloidal Quantum Dot Infrared Detectors for Enhanced Absorption

Colloidal quantum dots (CQDs) have been intensively investigated over the past decades in various fields for both light detection and emission applications due to their advantages like low cost, large-scale production, and tunable spectral absorption. However, current infrared CQD detectors still suffer from one common problem, which is the low absorption rate limited by CQD film thickness. Here, we report a simulation study of CQD infrared detectors with monolithically integrated meta-lenses as light concentrators. The design of the meta-lens for 4 μm infrared was investigated and simulation results show that light intensity in the focused region is ~20 times higher. Full device stacks were also simulated, and results show that, with a meta-lens, high absorption of 80% can be achieved even when the electric area of the CQD detectors was decreased by a factor of 64. With higher absorption and a smaller detector area, the employment of meta-lenses as optical concentrators could possibly improve the detectivity by a factor of 32. Therefore, we believe that integration of CQD infrared detectors with meta-lenses could serve as a promising route towards high performance infrared optoelectronics.

Evaluation of Carbon Based Molecular Junctions as Practical Photosensors.

Molecular junctions with partially transparent top contacts permit monitoring photocurrents as probes of transport mechanism and potentially could act as photosensors with characteristics determined by the molecular layer inside the device. Previously reported molecular junctions containing nitroazobenzene (NAB) oligomers and oligomers of two different aromatic molecules in bilayers were evaluated for sensitivity, dark signal, responsivity, and limits of detection, in order to determine the device parameters which have the largest effects on photodetection performance. The long-range transport of photogenerated charge carriers permits the use of molecular layers thick enough to absorb a large fraction of the light incident on the layer. Thick layers also reduce the dark current and its associated noise, thus improving the limit of detection to a few nanowatts on a detector area of 0.00125 cm2. Since the photocurrents have much lower activation energy than dark currents do, lowering the detector temperature significantly improves the limit of detection, although the present experiments were limited by environmental and instrumentation noise rather than detector noise. The highest specific detectivity (D*) for the current molecular devices was 3 × 107 cm s1/2 /W (∼109, if only shot noise is considered) at 407 nm in a carbon/NAB/carbon junction with a molecular layer thickness of 28 nm. Although this is in the low end of the 106-1012 range for commonly used photodetectors, improvements in device design based on the current results should increase D* by 3-4 orders of magnitude, while preserving the wavelength selectivity and tunability associated with molecular absorbers. In addition, operation outside the 300-1000 nm range of silicon detectors and very low dark currents may be possible with molecular junctions.

Polytypism of Cronstedtite From Nagybörzsöny, Hungary

AbstractThe present study provides an example of the accurate identification of polytypes of trioctahedral 1:1 layered silicates from single-crystal X-ray diffraction data collected with the aid of a four-circle diffractometer equipped with an area detector. Single crystals of the mineral cronstedtite from the Nagybörzsöny gold ore deposit, northern Hungary, were studied. The chemical composition of some crystals was determined by electron probe microanalysis (EPMA). The precession-like images of the reciprocal space (RS) sections created by the diffractometer software and presented in the study were used to determine the OD (ordered-disordered) subfamilies (Bailey’s groups A, B, C, D) and particular polytypes. With one exception, all crystals studied belong to subfamily A. The rare polytype 1M, a = 5.51, b = 9.54, c = 7.33 Å, β = 104.5°, space group Cm is relatively abundant in this occurrence. Another polytype 3T, a = 5.51, c = 21.32 Å, space group P31 was also found. Both polytypes occur separately or in mixed, mostly 1M dominant crystals. Some 1M polytype crystals are twinned by order 3 reticular merohedry with a 120° rotation along the chex axis as the twin operation. A rare 1M+3T mixed crystal with 1M part twinned also contains a small amount of subfamily C. A possible presence of the most common 1T polytype of this subfamily cannot be confirmed because of overlap of the characteristic reflections with those of 3T. Several completely disordered crystals produced diffuse streaks instead of discrete characteristic reflections on the RS sections. The EPMA revealed Fe, Si, traces of Mg, Al, S, and Cl. One black crystal originally considered to be cronstedtite was identified as (111) twinned sphalerite. Some crystals of cronstedtite are covered partially by a honey-brown crust or small crystals of siderite.

Crystal chemistry of schreibersite, (Fe,Ni)3P

Abstract Schreibersite, (Fe,Ni)3P, the most abundant cosmic phosphide, is a principal carrier of phosphorus in the natural Fe-Ni-P system and a likely precursor for prebiotic organophosphorus compounds at the early stages of Earth’s evolution. The crystal structure of the mineral contains three metal sites allowing for unrestricted substitution of Fe for Ni. The distribution of these elements across the structure could serve as a tracer of crystallization conditions of schreibersite and its parent celestial bodies. However, discrimination between Fe (Z = 26) and Ni (Z = 28) based on the conventional X-ray structural analysis was for a long time hampered due to the proximity of their atomic scattering factors. We herein show that this problem has been overcome with the implementation of area detectors in the practice of X-ray diffraction. We report on previously unknown site-specific substitution trends in schreibersite structure. The composition of the studied mineral encompasses a Ni content ranging between 0.03 and 1.54 Ni atoms per formula unit (apfu): the entire Fe-dominant side of the join Fe3P-Ni3P. Of 23 schreibersite crystals studied, 22 comprise magmatic and non-magmatic iron meteorites and main group pallasites. The near end-member mineral (0.03 Ni apfu) comes from the pyrometamorphic rocks of the Hatrurim Basin, Negev desert, Israel. It was found that Fe/Ni substitution in schreibersite follows the same trends in all studied meteorites. The dependencies are nonlinear and can be described by second-order polynomials. However, the substitution over the M2 and M3 sites within the most common range of compositions (0.6 < Ni <1.5 apfu) is well approximated by a linear regression: Ni(M2) = 0.84 × Ni(M3) – 0.30 apfu (standard error 0.04 Ni apfu). The analysis of the obtained results shows a strong divergence between the variation of unit-cell parameters of natural schreibersite and those of synthetic (Fe,Ni)3P. This indicates that Fe/Ni substitution trends in the mineral and its synthetic surrogates are different. A plausible explanation might be related to the differences in the system equilibration time of meteoritic schreibersite (millions of years) and synthetic (Fe,Ni)3P (~100 days). However, regardless of the reason for the observed difference, synthetic (Fe,Ni)3P cannot be considered a structural analog of natural schreibersite, and this has to be taken into account when using synthetic (Fe,Ni)3P as an imitator of schreibersite in reconstructions of natural processes.

Gamma-Ray Burst Triangulation with a Near-Earth Network

Abstract We study the characteristics of near-Earth networks (NENs) of gamma-ray burst (GRB) detectors, with the objective of defining a network with all-sky, full-time localization capability for multimessenger astrophysics. We show that a minimum network consisting of nine identical spacecraft in two orbits with different inclinations provides a good combination of sky coverage with several-degree localization accuracy with detector areas of 100 cm2. In order to achieve this, careful attention must be paid to systematics. This includes accurate photon timing (∼0.1 ms), good energy resolution (∼10%), and reduction of Earth albedo, which are all within current capabilities. Such a network can be scaled in both the number and size of detectors to produce increased accuracy. We introduce a new method of localization that does not rely on on-board trigger systems or on the cross-correlation of time histories, but rather it tests positions in ground processing over the entire sky and assigns probabilities to them to detect and localize events. We demonstrate its capabilities with simulations. If the NEN spacecraft can downlink at least several hundred time- and energy-tagged events per second, and the data can be ground-processed as they are received, it can in principle derive GRB positions in near-real time over the entire sky.

Overview of CMOS Sensors for Future Tracking Detectors

Depleted Complementary Metal-Oxide-Semiconductor (CMOS) sensors are emerging as one of the main candidate technologies for future tracking detectors in high luminosity colliders. Their capability of integrating the sensing diode into the CMOS wafer hosting the front-end electronics allows for reduced noise and higher signal sensitivity, due to the direct collection of the sensor signal by the readout electronics. They are suitable for high radiation environments due to the possibility of applying high depletion voltage and the availability of relatively high resistivity substrates. The use of a CMOS commercial fabrication process leads to their cost reduction and allows faster construction of large area detectors. In this contribution, a general perspective of the state of the art of CMOS detectors for High Energy Physics experiments is given. The main developments carried out with regard to these devices in the framework of the CERN RD50 collaboration are summarized.

High-speed spatial encoding of modulated pump–probe signals with slow area detectors

Most of today’s pump–probe experiments, which rely on two-dimensional detectors, suffer from low read-out rates that prevent the implementation of fast lock-in techniques to increase the signal-to-noise ratio. The first cameras running at true kHz-frame rates are available at large-scale facilities, but require sophisticated data management strategies. Here we present a scheme for high-speed spatial encoding of modulated pump–probe signals using slow area detectors at full repetition rate of a laser system without an increase in data rate or change of the sample environment. Towards that end we block the probe light in front of the detector alternatingly with two inverted masks at the same frequency as the signal is modulated, e.g. the chopping frequency of the pump light. Modulation frequencies up to 500 Hz are demonstrated using a commercial mechanical chopper and have been applied to a time-resolved Faraday microscopy experiment probing all-optical magnetic switching of a GdFe-alloy with femtosecond temporal resolution. We believe that our concept bridges the gap between today’s slow area detectors and the upcoming generation of true kHz-frame-rate cameras.

Spectrometer configuration and measurement uncertainty in X‐ray spectroscopy

How should one select the best detector and the best spectrometer configuration for a particular measurement in X‐ray spectroscopy? The end user is typically interested in obtaining the best precision, accuracy, and detection limit but these are indirectly related to the typical spectrometer specifications, such as energy resolution measured with 55Fe, maximum count rate, or detector area. In this article, we will quantify how the measurement uncertainty (precision, accuracy, and detection limit) are related to spectrometer parameters. We will derive the relationships for common measurement cases, will show data validating these relationships, and will indicate how this information can be used to select the optimum detector and spectrometer configuration for specific applications.

Characterization of an architecture for front-end pixel binning in an integrating pixel array detector

Optimization of an area detector involves compromises between various parameters like frame rate, read noise, dynamic range and pixel size. We have implemented and tested a novel front-end binning design in a photon-integrating hybrid pixel array detector using the MM-PAD-2.0 pixel architecture. In this architecture, the pixels can be optionally binned in a 2×2 pixel configuration using a network of switches to selectively direct the output of 4 sensor pixels to a single amplifier input. Doing this allows a trade-off between frame rate and spatial resolution. Tests show that the binned pixels perform well, but with some degradation on performance as compared to an un-binned pixel. The increased parasitic input capacitance does reduce the signal collected per x-ray as well as increases the noise of the pixel. The increase in noise is, however, less than the factor of 2 increase one would observe for binning in post-processing. Spatial scans across the binned pixels show that no measured signal intensity is lost at the inner binning unit boundaries. In the high flux regime, at a 2×2 pixel wide beam spot (FWHM) size, binned mode responds linearly up to a photon flux of 107 x-rays/s, and performs comparably with un-binned mode up to a photon flux of 108 x-rays/s. While this study demonstrates a proof of concept for front-end binning in integrating detectors, we also identify changes to this early-stage prototype which can further improve the performance of binning pixel structures.

Improvement of a point-contact detector performance using the terajet effect initiated by photonics

A simple millimeter wave and terahertz (THz) receiver scheme that uses subwavelength focusing of electromagnetic beam on the point-contact detector area with waveguide dimensions is studied. A detection system with such an optical coupling scheme is implemented, where the signal to be detected is coupled to a detector through a mesoscale dielectric particle lens based on terajet effect. We have experimentally demonstrated an enhancement of the point-contact detector sensitivity higher than 6 dB and with 1.5 times decreasing of the noise equivalent power value. The results show that the proposed method could be applied to reduce the size and increase the sensitivity of various THz systems, including imaging, which would enable significant progress in different fields such as physics, medicine, biology, astronomy, etc.