Abstract
A rapid, simple but precise procedure for microdetermination of halogen in organic compounds is described. This procedure consists of Schöniger's flask combustion technique with an improved method of mercurimetric titration for determination of the halogen. The improvement involves the use of alcohol-water mixture as the solvent in which the discernibility of the endpoint is greatly enhanced. Such enhancement will make the mercurimetric titration suitable for microdetermination. This procedure is just as reliable as the conventional methods, but by its simplicity and rapidity in operation the proposed method has a decided advantage over the more conventional ones.
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