The preparation of biodiesel from Styrax Tonkinensis catalyzed by solid acid S2O82-/ZrO2-TiO2-Fe3O4 at an autoclave was studied in this paper. The magnetic catalysts were characterized by XRD, which explained the high catalytic effect. At the same time, the recovery rate and usage count of catalysts were also studied. And the results showed that a high yield of transesterification can be obtained in a closed autoclave at the condition of catalyst amount 5 %, reaction time 1.5 h, reaction temperature 373K and methanol and oil molar ratio 10:1. The results also showed that the catalysts were still with a higher catalytic efficiency when the catalysts were calcinated after the forth usage.
Read full abstract