Assessment Of Toughness Research Articles

Indentation Fracture Toughness of Aluminium-Graphite Composites: Influence of Nano-particles

In the field of composite materials, extensive research has been undertaken on aluminum-graphite composites. However, a research gap has been identified regarding the specific influence of nano-sized graphite particles on their fracture toughness. Previous studies have predominantly focused on larger graphite particles or different reinforcement materials, resulting in relatively unexplored effects of nano-graphite particles. This research is deemed critical as it has the potential to generate lightweight, high-strength materials, aligning with the demands of aerospace, automotive, and structural engineering. The primary objective of this study is to investigate how the inclusion of nano-sized graphite particles affects the fracture toughness of aluminum-graphite composites. To achieve this objective, systematic dispersion and incorporation of nano-sized graphite particles into an aluminum matrix will be carried out. Mechanical testing, including fracture toughness assessments, will be conducted to evaluate the performance of the composite materials. Factors such as particle size, distribution, volume fraction, and interfacial bonding will also be characterized within the study. It is anticipated that the presence of nano-sized graphite particles will lead to a significant enhancement of the fracture toughness of the aluminum-graphite nanocomposites. This enhancement is expected to be attributed to crack deflection, tortuosity, altered stress distribution, and increased plastic deformation around cracks.

Numerical calibration for fracture parameters of three-point bending semi-circular specimens

This study aims to refine the fracture characterization of three-point bending semi-circular specimens used in rock fracture toughness assessments. The primary objective is to improve the accuracy of such evaluations by developing numerical simulations of specimens with pre-engineered cracks of varying geometries. Numerical simulations were conducted using the finite element method. The interaction integral method was employed to quantify the stress intensity factors (SIFs) and T-stress at crack tips. Initially, the model’s accuracy was validated by replicating stress singularities at crack tips in a benchmark circular disk with a central straight crack. Following validation, dimensionless fracture parameters specific to the three-point bending semi-circular specimens were calibrated. The numerical results demonstrate that the dimensionless stress intensity factor (YI) increases with both the relative crack length (a/R) and the spacing between support points. Notably, for relative crack lengths a/R ≤ 0.5, the dimensionless T-stress assumes negative values, initially decreasing and then increasing as the relative crack length increases. The findings of this study provide valuable insights into the fracture behavior of three-point bending semi-circular specimens with pre-engineered cracks. Based on the observed trends in the dimensionless fracture parameters, it is recommended that relative crack lengths within the range of 0.2–0.6 be used to maintain the accuracy of rock fracture toughness tests. The finite element method used in this study serves as a robust tool for calibrating fracture parameters, thereby laying a strong foundation for the application of these specimens in rock fracture toughness evaluations.

Assessment of fracture toughness in fibrous concrete via Brazilian test: Experimental study with low-clinker cementitious binder

As the predominant and cost-effective material in the construction industry, concrete is susceptible to tension weaknesses, leading to significant flaws such as cracking and brittle fracturing. Recent advancements in fibrous concrete have emerged as a solution to mitigate these issues. Incorporating steel fibers in concrete has emerged as a promising solution to improve crack resistance and structural integrity. This study focuses on developing eco-friendly concrete using a low-clinker cementitious binder and short steel fibers to enhance fracture toughness and mitigate the environmental impact by effectively utilizing lime sludge. Concrete specimens were prepared with three binder types: treated lime sludge (TLS) at 15 % and 30 % and calcined clay (CC) at 15 % and 30 %, replacing conventional clinker. Short steel fibers were added at 1.5 % by volume to enhance mechanical properties. Fracture toughness was evaluated using notched Brazilian disc specimens, assessing mode I, II, and mixed-mode (I/II) fracture at multiple notch orientations (β = 0°, 15°, 28.83°, 45°, 60°, 75°, and 90°). Microstructural analysis during strength development was performed using scanning electron microscopy and X-ray diffraction. The findings revealed that specimens containing 15 % TLS, 30 % CC, and 1.5 % steel fibers exhibited the highest fracture toughness. Mode II fracture toughness exceeded mode I, indicating improved resistance to crack propagation. The addition of fibers to the specimens under mode II demonstrated improved fracture toughness, ranging from 0.44 to 0.53 MPa·m^1/2 compared to the corresponding non-fibrous specimens. The fibrous specimens showed significantly higher ultimate loads at β = 90° compared to β = 0°, indicating superior crack resistance and structural integrity under perpendicular loading conditions. The Brazilian disc specimens demonstrated variability in fracture toughness across different loading orientations, highlighting their suitability for mixed-mode fracture assessment.

The impact of Si3N4 incorporation on the mechanical characteristics of ZrB2–SiC nanocomposite sintered via pressureless method

Due to their unique properties, ultra-high-temperature ceramics possess have great potential for aerospace and industrial applications. In this study, we utilized ZrB2 and Si3N4 powders in micron scale, along with SiC powder in both nano and micron scale. A nanocomposite comprising ZrB2-20 vol% SiC (15 % nano - 5 % micron)-10 % ZrC was incorporated into the base composition by adding Si3N4 in volumes of 1-2-3 volume and 4 %. The process is carried out by pressure-less sintering at 2150 °C. The evaluation in this study involved X-ray diffraction (XRD) analysis, hardness measurement, density determination, fracture toughness assessment, and bending test. The results showed that addition of Si3N4 enhances the relative density, hardness, and fracture toughness of this nanocomposite. The sample with Si3N4volume fraction of 3 % has the best performance, with a relative density of 99.4 %, a hardness of 20.33 GPa, and a fracture toughness of 3.12 MPa M1/2.

The importance of fracture toughness evaluation for additively manufactured metals

Yield strength and fracture toughness are key properties of structural materials used by designers for engineering applications, whereas secondary properties like ductility are not generally used in quantitative design calculations. However, since ductility is usually measured along with strength in the same tensile test, it is often used as an indication of the fracture toughness even though these properties are usually not directly proportional. As a result, many researchers initially, and only, screen new materials and processing routes for good combinations of strength and ductility rather than evaluating fracture toughness independently. This can result in poorly informed decisions being made early in the development stages for structural applications where materials with combinations of high strength and good fracture toughness are required. In this article, we evaluate the correlation between fracture toughness and ductility of Al-, Fe-, and Ti-based alloys that were processed using conventional methods as well as by additive manufacturing (AM) routes. We highlight that the correlation between fracture toughness and ductility is very weak, which in the case of AM materials is attributed to their often-metastable microstructures, their layer-by-layer mesostructures, and their anisotropic failure characteristics that lead to pronounced variability in the fracture toughness data for materials with similar ductility. Our findings suggest that an independent assessment of fracture toughness alongside the tensile properties (strength and ductility) is required to correctly optimize the AM processing of structural materials and provide engineers with the properties required for the design of parts and components for structural and safety-critical applications.

Comparative analysis of unloading compliance and normalization methods for fracture toughness assessment in 316L stainless steel at cryogenic temperatures

In the present study, the impact of test temperature, specimen geometry, and evaluation methodologies on the fracture toughness of 316L stainless steel was evaluated. Tensile and fracture mechanics tests were conducted utilizing a cryostat across a range of temperatures from ambient conditions to liquid hydrogen environments. The analysis of crack length prediction and resistance curve was performed using two fracture toughness evaluation methods: the unloading compliance method and the normalization method. The difference in fracture toughness by specimen thickness using the normalization method was within acceptable tolerances for all temperatures. However, fracture toughness evaluation using the unloading compliance method showed apparent negative crack growth at all temperatures, causing differences in J-integrals between specimen thicknesses and discrepancies between physical and estimated crack extensions. The application of the offset technique to the unloading compliance method significantly reduced these differences and made the J-integral of the normalization method and the unloading compliance method agree well. The substantial underestimation in the correction of the rotation angle at ambient temperatures was confirmed through real-time imaging of the crack tip with the unloading compliance method, which contributed to the large deviations between estimated and measured crack extensions.

Experimental and numerical assessment of fracture toughness variations in steam boiler components after a long period of operation

This study presents an experimental and numerical assessment of the fracture toughness of steam boiler components, which have been in operation for more than 100,000 h. The materials tested are components of two different parts of a steam turbine unit: the pipeline section that connects the headers with turbines, which is made of 13HMF steel, and the valve chamber section, which is made of L17HMF steel grades. Full-size arc-shaped tension specimens (AT) are employed for the experimental evaluation. AT and single-edge notch tension (SENT) specimens are used for numerical assessment. The finite element method (FEM) formulations are developed and examined in Abaqus, which is set up as a shell model with the specimen thickness designated as the mid-surface for the analysis. The notch is modeled using a contour integral definition based on the maximum energy release rate criterion. The fracture toughness is quantified using the stress intensity factor (KI), and the results are compared. The valve chamber is found to have a higher fracture toughness than the pipeline section. The effect of specimen geometry is also noticeable, and the fracture toughness of SENT and AT specimens are compared. The results are useful in assessing the component's durability after long operation.

Experimental exploration of fracture behavior (pure mode III) in eco-friendly steel fiber-reinforced self-compacting concrete with waste tempered glass as coarse aggregates

To aid in the creation of sustainable structures, scientists have utilized waste materials found in the environment to serve as alternatives for traditional resources in the construction sector. They have undertaken extensive investigations pertaining to this matter. In this particular study, tempered glass as waste glass coarse aggregate (WGCA) was substituted for natural coarse aggregate (NCA) at varying proportions of 15%, 30%, and 45% in the formulation of eco-friendly self-compacting concrete (SCC), combined with hooked-end steel fibers (SFs) at various volumes. The study assessed concrete’s flowability, permeability, compressive strength, and fracture parameters at 28 and 56 days. A total of 240 edge-notched disc bending samples (ENDB) and 60 cubic samples (150 × 150 mm) were tested to assess fracture resilience and compressive strength, respectively. The results showed that increasing SF and WGCA content reduced slump flow diameter and blockage ratio, particularly at higher levels. The solidified characteristics of all specimens incorporating SF and WGCA displayed heightened attributes when contrasted with the reference sample. Among the entire array of specimens, WG15SF0.5 and WG30SF0.5 exhibited the most superior performance, demonstrating an average percentage elevation of 20.29 and 27.63 in both compressive strength and fracture toughness assessments across the different curing periods. SF had the most significant impact on post-cracking behavior by enhancing load-bearing capacity through a bridging fiber mechanism. Through a comparison of the influence of SFs and WGCA on the fracture toughness of pure mode III, it was observed that the inclusion of SF in samples with a 30% replacement of WGCA resulted in an average increase of approximately 15.48% and 11.1% in this mode at the ages of 28 and 56 days, respectively, compared to the control sample.

Microstructure and Impact Toughness of Laser-Arc Hybrid Welded Joint of Medium-Thick TC4 Titanium Alloy

This study delves into the impact toughness of medium-thick (12 mm thick) titanium alloy joints crafted through a multi-layer, multi-pass welding technique that blends laser-arc (MIG) hybrid welding technology. Microstructural scrutiny, employing optical microscopy, SEM and TEM, unveils a consistent composition across weld passes, with prevailing α/α′ phases interspersed with some β phase, resulting in basket-weave structures primarily dominated by acicular α′ martensite. However, upper regions exhibit Widmanstatten microstructures, potentially undermining joint toughness. Hardness testing indicates higher values in cosmetic layers (~420 HV) compared to backing layers and bending tests manifest superior toughness in lower joint regions, attributed to smaller grain sizes induced by repetitive welding thermal cycles. Impact toughness assessment unveils diminished values in the weld metal (WM) compared to the heat-affected zone (HAZ) and base material (BM), amounting to 91.3% of the base metal’s absorption energy. This decrement is ascribed to heightened porosity in upper regions and variations in grain size and phase composition due to multi-layer, multi-pass welding. Microstructural analysis proximal to failure sites suggests one mechanism wherein crack propagation is impeded by the β phase at acute crack angles. In essence, this study not only underscores the practicality of laser-MIG hybrid welding for medium-thick TC4 alloy plates but also underscores the reliability of joint mechanical properties.

Urban transportation system toughness assessment under New Crown epidemics.

Since the concept of toughness was introduced to transportation systems, transportation system toughness has received extensive attention from researchers in the field of transportation worldwide. In this paper, a methodology for quantifying and assessing the toughness of urban transportation systems is proposed in the context of the New Crown epidemic. Firstly, the definition of urban transportation system toughness in this context is clarified, and the entropy evaluation method is applied to construct the performance curve of urban transportation systems over time. Then, it is proposed to quantify the system's resistance, recovery, and adaptive ability in terms of the change in the cumulative amount of system performance. Finally, the three characteristic abilities of system toughness are organically combined to obtain a comprehensive assessment of system toughness. Example calculations and analyses are carried out in four Chinese cities with different levels of development, and the results show that the performance of urban transportation systems is positively correlated with their levels of development, and all of them fluctuate greatly under the influence of the epidemic, but Wuhan has the strongest resistance and recovery ability of the transportation system, and shows the highest toughness, followed by Lanzhou, Changchun, and Shanghai. The system toughness quantification and assessment methods proposed in this paper provide a reference for research on improving the ability of urban transportation systems to deal with multiple uncertainty disturbances.

Tensile and Fracture Characteristics of 304L Stainless Steel at Cryogenic Temperatures for Liquid Hydrogen Service

As the urgency for carbon-neutral fuels grows in response to global warming and environmental pollution, liquid hydrogen, with its high energy density, emerges as a promising candidate. Stored at temperatures below 20 K, liquid hydrogen’s containment system requires materials resilient to such cryogenic temperatures. Austenitic stainless steel, including 304L grade, has been widely used due to its favorable properties. However, designing pressure vessels for these systems necessitates a deep understanding of fracture mechanics and accurate assessments of the material’s fracture toughness at cryogenic temperatures. The mechanical behavior at these temperatures differs significantly from that at room temperature, making testing at 20 K a complex procedure that requires stringent facilities. This study examines the tensile behavior and fracture toughness of 304L stainless steel at cryogenic temperatures, comparing and analyzing the characteristics observed at 20 K with those at room temperature. The phenomenon of discontinuous yield, with abrupt stress drops and stepwise deformation at low temperatures, has been identified, resulting in more complex stress–strain curves. Limitations were found in the calculation of the crack length during the assessment of fracture toughness in stainless steel under extremely low-temperature environments through the J-integral compliance method. To address these constraints, a comparative analysis was carried out to determine potential corrective measures.

Determination on the fracture toughness of the welded joints of X80 pipeline steels based on small punch test

For the sake of design and integrity assessment of the fracture toughness of high-grade pipelines, it is necessary to carry out accurate fracture toughness assessment of the welded joints. The study of more concise and effective fracture toughness testing methods has important theoretical and engineering value. At present, the fracture control of girth welding joints is mainly based on J integral, CTOD and CTOA. However, it is hard to carry out standard fracture toughness tests at some local narrow areas of the welded joints such as the heat affected zone for the difficulty of sampling. On this basis, this paper aims to propose a method to determine the fracture initiation toughness JIC of the welded joints of high-grade pipeline steels based on the micro-sample test method - small punch test. Firstly, small punch specimen with through-thickness notch was designed. Secondly, the finite element model of the notched specimen was established, and verified by the notched specimen tests of X80 steel. Furthermore, the elastic–plastic material properties of different zones of the welded joint were obtained by the empirical correlation method of small punch test and further used for the determination of J contour integral. The GTN damage parameters were calibrated by the three-point bending tests and further used for the determination of the crack initiation displacement. Finally, the fracture initiation toughness JIC(SPT) of different zones of the welded joint were obtained by the SPT method and verified by the three-point bending test. The results show that the fracture initiation toughness JIC(SPT) of each region of the welded joint obtained by notched SPT specimen were all less than the SENB test results. But there is a good empirical correlation between the two results so that the SPT method can be further modified by establishing an empirical correlation model. The SPT method has good engineering application prospect for the accurately characterization of the different distribution of fracture toughness in different areas of the welded joints.

Thermally Activated Crack Growth and Fracture Toughness Evaluation of Pipeline Steels Using Acoustic Emission

The article presents an approach to assessing the fracture toughness of structural alloys based on thermally activated crack growth and recording acoustic emission signals. The kinetic and structural features of the stable growth of the initiated crack are estimated using a multilevel acoustic emission model based on the time dependence of the logarithm of the cumulative acoustic emission count. The article provides an evaluation of the stable kinetic constants included in the equation of the thermal fluctuation steps of a crack according to literature sources and using the acoustic emission method. It is shown that parameters such as activation energy, activation area before the crack tip, and the rate of non-activation crack growth are stable and show a satisfactory correspondence between the reference literature and real experiments. The approach does not require a set of laboratory experiments to determine the empirical constants of traditional crack growth rate equations, and it also differs in that it takes into account the unique features of the destruction of a particular specimen or technological equipment and allows for a non-destructive assessment of fracture toughness. The values obtained are conservative. The concentration criterion of destruction requires further investigation.

Fracture toughness assessment of surface cracks in slender ultra-high-strength steel plates

Safe design against unstable fractures in load-bearing structures is crucial at sub-zero temperatures where the brittle fracture toughness can be unfavourable, especially for high-stress designs incorporating ultra-high-strength steels. The brittle fracture toughness of surface cracks in structural steel with a minimum yield strength of 1300 MPa is, for this reason, tested in the present study at sub-zero temperatures. The realistic flaws are compared with single-edge notched specimens (SEN(B)) from thicker plates with the same chemical composition, using a representative fracture toughness for a three-dimensional crack front according to the Master Curve method. A novel approach determines the latter without considering the local temperature and constraint variation through empirical relations. The experimental result shows a difference in the reference temperature between the two specimen types, which likely is the natural variation of the manufactured materials and/or a loss of constraint due to the difference in the scaled specimen deformation level.

Comments on “Identification of micro‐failure processes of HDPE‐henequen fiber composite material by using acoustic emission monitoring: Effect of fiber surface modification”

AbstractA few comments on the study “Identification of micro‐failure processes of HDPE‐henequen fiber composite material by using acoustic emission monitoring: Effect of fiber surface modification,” have been argued in this research article. These comments are mostly focused on the method exploited for fracture toughness assessment. The fracture toughness of all compounds was utilized via essential work of fracture (EWF), but several specimens did not consider the EWF prerequisites. These requirements are that the ligament shall be fully yielded previous to the onset of crack growth and the fracture takes place under plane‐stress circumstances. Consequently, the data that the writers acquired are questionable.

Fracture Toughness Assessment of 15Kh2NMFA-A Steel Based on Local Fracture Models

Fracture Toughness Assessment of 15Kh2NMFA-A Steel Based on Local Fracture Models

Fracture Testing of Lithium‐Ion Battery Cathode Secondary Particles in‐situ inside the Scanning Electron Microscope

AbstractFracture of cathode secondary particles is a critical degradation mechanism in lithium‐ion batteries. The microindentation strength of LiNi0.8Mn0.1Co0.1O2 secondary particles is measured in situ in the scanning electron microscope (SEM), enabling dynamical imaging of fracture. Crack propagation is intergranular between primary particles when induced by compressing between flat platens (analogous to calendaring), and with a cono‐spherical indenter (representing particle‐particle contact). Fracture occurs directly beneath the cono‐spherical tip and at the centre of secondary particles when compressed between flat platens. Finite element modelling of stress states provides insight into the dependence of fracture load upon cohesive strength and particle toughness. Secondary particle indentation strength decreases with increasing secondary particle size, with cycling, and with increasing state of charge. The indentation strength decrease is greatest in earlier stages of delithiation. The novel microindentation technique allows assessment of strength and toughness of different cathode morphologies, aiding prediction of optimal particle structure and processing conditions.

Assessing Toughness Levels for Nuclear Containment Vessels Steel to Determine the Need for Postweld Heat Treatment Based on the Master Curve Method

AbstractIn this paper, a minimum toughness assessment method of exempting postweld heat treatment (PWHT) based on the master curve method is proposed to replace the current method of determining whether to perform PWHT by material thickness. Reference temperature to prevent fracture (T0-required) for structure to be exempt from PWHT at minimum design metal temperature (MDMT) was obtained by using the master curve method under presumed stresses and flaw size. A series of exemption curves were generated for the steels used in pressure vessels with yield strength of 300∼550 MPa, and the method was corrected for low-stress conditions. Then the feasibility of this method was verified by an engineering example. A SA-738Gr.B welded joint in the example was taken as the research object, the experiment showed that the weld metal was the worst part of the fracture toughness of the joint. The results of research objects which were exempted from PWHT by the proposed method are consistent with ASME Code Case N-841, which proves that this method is feasible in assessing the exemption from PWHT.

Reduced-dimensional phase-field theory for lattice fracture and its application in fracture toughness assessment of architected materials

To develop an efficient numerical scheme for investigating the fracture characteristics of modern architected lattice materials, we present a phase-field fracture model for shallow beams, an assemblage of which forms the lattice. Our approach introduces a simple hypothesis for the variation of phase-field across the beam cross-section along with the standard Euler–Bernoulli type kinematic assumptions to reduce the three-dimensional problem to a one-dimensional one. A variationally consistent formulation based on these hypotheses leads to an overestimation of crack driving energy. Our proposition overcomes it by incorporating a correction within the popular hybrid framework of phase-field fracture. We establish the efficacy and accuracy of the proposed formulation by performing a series of numerical simulations of fracture in beams and comparing the one-dimensional predictions with two-dimensional responses. The beam fracture model is then utilized in several investigations pertaining to architected brittle lattice materials, e.g. direct numerical simulation of crack propagation in lattices, application to concurrent multiscale approach, and utility in sequential multiscale modelling via predicting the fracture toughness of the homogenized material.

A Simple Principle for Fracture Toughness Assessment of Ductile Materials by Ball Indentation Technique

A simple principle for determining fracture toughness (FT) of ductile materials by ball indentation (BI) technique is suggested here. The principle is based on the consideration that the total fracture energy of a material is equivalent to the indentation energy corresponding to a critical plastic strain (CPS); the latter can be estimated from the true fracture strain in tensile test and stress triaxiality ratio in tensile and BI test. Fracture toughness values of 304LN stainless, 316LN stainless, interstitial free (IF), 0.14% C and SA333 steels have been determined by the modified BI technique as well as by standard J-integral test for two steels. A comparative assessment indicates that the equivalent FT values determined by the suggested BI technique is within 5% of the estimated or reported values of J-integral FT of the materials, and thus validates the consideration behind the principle of the suggested BI technique.