Effect of lateral tip motion on multifrequency atomic force microscopy

Abstract

In atomic force microscopy (AFM), the angle relative to the vertical axis (θi) that the tip apex of a cantilever moves is determined by the tilt of the probe holder and the geometries of the cantilever beam and actuated eigenmode i. Even though the effects of θi on static and single-frequency AFM are known (increased effective spring constant, sensitivity to sample anisotropy, etc.), the higher eigenmodes used in multifrequency force microscopy lead to additional effects that have not been fully explored. Here, we use Kelvin probe force microscopy (KPFM) to investigate how θi affects not only the signal amplitude and phase but can also lead to behaviors such as destabilization of the KPFM voltage feedback loop. We find that longer cantilever beams and modified sample orientations improve voltage feedback loop stability, even though variations to scanning parameters such as shake amplitude and lift height do not.