Abstract
Highly halogenated organic compounds are combusted in a oxygen flask using water as absorbant in the case of chlorine and 0.05% hydrogen peroxide in the case of bromine. The halogenide ion formed is determined by an iodometric procedure. Results showed an average error of ± 0.1% for Cl and ± 0.2% for Br. They are in close agreement with those obtained by a mercurimetric titration. The iodometric titration is to be preferred because of simplicity and rapidity
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