Abstract Composite materials play a vital role in developing new materials in engineering and technology. Composites show how the properties of the matrix and reinforcement work together to create more robust, more rigid materials than would be possible from the individual components working alone. They consist of two or more component materials combined with notably dissimilar physical or chemical characteristics. Two categories of composite coupons have been developed in this research work: the first category (C1) is made up of jute twisted-Kevlar twisted jute fiber (0/90 degree), and the second category (C2) is made up of jute twisted-Kevlar twisted jute fiber (0/45 degree). The nano-silica is reinforced with the matrix with a weight percentage of 0%,5%,10% and 15%. The necessary interfacial adhesion and bonding between fiber layers have been accomplished using a 10:1 mixture of epoxy resin (LY556) and hardener (HY951). According to ASTM guidelines, the tensile, flexural, impact, double shear, wear, and hardness tests were carried out. This study uses two natural and synthetic fibers—twisted Jute and Kevlar fibers—as reinforcement. The Jute fibers have a high strength since they are high in cellulose. Efforts have been made to create a composite material with completely different twisted fiber orientations and to assess the mechanical properties of the composites. This involved various mechanical tests, analysis of wear surfaces, as well as DMA, DSC, FEA testing, and ultimately, the machining of the composites studied. The machining parameters used in waterjet machining have been carefully analyzed.