Wear Tests Research Articles

Wear studies on friction stir processed surface modified AZ61 magnesium alloy with nano titanium oxide

ABSTRACT Surface modification of magnesium alloy enables the improvement of wear characteristics for use in sliding applications and places where surface hardness improvement is essential without affecting the microstructure of the underneath material. In this study, a pin-on disc wear test was used to examine the dry sliding wear behaviour of AZ61 Mg alloy reinforced with nTiO2 by a recursive friction stir processing technique. The trio-behavior of the surface-modified Mg alloy was detailed by the response surface methodology-central composite design matrix with the use of design experiments, considering three levels of reinforcement (%), sliding speed, and axial load parameters. In order to achieve the desired results of minimal wear loss, lower friction coefficient (COF), and lower friction force between surfaces (FF), this present work employed design expert software to develop a generative mathematical model to optimize the process parameters. Wear mechanisms were investigated using images captured by scanning electron microscope.

Heat treatments-induced wear resistance of Inconel 718 superalloy fabricated via Laser based Powder Bed Fusion

Laser based Powder Bed Fusion (LPBF) stands out among Additive Manufacturing (AM) techniques for its ability to fabricate intricate geometries with high precision. However, LPBF produced parts, particularly Inconel 718 (IN718) superalloys, demand further exploration in microstructural and mechanical properties aspect. This study explores the effect of heat treatments on LPBF fabricated Inconel 718. Three distinct heat treatments involving diverse solutionizing temperatures and ageing steps were applied to the LPBFed IN718 alloy. As-printed samples showed columnar dendritic microstructure. The heat treatments led to precipitation of strengthening γ′′ and γ′ phases. A substantial increase in microhardness was observed after heat treatments. Wear tests revealed as-printed specimens suffered higher wear loss (∼889 μm) and coefficient of friction (COF) (∼0.627) attributed to Laves phase and low hardness of the matrix. However, heat-treated specimens exhibited substantially lower wear loss (∼217 μm) and COF (∼0.342), with HT2 condition demonstrating superior wear resistance attributed to a homogeneous microstructure.

Tribological properties and related effects of compressed, thermally modified and wax-impregnated wood

AbstractThis paper develops a process for the preparation of modified wood with low friction and low wear for tribological applications such as self-lubricating bearings. Two types of wood, beech (Fagus sylvatica) and robinia (Robinia pseudoacacia), have been studied and the results compared with naturally lubricated native lignum vitae. The process developed consists of plasticisation followed by compression in a mould, thermal modification and subsequent wax impregnation. Plasticisation was carried out by conditioning the samples to a low equilibrium moisture content of 10%, followed by heating to a sample core temperature of 80 °C. This process protects the internal wood structure from mechanical damage during densification. After plasticisation, the wood was compressed in a press mould. A low springback effect (SBE), resulting in compression of up to 40%, was achieved by unloading the mould without opening it. This step optimises compressive strength and hardness. Subsequent heat treatment reduces thickness swelling by up to 85%. Finally, a wax impregnation was applied to reduce friction. Sliding wear tests on modified beech wood have shown that the lowest wear occurs in the cross-sectional orientation (load perpendicular to the fibre ends; rxt orientation). Sliding friction studies using a steel ball on a ball-on-disc tribometer showed that compressed and thermally modified samples impregnated with rapeseed wax or beeswax exhibited coefficients of friction in a range of 0.08 to 0.09. These values are almost four times lower than those of plain compressed wood and even lower than those of lignum vitae, which was used for plain bearings decades ago. This study clearly demonstrates the high potential of compressed, thermally modified and wax-impregnated wood.

Microstructure, hardness and wear resistance of plasma-sprayed and electron beam remelted Ni-Cr-Re coatings on Inconel 625

This paper presents research on the microstructure as well as mechanical properties of electron remelting of air plasma spraying (ASP) layers made of Ni-Cr-Re alloy with varying amounts of rhenium on Inconel 625. Initially, Ni-20 %Cr powder alloys with 10, 20 and 30 % (by weight) rhenium content were prepared and applied to the Inconel by ASP. Then, the air plasma sprayed coatings were remelted by electron beam under different parameters. The remelting by electron beam improved the density and smoothness of the ASP coatings. The remelted coatings were characterized by a dendritic microstructure. Wear tests revealed that the sprayed and electron-remelted coatings had a lower weight loss for higher Re content and that the hardness the remelted coating increased with increasing Re content.

Effect of Zn on Microstructure and Wear Resistance of Sn-Based Babbitt Alloy

Tin-based Babbitt alloys are a widely used bearing bushing material which have good comprehensive properties. However, problems such as high-temperature softening and insufficient bearing capacity occur during their use, so the optimization of tin-based Babbitt alloys has become a research hotspot. In this paper, ZChSnSb11-6 alloy was mainly prepared by the gravity casting method, and different amounts of Zn were added to the alloy (the mass fraction values were 0 wt.%, 0.05 wt.%, 0.1 wt.%, 0.15 wt.%, and 0.2 wt.%, respectively). Through the hardness test, the tensile test, the friction and wear test, and the microstructure observation of the prepared alloy, the influence of Zn on the organization and properties of the ZChSnSb11-6 alloy was analyzed. The results show that the size of the SnSb hard phase changed with the increasing content of Zn. The size of the hard phase of the SnSb tended to increase first and then decrease, and the number of phase particles increased first and then decreased, resulting in changes in performance. Through comparison, it was learned that the addition of Zn can effectively improve the hardness, tensile strength, yield strength, and wear resistance of the alloy, but the elongation rate was reduced. When the Zn content was 0.1 wt.%, the hardness value of the alloy reached the maximum value, 25.82 HB, which increased by 7.3% when compared with the sample without Zn. The hardness of the Zn, 0.15 wt.%, is close to that of the Zn, 0.1 wt.%. Compared to the sample without Zn, the tensile strength and elongation of the alloy were maximized at a Zn content of 0.15 wt.%. Compared to the sample without the Zn, the tensile strength was increased by 21.29%, and the elongation rate was increased by 46%. An analysis showed that the alloy has good comprehensive mechanical properties when the Zn content is 0.15 wt.%.

Development and characterization of sustainable epoxy resin composites reinforced with palm kernel shell particulate and sisal fiber

This study explores the development and characterization of epoxy resin composites reinforced with palm kernel shell (PKS) particulate and sisal fibers, aiming to create sustainable and high-performance materials. Elemental composition analysis using energy dispersive X-ray revealed significant increases in carbon and oxygen content with higher PKS particulate content, indicating successful reinforcement integration. The mechanical properties were evaluated through Brinell hardness, impact energy, impact strength, tensile stress, and wear resistance tests. The Brinell hardness increased from 31.8 kg/mm2 in the control sample to a peak of 60.6 kg/mm2 in sample SP4, demonstrating enhanced hardness with PKS particulate addition. Impact tests identified an optimal reinforcement level in sample SP3, which achieved the highest impact energy (83 J) and impact strength (47.43 kJ/m2). Tensile stress analysis showed a maximum tensile stress of 28.7991 MPa for SP3, while excessive PKS content in SP4 reduced this to 20.4612 MPa. Wear tests indicated a trade-off between mechanical reinforcement and wear resistance, with the control sample exhibiting the lowest wear rates and SP4 the highest having a 91.9% increase. Based on the obtained results, SP3 with 0.8 g PKS particulate, 0.2 g sisal fiber in epoxy resin matrix seems the optimized composite with enhance mechanical properties without compromising wear resistance.

In Vitro Testing of Protective Eye Wear in Blocking Blue Light from Dental Light Curing Unit

Aim: To evaluate the ef?cacy of wearing protective eyewear in preventing harmful Dental light-curing units (LCUs). Background: Dental light-curing units generate blue light, capable of inducing soft-tissue burns and ocular harm like retinal damage. The intensity of blue light emitted by dental Light Curing Units is substantially higher, thereby potentially constituting a significant "blue light hazard." Material and Methods: To study the effect of protective glasses, reverse methodology was followed as the effect of blue light on the eye is difficult to measure; Circular composite disc samples were grouped into two, one of which was polymerized directly while the other had protective glass in between, Fourier transform infrared spectroscopy (FTIR) analysis was done and the degree of conversion was calculated. Results: Data obtained were analysed using One Way ANOVA. The mean values for "Degree of Conversion" in Group I (Without Protective Glass) is 1.334 +512 and for Group II (with protective glass) is -2.623 + 1.544 .One Way ANOVA revealed statistically significant difference between Group I and Group II (p=0.000) Conclusion: Within the limitations of this in vitro study, it can be concluded that the protective glasses are successful in filtering the harmful blue light emitted by LCU and should be used in day-to-day practice to improve the amount of light they deliver to the restoration from the LCU and prevent any harm to the ocular tissues. Clinical implications: Blue light filtering glasses in a dental operatory provide optimum protection, and the operator can safely watch and improve the amount of light delivered to the restoration from the LCU.

Enhancing tribological performance of AISI 52100: the role of laser surface texturing in dry and lubricated conditions

Abstract Laser surface texturing (LST) is a valuable technique in surface engineering that offers significant improvements in the tribological behavior of metals and alloys. This study investigates the synergistic effect of incorporating hexagonal boron nitride (h-BN) as a solid lubricant with laser surface texturing on the tribological performance of AISI 52100. Dimple textures with varying pitch distances (100, 150, and 200 μm) were created on the surfaces of the mentioned materials using LST. The friction coefficient and wear behavior of both non-textured surface (NTS) and textured surfaces (TS) were analyzed under dry sliding (DS) and lubricating sliding (LS) conditions. Wear tests were conducted using a universal tribometer under a load of 10 N, a sliding frequency of 10 Hz, and a sliding time of 1250 s. The results demonstrate that the presence of dimple textures significantly influences the tribological behavior of the materials. In DS, the wear coefficient exhibits a significant reduction compared to NTS, with decreases of 88.1% for TSP-100, 28.5% for TSP-150, and 76.1% for TSP-200. In LS, the TSP-L-100 (h-BN NPS) surface demonstrates the lowest average wear coefficient among all textured surfaces. Specifically, the TSP-L-100 surface shows a remarkable 97.61% reduction in average wear coefficient compared to NTS. This study demonstrates the potential of LST combined with h-BN as a solid lubricant in improving the tribological properties of metals, offering valuable insights for surface engineering applications in various industries.

Effect of ionic liquid on dispersion stability and antiwear behavior of CuO nanoparticles added to polyalphaolefin base oil

The experimental study assessed the impact of choline chloride cation-based ionic liquid (IL), on the dispersion stability and wear characteristics of copper (II) oxide (CuO) nanoparticles (NPs) in synthetic base oil (PAO 10). CuO NPs, averaging 50 nm in size, underwent surface modification using varying concentrations of the IL (0.25%, 0.5%, 0.75%, and 1% by weight). The formulations were subjected to sliding wear tests to evaluate their wear behavior. Analysis of the worn surfaces utilized scanning electron microscopy, energy-dispersive x-ray spectroscopy, and atomic force microscopy. The results indicated that the combination of 0.75% IL and 1% CuO NPs provided optimal dispersion and exhibited effective surface mending, enhancing wear protection by 21.1% than that of PAO 10. The formulation containing 1% IL and 1% CuO NPs demonstrated the highest load carrying capacity among all tested compositions. In terms of wear behavior, the nanolubricant formulations with 0.75% and 1% IL outperformed the lubricant formulation containing 1 wt% of the commercial antiwear additive Zinc dialkyldithiophosphates (ZDDP).

Investigation of Friction and Erosion Wear Properties of Titanium and Titanium Alloy Pipes.

Titanium alloys are applied in oil and gas development and transportation to improve conditions because of their high specific strength and corrosion resistance. However, the disadvantage of poor wear resistance has become an obstacle to developing titanium alloys. The friction and wear properties of pure titanium TA3 and titanium alloy TA10 were tested under different loads and different friction forms using a reciprocating friction and wear tester. Moreover, the erosion resistance of pure titanium TA3 and titanium alloy TA10 was studied using a gas-solid erosion tester. The results show that the wear rate of TA3 and titanium alloy TA10 increases with increasing friction load. Under a load of 50 N, the mass losses of TA3 under dry friction and wet friction were 0.0013 g and 0.0045 g, respectively, while the mass losses of TA10 were 0.0033 g and 0.0046 g, respectively. While the load increased to 70 N, the mass loss of TA3 was even greater, reaching 0.0065 g, and the mass loss of TA10 was 0.0058 g. The wear forms of TA3 and TA10 include abrasive wear, adhesive wear and oxidation wear. The joint action of various friction forms leads to the loss of materials. Under the simulated working conditions, the erosion rates of TA3 and TA10 were 1.01 × 10-3 g/s and 0.94 × 10-3 g/s. The erosion mechanism is the same, including plowing, indentation and cracking.

Wear mechanisms in polymeric mooring ropes during yarn-on-yarn wear tests

Wear mechanisms in polymeric mooring ropes during yarn-on-yarn wear tests

Study on corrosion behavior and first-principle analysis of M50 steel in lubricating oil contaminated by salt water

The corrosive wear of M50 steel in lubricating oil contaminated with saline is a form of wear that often occurs within the main shaft bearings of aviation engines carried by aircraft working at sea. In the present paper, the corrosion behavior of M50 steel in lubricating oil contaminated with saline was studied. The open-circuit potential, polarization curve and impedance spectrum were analyzed by rotating electrochemical corrosion wear test. A three-layer interface microscopic molecular model was established with Materials Studio to simulate the dynamic corrosion evolution process of M50 steel self-matching pairs and the adsorption energy was calculated. The results show that the corrosion type is pitting corrosion. With the increase of saline concentration, the corrosion area becomes wider and shallower, and the size of the pitting core gradually decreases. The weight loss of M50 steel increases over time, but the trend slows down, which is also shown in the MS simulation results. Electrochemical tests show that the tribocorrosion of M50 steel is related to load, speed. As the load increases, the corrosion rate decreases. And, as the speed increases, the corrosion rate increases. This has practical significance for extending the understanding of tribocorrosion of M50 steel in marine atmospheric environments.

Tribo-technological features of laser powder bed fusion process: scratch and wear resistance of AlSi10Mg aluminium alloy

Mechanical systems, regardless of their complexity, very often require that different parts must move relative to each other by sliding their surfaces, therefore appropriate tribological properties are needed. This request appears particularly evident for components fabricated through Metal Additive Manufacturing processes, due to their typical high surface roughness. In the current study, the Laser Powder Bed Fusion technique with optimized parameters is used to produce samples made of AlSi10Mg alloy. Their tribo-technological properties are investigated through progressive load scratch and dry ball-on-plate wear tests. Along with a global characterization, a local analysis has been performed to identify any variations induced by the building direction. The friction coefficient and the wear rate are generally higher than as-cast specimens. Finally, local trends suggest that the central parts of the samples average offer higher resistance to wear and scratch than the outer areas.

Precipitation Refinement via Aging Time Modification for Enhancing Wear Resistance in Ti–V–Nb Microalloyed High‐Manganese Steels

It is imperative to ensure an even distribution of refined precipitates to enhance wear resistance. Herein, different heat treatments are to control the size and distribution of precipitates. The treatments include water quenching at 1100 °C followed by aging at 400 °C for 24, 60, and 84 h, designated as AT24, AT60, and AT84, respectively. The microstructure, mechanical properties, and impact wear properties of high‐manganese steel are investigated under solution and aging conditions using scanning electron microscopy, field‐emission scanning electron microscopy, tensile testing, and impact abrasive wear testing. Notably, the absence of nanoscale precipitates largely accounts for the poor wear resistance of as‐casting steel, whereas the strengthening effect of larger micrometer‐sized precipitates is insufficient. After the solution and aging treatment, nanosized precipitates continuously form within the matrix, conducive to the formation of the deeper work‐hardening layer, thereby improving the wear resistance. The fine micrometer‐sized precipitates and evenly distributed nanoscale precipitates in AT60 actively contribute to toughness. Additionally, these precipitates interact with slip dislocations, providing stronger strengthening via the Orowan looping mechanism. The wear mechanisms of steel can be transformed from wide, deep pits to shallow grooves and microcutting by extending the aging time.

Erosion Wear Behavior of HVAF-Sprayed WC/Cr3C2-Based Cermet and Martensitic Stainless Steel Coatings on AlSi7Mg0.3 Alloy: A Comparative Study

The paper presents a comparative study of the erosion wear resistance of WC-10Co4Cr, Cr3C2-25NiCr and martensitic stainless steel (SS) coatings deposited onto an AlSi7Mg0.3 (Al) alloy substrate by high-velocity air‒fuel (HVAF) spraying. The influence of the abrasive type (quartz sand or granite gravel), erodent attack angle, thickness, and microhardness of the coatings on their and Al substrate’s wear resistance was comprehensively investigated under dry erosion conditions typical for fan blades. The HVAF-spraying process did not affect the Al substrate’s structure, except for when the near-surface layer was 20‒40 μm thick. This was attributed to the formation of a modified Al-Si eutectic with enhanced microhardness and strength in the near-substrate area. Mechanical characterization revealed significantly higher microhardness values for the cermet WC-10Co4Cr (~12 GPa) and Cr3C2-25NiCr (~9 GPa) coatings, while for the SS coating, the value was ~5.7 GPa. Erosion wear tests established that while Cr3C2-25NiCr and SS coatings were more sensitive to abrasive type, the WC-10Co4Cr coating exhibited significantly higher wear resistance, outperforming the alternatives by 2‒17 times under high abrasive intensity. These findings highlight the potential of HVAF-sprayed WC-10Co4Cr coatings for extending the service life of AlSi7Mg0.3-based fan blades exposed to erosion wear at normal temperatures.

Numerical simulation of multiphase flow and prediction of sediment wear in a large Pelton turbine

AbstractThe problem of sediment wear presents a significant challenge for hydraulic turbines operating in sediment‐rich rivers, particularly for high‐head Pelton turbines. In this study, the VOF model, SST k–ω model, and DPM model were employed to simulate the gas–liquid–solid three‐phase flow within a large Pelton turbine, which operates under a rated water head of 671 m and has a single capacity of 500 MW, at a hydropower station situated on a sediment‐laden river. The sediment wear prediction model, derived from the sediment wear test of the model turbine, was utilized to forecast the sediment wear on the flow components of the Pelton turbine at the hydropower station. The results show that there are obvious pressure and velocity gradients near the nozzle outlet of the Pelton turbine in the power station, and the wear of the nozzle surface is gradually increasing, and the wear in the downstream area of the nozzle is more serious. The wear rate at the needle tip surface reached 1.372 μm/h, while the socket ring surface exhibited a wear rate of 3.175 μm/h. he highest wear rate recorded for the water bucket is 0.940 μm/h. After a year of continuous operation, the maximum erosion observed was 5.62 mm on the runner bucket made of stainless steel and wear‐resistant metal, 8.23 mm on the spray needle, and 19.05 mm on the nozzle mouth ring, highlighting the severity of sediment wear on the Pelton turbine. It is recommended that surface treatment technology be applied to the flow‐through components of the Pelton turbine at this hydropower station to enhance the wear resistance of the turbine and extend the operational life of the unit.

Effect of current on the tribological behavior of Cu-Fe-P immiscible alloy produced by laser powder bed fusion

Cu-based immiscible alloys have significant potential application value in the field of electrical contacts. This study investigated the tribological behavior of Cu-Fe-P immiscible alloys produced via laser powder bed fusion (LPBF) under current-carrying conditions. The alloys consist of softer ε-Cu phase and harder Fe-rich phases. The Fe-rich phase acts as a protective reinforcement during current-carrying friction and wear tests, improving the wear resistance of the alloy. With the increasing current, the coefficient of friction initially rose and then decreased, whereas the wear rate showed a gradual increase. At low currents (0, 2, 3 and 5 A), mechanical wear predominantly governs the wear mechanism. As the current increases, the mechanical wear gradually transitions from adhesive wear to abrasive wear, accompanied by weak oxidative wear. At higher currents (7 A and 10 A), the wear mechanism is dominated by arc erosion wear and oxidative wear. Notably, when the current exceeded 2 A, an oxide film consisting of CuO, Fe2O3, and Fe3O4 formed, enhancing the frictional properties of the alloy. Once the current surpassed 5 A, the arc discharge occurred at high currents, forming molten phases and arc erosion pits on the worn surface of the Cu-Fe-P immiscible alloy.

The effects of different strengthening treatments on wear performance of ZL109 aluminum alloy at high temperature

Enhancing strength or hardness is a widely employed strategy to improve wear resistance of ZL109 aluminum alloy at elevated temperatures. This study aimed to investigate the effects of various strengthening treatments on the wear performance of ZL109 aluminum alloy. Three strengthening methods, namely structural refinement, strain hardening, and precipitation strengthening, were employed to achieve a similar hardness level. Subsequently, the wear tests were conducted using a reciprocating ball-on-disk tribometer under different temperature conditions. The results showed that all the strengthening samples exhibited a similar wear rate (approximately 7.0 × 10−4 mm3/N·m) at room temperature. However, at 250 °C, the precipitation strengthening sample performed best with a wear rate of 1.32 × 10−3 mm3/N·m, followed by the strain hardening and structural refinement samples (approximately 1.7 × 10−3 mm3/N·m). This superior performance was attributed to the precipitation phase, which could effectively maintain material strength through dislocation pinning. By contrast, dynamic recovery and recrystallization behavior weakened the effectiveness of strain hardening, while crystal growth diminished the efficacy of structural refinement. In addition, the wear mechanisms transitioned from abrasion to adhesion and slight oxidative wear as the temperature increased.

Effect of torsional angle on the fretting wear behavior and fracture failure mechanism of steel wires with spiral contact structure

The fretting wear of steel wire will reduce the service life of wire rope and severely threaten the safety of mine hoisting. To investigate the influence of torsion on the fretting wear behavior of steel wire, the fretting wear tests of steel wires with spiral contact structure under the action of tensile-torsional coupling forces were conducted, and the fatigue fracture failure mechanism was revealed. The result indicates that the CoF increases with increasing torsional angle. As the cycles increase, the sliding distance between the wires decreases, while the adhesion increases. The fretting area gradually transitions from gross sliding status to partial sliding status. The sliding distance and energy loss between the wires increase with increasing torsional angle. The wear depth and coefficient increase with increasing torsional angle, and the wear level of peak contact structure is more serious than that of valley contact structure. The primary wear mechanisms of steel wire are abrasive wear, adhesive wear and fatigue wear. The fatigue fractograph of steel wire is obviously divided into fatigue source zone, crack growth zone and final fracture zone. Abundant secondary cracks and dimples exist in the final fracture zone, and the fatigue fracture failure mechanism is mainly ductile fracture.

High-temperature oxidation resistance and wear properties of functionally graded CrHfNbTaTiN high-entropy nitride coating on Ti alloy

High-entropy nitrides have emerged as promising alternatives to traditional protective coatings due to their excellent comprehensive properties. However, there is still a long-standing technical challenge in the design and manufacture of hard and high-temperature stable high-entropy nitride coatings. This study utilized first-principles calculations to evaluate the thermodynamic stability between high-entropy nitrides and corresponding high-entropy metals, as well as titanium alloy substrates, confirming the rationality of the structural design of the functional gradient high-entropy ceramic coating. Subsequently, a double-glow plasma surface alloying technique were conducted to prepare a CrHfNbTaTiN functional gradient high-entropy ceramic coating on titanium alloy, followed by high-temperature cyclic oxidation experiments and high-temperature ball-on-disk wear tests. The research demonstrates that the gradient composition coating exhibits strong interfacial bonding, with an adhesion strength of around 40 N. It maintains excellent oxidation resistance in environments below 700 °C and displays good high-temperature wear resistance. This study contributes to providing insights and guidance for the further development of high-temperature, high-hardness, and wear-resistant materials.