Texture Evolution Research Articles

Effect of texture on bending behavior of Mg alloy sheets

The effect of Li elements on the microstructure and texture evolution of AZ31 alloy sheets during room-temperature three-point bending was investigated. The results showed that the conventional c-axis//ND basal texture of the extruded AZ31 sheet could be modified to a TD-elongated fiber texture with a 5 wt% Li addition. As a result, the room-temperature bendability of the Mg–3Al–5Li sheet was improved effectively, and this sheet showed a minimum bending radius of only 2 mm. The superior bendability exhibited surpasses the room-temperature bending capabilities commonly observed in the majority of commercial Mg alloys. The improvement in bendability of the Mg–3Al–5Li sheet was attributed to the TD-elongated texture distribution. This type of texture distribution may offer more effective deformation modes to alleviate thickness strain during bending in comparison to the texture in extruded AZ31 sheets. This study could provide insights into developing Mg alloys with high room-temperature bendability by tailoring texture distribution rather than texture weakening.

Low-temperature phase stability in calc-alkaline granitic systems and significance for cold granites

Granite formation and evolution are influenced by various physical and chemical processes in magmatic systems, resulting in diverse textures and compositions. While the generation of granitic rock through dehydration melting of hydrous minerals, which requires higher temperatures, is widely accepted, the formation and evolution of cold granite remains a topic of considerable debate. Our experiments aim to understand how small changes in granitic magma composition influence late-stage crystallization, providing insights into the chemical and textural evolution of granitic rocks and determining the significance of these conditions in shaping the diversity observed in nature. We conducted crystallization experiments at 1 and 2 kbar, between 680 and 815 °C, using two granitic compositions: a natural I-type granitoid (MA) and a slightly more mafic, synthetic analogue (FC). In these relatively low-pressure and low-temperature experiments, orthopyroxene remains stable at 1 kbar regardless of the starting material. At 2 kbar, its stability is limited to the more mafic sample FC when containing 3.7 wt% water. Hornblende only crystallizes in the more mafic rock FC at 2 kbar across all temperatures tested when water concentration exceeds 4 wt%. Plagioclase spans a broad temperature range (700–815 °C) at both 1 and 2 kbar in the FC material, whereas in the MA material at 2 kbar, it appears only at temperatures ≤725 °C. At 2 kbar few crystals were observed in the MA run at 750 °C, indicating that the liquidus temperature was nearly reached, contrasting with the FC starting material. Additionally, temperature cycling proved more efficient in promoting crystal growth in FC samples. Under low-temperature conditions, only local equilibrium was achieved, highlighting the significant role of late-stage crystallization processes and kinetic limitations in shaping the diversity observed in cold granites. Our experiments demonstrate that even small changes in CaO and FeO content can markedly alter the solidus/liquidus temperature of melts, significantly influence phase stability, melt production, and texture in granitic systems. This study surmises the need to further pursue systematic investigations of the influence of major elements on crystallization sequences in granitic systems, and we compare our findings to previous observations made on the Gentio metagranitoids of the Mineiro belt, Brazil.

Controlling the crystal texture and microstructure of NiTi alloy by adjusting the thermal gradient of laser powder bed melting

The development of a favorable texture can enhance the recoverable strain of polycrystalline NiTi shape memory alloy. Nevertheless, texture tuning of NiTi alloy prepared through additive manufacturing presents more intricate challenges compared to alloys produced using traditional thermomechanical methods, as the solidification process is influenced by various factors. In this study, dense NiTi alloys were fabricated in laser powder bed melting (LPBF) technology. The optimal processing parameters were obtained including a hatching spacing of 24 μm, a forming angle of 90°, and a volume energy density of 139 J/mm3. A robust [001] texture has been developed in NiTi alloys by adjusting the thermal gradient through the precise control of hatching space and energy density. Alloys with this texture manifest a stable and fully recoverable strain of 4.82 %. A novel microstructure evolution mechanism has been proposed to elucidate the texture development during the LPBF manufacturing process under varying thermal gradients. Our findings provide insights into adjusting crystal texture in additive-manufactured NiTi parts through thermal gradient manipulation to achieve superior superelasticity.

Investigating the role of fine grain structure on mineral deposition and resistance to corrosion initiated mechanical failure of the fine grained AZ31 magnesium alloy

ABSTRACT In the present work, fine grained AZ31 magnesium (Mg) alloy was produced by equal channel angular pressing (ECAP) and exposed to simulated physiological conditions to investigate the role of refined microstructure on biomineralisation, degradation and corrosion initiated mechanical failure. ECAP was carried out at 200°C in Bc route for up to four passes (one complete cycle) and a grain refinement up to 1.9 ± 1.1 μm was achieved in AZ31 Mg alloy from a starting size of 36 ± 4.1 μm. X-ray diffraction (XRD) analysis confirms the development of non-basal texture in the ECAPed AZ31 alloy. The phases deposited on the surface of the samples after immersion carried out in simulated physiological environment were analysed by XRD and scanning electron microscopy which confirms the higher level of mineral phase deposition on ECAPed AZ31 alloy due to increased surface energy (39.11 ± 2.1 mJ/cm2) compared with base alloy (20.5 ± 5.3 mJ/cm2). Higher tensile strength (169.9 ± 5.5 MPa) was observed for the fine grained AZ31 Mg alloy compared with the base alloy (120.5 ± 3.7 MPa) to resist the corrosion initiated mechanical failure after exposing the samples to corroding simulated physiological environment for 1 day.

Dual-phase polycrystalline crystal plasticity model revealing the relationship between microstructural characteristics and mechanical properties in additively manufactured maraging steel

To elucidate the relationship between microstructural characteristics and mechanical properties in additively manufactured (AM) maraging steel, this study introduces a computational approach that addresses two fundamental challenges. Firstly, it addresses the creation of representative volume elements (RVEs) that mimic the observed microstructural complexities, such as meltpool boundaries, prior austenite grains, packets and blocks of lath martensite. This is accomplished through the application of Potts Monte-Carlo methods and grain segmentation techniques in accordance with the Kurdjumov–Sachs orientation relationship. Secondly, this study develops a comprehensive crystal plasticity (CP) model encompassing both bcc and fcc plasticity. Inspired by atomistic and discrete dislocation dynamics studies, the proposed CP model incorporates characteristics intrinsic to bcc plasticity, including non-Schmid effects, dislocation and precipitate strengthening, and Hall–Petch type strengthening of elongated martensitic blocks. Utilizing the created RVEs and the proposed CP framework, finite element simulations are conducted based on an update-Lagrangian formulation. The purpose of this study is to investigate the deformation behavior, texture evolution, tension–compression asymmetry, and evolution in dislocation density in RVEs representative of as-built and heat-treated samples of maraging steel. This computational approach and its findings deepen our understanding of the intricate interplay between microstructural characteristics and mechanical properties in maraging steel and also provide valuable guidelines for refining its additive manufacturing and heat treatment processes.

Heat treatment effects and variant selection in multi-material laser powder bed fusion of FeNi- and CoCr-based alloys

ABSTRACT This study demonstrates the successful fabrication of a multi-material 18Ni(300) maraging steel – CoCrMo alloy using laser powder bed fusion (L-PBF), which in its as-built state, displays suboptimal mechanical performance. Addressing this, we propose different heat treatments that mutually enhance the properties of both alloys. Comparative analysis of texture development, precipitation sequence and mechanical properties of the dual structures at different scales has been conducted. The results indicate the cooperative strengthening of intragranular γ–ϵ transformation in CoCrMo, and Ni3Ti precipitation in maraging steel. Adding the solution treatment also balanced the formation of acicular Ni3Ti clusters with (Fe, Ni, Co)2(Ti, Mo) precipitates, and revealed that chemical segregation influences austenite reversion. Initial evidence of local grain variant selection has been revealed in as-built samples due to thermal cycling and austenite reversion, which generates residual stresses, recoil forces and convective flow. Surprisingly, the missing variants can also be inherited after heat treatment with insufficient solution temperatures.

Machine Learning-Aided Analysis of the Rolling and Recrystallization Textures of Pure Iron with Different Cold Reduction Ratios and Cold-Rolling Directions.

We performed a machine learning-aided analysis of the rolling and recrystallization textures in pure iron with different cold reduction ratios and cold-rolling directions. Five types of specimens with different cold reduction ratios and cold-rolling directions were prepared. The effect of two-way cold-rolling on the rolling texture was small at cold reduction ratios different from 60%. The cold reduction ratio in each stage hardly affected the texture evolution during cold-rolling and subsequent short-term annealing. In the case of long-term annealing, although abnormal grain growth occurred, the crystal orientation of the grains varied. Moreover, the direction of cold-rolling in each stage also hardly affected the texture evolution during cold-rolling and subsequent short-term annealing. During long-term annealing, sheets with the same cold-rolling direction in the as-received state and in the first stage showed the texture evolution of conventional one-way cold-rolled pure iron. Additionally, we conducted a machine learning-aided analysis of rolling and recrystallization textures. Using cold-rolling and annealing conditions as the input data and the degree of Goss orientation development as the output data, we constructed high-accuracy regression models using artificial neural networks and XGBoost. We also revealed that the annealing temperature is the dominant factor in the nucleation of Goss grains.

Second phase and matrix texture evolution influence mechanical properties of Al-Mg-Al composite plate by HPR with annealing temperature

Annealing treatment can determine the quality of heterogeneous composite plate by regulating the matrix and interface structures and interlayer bonding ability. Al-Mg-Al composite plate was used as an example. Al-Mg-Al composite plate was rolled with 50 % reduction by hard plate rolling. After that, it was annealed at 250 ℃, 300 ℃, 350 ℃ and 400 ℃ for one hour respectively. Through microstructure observation and performance test, the results show that the reaction phases of Al3Mg2 and Al12Mg17 were formed at the interface during annealing treatment. As the temperature continued to climb, yield strength and elongation after fracture of Al-Mg-Al composite plate showed a trend of increasing first and then decreasing, in addition, the tensile strength gradually decreased. As temperature reached 300 °C, its performance reached the best, the tear strength increased to 0.367 KN, and yield strength and elongation reached 172 MPa and 14.5 %, respectively. The study showed that although annealing temperature didn't change types of texture configuration of magnesium alloy, it affected the grain growth, resulting in the change of base surface texture and the overall performance of heterogeneous composite plate. This research provides a theoretical basis for precise regulation of microstructure and comprehensive performance of heterogeneous composite plate by annealing treatment.

Microstructure and texture evolution in cold-rolled W during annealing

The tungsten(W) was prepared by cold isostatic pressing and sintering, and its characteristics were further enhanced by cold rolling in this paper. The microstructure and textural evolution of cold-rolled and annealed W were primarily studied, and the slip system and dislocations were also deeply researched. The study reveals that grain boundaries in cold-rolled W and samples annealed at 1200 K have small angles of misorientation and high kernel average misorientation (KAM) values, while samples annealed at 1500 K and 1800 K have high angles of misorientation and low KAM values. Low angle grain boundaries (GBs) promote dislocation transfer and improve ductility. After 1800 K annealing, W becomes nearly-equiaxed polyhedrons, with γ-fiber texture dominating. The rolling direction (RD) is better suited for plastic deformation than the transverse direction (TD), but plasticity deteriorates due to changes in microstructure.

Microstructure and Texture Evolution in Thermomechanically Processed FCC Metals and Alloys: a Review

Microstructure and Texture Evolution in Thermomechanically Processed FCC Metals and Alloys: a Review

Evolution of magnetization textures in Mn1.4PtSn under magnetic field

We have used Lorentz transmission electron microscopy (LTEM) and the transport of intensity equation (TIE) method to investigate the spin structures in the Mn1.4PtSn magnet, which exhibits D2d symmetry. The evolution of the spin structures under the external magnetic field was observed. In particular, a perpendicular field is able to modulate the striped domain widths and to induce the formation of anti-skyrmions and bubbles. While an in-plane magnetic field can control the state of these structures, the coexistence of different types of skyrmions suggests that the hysteresis properties of the magnet may affect the effectiveness of the field control.

Microstructure Characteristics, Texture Evolution and Mechanical Properties of Al–Mg–Si–Mn–xCu Alloys via Extrusion and Heat Treatment

Microstructure Characteristics, Texture Evolution and Mechanical Properties of Al–Mg–Si–Mn–xCu Alloys via Extrusion and Heat Treatment

Electric pulse-induced suppression of the Portevin – Le Chatelier behavior of 5086 aluminum alloy under uniaxial tension

The electrical-assisted tensile tests of 5086 Al alloy sheets with different current parameters were carried out at room temperature with a frequency of 150 Hz and voltages of 50 V, 60 V and 70 V. It was found that the serrated plastic instability (named PLC effect) was eliminated as the pulse current increased to 150 Hz/60 V, but the PLC effect was observed with 150 Hz/50 V. To distinguish the thermal effect and athermal effects of pulse current on PLC effect, the comparative heating tensile (HT) test in furnace with a temperature rising trend of 150 Hz/60 V was conducted. The obtained curves still showed serrated flow behavior, indicating that the thermal effect was insufficient to suppress the PLC effect. The influence of pulse current on the microstructure and texture evolution was investigated through TEM and EBSD. According to the microscopic analysis, the pulse current accelerated the solute atoms' diffusion and dislocation movement. S orientation {123}<634> of 150 Hz/60 V presented more obvious transformation compared with that of HT specimen. It was illustrated that the athermal effect of pulse current plays an important role in the crystal orientation and suppressing the PLC effect.

The impact of annealing temperature and time on the grain distribution and texture evolution of cold-rolled electric-furnace annealed low-carbon steel

This study investigated the effect of annealing temperature and time on the grain distribution and textural development of commercial-grade low-carbon steel that undergone cold rolling and subsequent electric-furnace annealing at either 700 or 800 °C for 5 and 10 min. Scanning electron microscopy and electron backscatter diffraction analyses of the annealed samples revealed equiaxed microstructures with cementite at the ferrite grain boundaries. The samples annealed at 700 °C for 5 and 10 min exhibited a bimodal grain distribution, while larger ferrite grains formed at 800 °C. The orientation distribution function texture of the sample annealed at 700 °C for 5 min exhibited both a γ-fiber ND//〈111〉 and a cube texture ND//〈001〉 . Raising the annealing temperature and time reduced the intensity of cube texture and strengthened the γ-fiber, increasing tensile elongation from 8 to 38 %.

Grain Refinement and Texture Evolution of an AA5052 Aluminum Alloy during Flow Forming

Grain Refinement and Texture Evolution of an AA5052 Aluminum Alloy during Flow Forming

Texture evolution prediction of diffusion bonded titanium alloy with hot gas bulging experiments by cross-scale simulation modeling

Texture evolution prediction of diffusion bonded titanium alloy with hot gas bulging experiments by cross-scale simulation modeling

Wire arc additive manufacturing method for Ti–6Al–4V alloy to improve the grain refinement efficiency and mechanical properties

Wire and arc additive manufacturing (WAAM) technique has introduced a novel approach for producing complex Ti–6Al–4V parts with metric dimensions. However, the produced part leads to the development of a strong texture and anisotropic mechanical properties due to the formation of large columnar β grains. To resolve this issue, the plastic deformation of each deposited track through hammer peening was developed as a means to refine these large β grains. In this study, we have investigated an innovative approach to further enhance the efficiency of β grain refinement by minimizing the arc heat input associated with previous deposited layer, which is achieved by employing a C-type filler wire. Our findings reveal a notable enhancement in grain refinement efficiency through the utilization of a C-type filler wire with peening process, as compared to available conventional commercial round shape filler wire. Specifically, the employment of the C-type filler wire results in a reduced melt pool penetration depth of WAAM Ti–6Al–4V (3.3 mm), compared to the commercially available round shape (R-Type) filler wire (4.48 mm). Within the plastically deformed region by peening, fine and randomly oriented β grains are observed, extending to a depth of deformation reaching 844 ± 32.65 μm. Peening WAAM Ti–6Al–4V with the C-type filler wire leads to the development of isotropic mechanical properties in both horizontal and vertical directions, offering high strength due to the presence of small equiaxed β grains and thin α laths (0.56 ± 0.18 μm), in contrast to the use of conventional commercial round shape filler wire.

Textural and compositional evolution of quartz and cobalt-bearing minerals from the Wubaoshan Deposit, Jiangxi Province, South China: Implications for cobalt mineralization

Cobalt resources are primarily derived from hydrothermal-related deposits; however, our understanding of the mechanisms governing cobalt transportation and deposition, particularly for cobalt arsenides and sulfarsenides within hydrothermal fluids, remains limited. In this study, we present a comprehensive investigation into the Wubaoshan cobalt deposit located in the Qin-Hang ore Belt, South China. This deposit exhibits mineralization associated with multiple hydrothermal fluids, resulting in complex paragenesis and the formation of cobalt minerals. By employing a combination of petrographic and geochemical observations, we explore the conditions of the ore-forming fluid and the hydrothermal mechanisms underlying cobalt mineralization. Our analysis reveals three distinct hydrothermal stages of mineralization: Stage 1 is characterized by quartz-arsenopyrite-pyrite assemblages formed at relatively high temperatures (352–390 °C), neutral pH, and high fS2 (log fS2 = −6.9 ∼ −8.8); Stage 2, the pivotal stage for cobalt mineralization, displays various sulfides-sulfarsenides formed at lower temperatures (229 ± 6.0 °C), under acidic conditions, and low fS2 (log fS2 = −12.0 ∼ −14.0); and Stage 3 comprises minor sulfides and carbonates formed at relatively lower temperature and pH. Sulfur isotope analysis of pyrite from Stage 1 (+13.49 to +14.30 ‰) and sphalerite from Stage 2 (+5.53 to +9.21 ‰) suggests a mixed sulfur source derived from both Permian seawater sulfate and related magmatic rocks. Additionally, our results reveal that a transformation from cobalt arsenide to sulfarsenide during Stage 2, likely influenced by the change of As/S ratio in ore fluids, which is affected by the influx of external sulfur from magmatic hydrothermal fluids. Our findings, together with the previous thermodynamic modelling results, indicate that the variations of the ore fluid condition, particularly temperature and pH, govern the precipitation and dissolution of mineral during cobalt mineralization. These findings contribute to our understanding of the formation processes of the Wubaoshan deposit and provide valuable insights into the mechanisms of cobalt enrichment.

Effect of Cold Drawing Deformation on Themicrostructure and Evolution of Texture of Near Eutectoid Pearlitic Steel

Effect of Cold Drawing Deformation on Themicrostructure and Evolution of Texture of Near Eutectoid Pearlitic Steel

Effect of initial grain size on microstructure, texture and magnetic properties of non-oriented electrical steel

The effect of initial grain size prior to cold rolling on the microstructure, texture evolution, and magnetic properties of Fe-3.5 wt% Si non-oriented electrical steel (NOES) was investigated through the introduction of normalization. There were massive intragranular shear bands in {111}<110> and {111}<112> deformed grains in the cold-rolled sheet with large initial grain size, providing nucleation sites for new recrystallized grains with Goss ({110}<001>), λ-fiber, γ-fiber, and {113}<631> components. Subsequent annealing resulted in weaker γ-fiber ({111}<110>−{111}<112>), stronger α*-fiber concentrated at {113}<631>, along with Goss and λ-fiber ({100}<001>−{100}<012>) textures. In addition, appropriate final annealing temperature effectively reduced iron loss. The simultaneous optimization of texture and grain size by normalization and annealing treatments led to improved magnetic properties, with the superior magnetic induction (B50 = 1.719) T, and the lowest core loss (P15/50 = 2.69 W/kg, P10/400 = 16.337 W/kg).