Tensile Behavior Research Articles

Synergistic effects on dielectric and complex impedance properties in Ti3AlC2 MAX phase‐infused PVDF‐HFP/PMMA nanocomposites

AbstractA simple solution casting technique was used to formulate films of polyvinylidenefluoride‐co‐hexafluoropropylene, polymethylmethacrylate, and Ti3AlC2 MAX phase polymer nanocomposites (PPT) with different filler content. The functional groups present in the PPT films were studied using the Fourier transform infrared spectroscopy and the nature of crystallinity was observed using X‐ray diffraction technique. The morphology of the films was studied by scanning electron microscopy. The thermal analysis was done using the thermogravimetric analysis and differential thermogravimetry analysis. The tensile behavior of the prepared films was studied from the stress‐strain graphs. The ultraviolet–visible spectra revealed their optical characteristics. The dielectric parameters of the polymer blend and nanocomposite films like dielectric constant, loss tangent, AC conductivity, and complex impedance spectroscopy with corresponding equivalent circuits were studied. A comparative study of the above parameters was done for both the polymer blend and nanocomposites to find out the advancement in the properties of the prepared nanocomposite compared with the polymer blend. The nanocomposite film having 3 wt% of Ti3AlC2 MAX phase filler loading exhibited the best properties among all the nanocomposites. The enhanced dielectric properties of the nanocomposites with mechanical and thermal resistance can be used for real‐time efficient energy storage applications.

Cryogenic damage behavior of carbon fiber reinforced polymer composite laminates via fiber-optic acoustic emission

Cryogenic temperatures cause significant changes in the mechanical response and microscopic failure mechanisms of carbon fiber reinforced polymer (CFRP) composites. However, the mechanisms by which cryogenic temperatures affect composites are not yet fully understood due to a lack of adequate in-situ characterization techniques. Herein, the cryogenic damage evolution process of CFRP composites was investigated by constructed fiber-optic acoustic emission (AE) detection system. Tensile damage behavior of woven CFRP composites at 300 K, 153 K and 77 K was evaluated by AE characteristic response and cluster analysis combined with scanning electron microscopy. According to the results, increased damage activity within the composites at cryogenic condition promoted the release of mechanical energy, as well as an increase in the contribution of fiber damage to overall damage, which are the dominant micro-strengthening mechanisms of composite laminates under cryogenic conditions. This study provides a novel explanation for understanding the cryogenic damage behavior of composites.

Exploring the impact of epoxy coated 3D-Printed polymers on surface roughness and mechanical behavior: An experimental and numerical study

The present study used polymers such as PLA and ABS filaments for the 3D printing parts with varying layer thicknesses. The mechanical properties and surface finish of the as-printed and epoxy resin-coated samples were investigated. Noteworthy findings indicate that when the PLA material is printed at a layer thickness of 0.06 mm followed by no coating one can achieve superior tensile strength of approximately 39 MPa as compared to 20 MPa of ABS material. The ultimate tensile strength of the coated materials averaged approximately 15 MPa for both PLA and ABS. The surface roughness of PLA material printed with a 0.06 mm layer thickness showed a 95.13 % reduction after coating. Despite ABS samples being harder than PLA material, the layer thickness emerged as the most influential factor in enhancing the hardness. The dominance of lower layer thickness over other conditions is particularly evident in the modulus of elasticity. In addition to the experimental investigation, a non-linear structural analysis of the uniaxial tensile behaviour of the coated and uncoated 3D prints was also carried out. The fracture modes and deformation behaviours in numerical modelling and experimental results across various parametric conditions were found to be in good agreement. Specifically, the numerical results at lower loading conditions for a layer thickness of 0.06 mm PLA and ABS samples, in the uncoated conditions, mirrored the experimental outcomes.

Tensile properties and damage behaviors of the prepreg-RTM co-cured composite bolted T-joint with a novel configuration

The tensile properties and damage behaviors of prepreg-resin transfer molding (RTM) co-cured composite bolted T-joints, consisting of an internal skeleton and an external skin, were investigated through experimental and numerical methods. With the validated finite element model, the effects of adding load-carrying beams, the corner radius and the stacking sequence were investigated. Results indicate that the novel T-joint, weighing only 55.7% of an equivalent sized 2A12 aluminum T-joint, can achieve 82% of the aluminum T-joint’s tensile stiffness and 107% of its proportional limit load. Damage in the joint initiates near the bolt holes and leads to delamination failure within the skeleton. With load-carrying beams including bolt holes, the tensile stiffness and ultimate load increase to 1.11 and 1.51 times that of the original configuration, respectively, with the final failure mode shifting to the fracture of the base panel. With the final failure mode unchanged, the ultimate load remains essentially unchanged with increasing the corner radius. Under tensile loads, the preferred stacking sequence for the skeleton is [0/+45/90/−45]nS. For the skin, the greater the number of ±45° plies, the higher the ultimate load, while the greater the number of 90° plies, the higher the tensile stiffness.

Simulating loading–unloading hysteretic behaviors of nematic-genesis polydomain nematic elastomers

Nematic elastomers (NEs) are lightly cross-linked elastomers with nematic mesogens integrated in their polymer networks. Combination of large deformation capability with nematic-isotropic phase transition enables NEs to be the most promising soft materials for impact attenuation, actuation and soft robotics. In this paper, we focus on nematic-genesis polydomain NEs (N-PNEs) where mesogens are cross-linked at nematic states. N-PNEs are capable of absorbing and dissipating energy and easy to synthesize. We present a Voronoi diagram-based finite element model for specimen-scale N-PNEs, and investigate the cyclic tensile and compressive behaviors of N-PNEs at different strain rates. Our simulations reveal a smooth polydomain-monodomain transition during loading, accompanied by a full recovery of polydomain texture after the load is removed, indicating a memory effect of initial disordered mesogen alignment. The predicted behaviors align well with experimental observations, which validates our model. Furthermore, we assess the energy absorption and dissipation capabilities of N-PNEs compared to monodomain NEs, identifying conditions where N-PNEs exhibit superior performance. This study not only enhances our understanding of polydomain-monodomain transitions in N-PNEs, but also lays the groundwork for the development of N-PNE-based energy absorbers.

Anomalous temperature-dependent strength of copper alloy manufactured by laser-beam powder bed fusion

This study reports an anomalous temperature-dependent tensile behavior of laser-beam powder bed fusion (PBF-LB) processed Cu–Cr–Zr alloy. The yield strength of the alloy initially decreases as the temperature increases to 200±5 MPa and then increases to 350±11 MPa at 500°C before reducing to 234±6 MPa at 600°C. The microstructure consists of elongated Cu grains with a high concentration of Cr solute (∼1 mass%), resulting from rapid solidification during the PBF-LB process. Transmission electron microscopy for the specimens deformed at 500°C revealed the presence of numerous nanoscale Cr-rich particles embedded inside the supersaturated solid solution of the Cu matrix. Nanoscale particles can act as barriers to dislocation motion, leading to an increase in internal stress during plastic deformation at elevated temperatures. This work provides the high potential of post heat treatments for achieving superior mechanical performance using high solute supersaturation formed by the PBF-LB process.

Synergic effects of silica aerogel (SA) particles on tensile behavior of cryo-conditioned epoxy: The role of particle morphology and mixing sequence

Cryogenic conditions are of crucial importance for gas storage tanks to provide increased storage density, reduced pressure requirements and minimized energy losses. Incorporation of silica aerogel (SA) particles as a nanostructured material with extremely low density and exceptional thermal insulating properties into epoxy matrices has the potential to facilitate the progress of high performance nanocomposite coatings for advanced cryogenic applications. The objective of this study is therefore to investigate the impacts of particle size, particle content, milling method and mixing sequence on toughness of the cryo-conditioned epoxy coatings. SA particles of varying size (50 μm to 300 μm) were prepared using two different techniques (planetary ball milling vs. 2-blade grinding). Nanocomposite samples were prepared using two distinct mixing sequences, i.e., adding particles (in 0, 0.5, 1 and 1.5%wt.) to epoxy followed by mixing with hardener or adding particles to epoxy/hardener (with 3 or 15 min delay). The nanocomposite samples were subjected to different cryogenic conditions (single 3-h immersion in liquid nitrogen vs. three consecutive 1-h immersions). Mechanical properties of the samples were evaluated by conducting fractography, dynamic mechanical thermal analysis (DMTA) and tensile tests. Large SA particles settled towards the bottom of nanocomposite and resulted in loss of mechanical properties at cryo-conditions. Mixing 1 wt% of optimized SA particles with epoxy/hardener system led to an enhanced tensile strength (26 %), stiffness (3 %) and toughness (71 %) by providing uniform cross-linking reactions and mitigating thermal shock effects at cryo-conditions. Toughening mechanisms included crack deflection, crack pinning, crack arrest and crack branching.

Preliminary Experimental and Numerical Study of the Tensile Behavior of a Composite Based on Sycamore Bark Fibers

In the context of global sustainable development, using natural fibers as reinforcement for composites have become increasingly attractive due to their lightweight, abundant availability, renewability, and comparable specific properties to conventional fibers. This paper investigates the tensile properties of a sycamore bark fiber-reinforced composite. The tensile tests using digital image correlation showed that, by adding 18% by volume of sycamore bark for the polyester matrix, the tensile modulus achieves 4788.4 ± 940.1 MPa. Moreover, the tensile strength of the polyester resin increased by approximately 90% when reinforced with sycamore bark fiber, achieving a tensile strength of 64.5 ± 13.4 MPa. These mechanical properties are determined by the way loads are transferred between the polyester matrix and fibers and by the strength of the bond between the fiber-matrix interfaces. Since it is difficult and time consuming to characterize the mechanical properties of natural fibers, an alternative approach was proposed in this study. The method consists of the identification of the fiber elastic modulus using a finite element analysis approach, based on tensile tests conducted on the sycamore bark fiber-reinforced composites. The model correctly describes the overall composite behavior, a good agreement is found between the experimental, and the finite element predicted stress–strain curves. The identified sycamore bark fiber elastic modulus is 17,763 ± 6051 MPa. These results show that sycamore bark fibers can be used as reinforcements to produce composite materials.

Insight into the dynamic tensile behavior of deep anisotropic shale reservoir after water-based working fluid cooling

During deep shale gas production, flowing water-based working fluid inevitably cools shale reservoirs around boreholes and some fractures, and possible extraction methods induce dynamic stresses. To understand the dynamic tensile behavior of deep anisotropic shale reservoir after water-based working fluid cooling, a split Hopkinson pressure bar was used for performing the dynamic Brazilian tests on shale samples with bedding angles of 0°, 30°, 45°, 60° and 90° after reservoir temperature realization (25–200 °C) and water cooling. The results illustrate that dynamic tensile strength of shale samples decreases gradually as reservoir temperature increases under the loading rates 100–1000 GPa/s. From room temperature to 200 °C the most strength deterioration appears on samples with the bedding angle of 90°. A dynamic tensile strength deterioration model for deep shale reservoirs after water-based working fluid cooling is proposed considering the influence of loading rate and bedding angle. Geometrical trajectories of the main failure cracks are separated into three types, i.e., fully central tensile failure, tensile-shear failure and fully shear failure (sliding of bedding planes). For samples with bedding angles of 30°, 45° and 60°, increasing reservoir temperature encourages tensile failure to change into shear failure. The roles that bedding planes play in interacting with failure crack growth are summarized as IP mode (intersecting propagation), TP mode (turning propagation) and PP mode (promoting propagation). Anisotropic dynamic tensile strength responses are systematically discussed by using thermal stress simulation in ABAQUS, microstructure analyses, crack interaction conditions and the one-dimensional stress wave propagation theory. Based on experimental observations, field implications in borehole stability and fracturing of deep shale reservoirs are proposed under medium and high loading rates. This work is instrumental in providing valuable information and technology assistance for real deep shale gas production projects.

Carbon effect on tensile and wear behaviors for a dual-phase Fe61.5Cr17.5Ni13Al8 alloy

High entropy alloys (HEAs) series were produced by doping carbon into Fe61.5 Cr17.5Ni13-xAl8Cx (x = 0, 0.25, 0.5, and 1.5 at.%) by a vacuum arc melting. The carbon doping effect on the phase composition, mechanical properties, and wear behavior was studied. Fe61.5 Cr17.5Ni13Al8 alloy microstructure was a heterogeneous structure comprising FCC, BCC, and B2 phases. By introducing carbon into Fe61.5 Cr17.5Ni13-xAl8Cx (x = 0, 0.25, 0.5, and 1.5 at.%), the BCC phase fraction increased with decreasing FCC phase during annealing, accompanied by the formation of M23C6-like carbides at temperatures of 800 °C and 900 °C. The carbon-doped HEAs exhibited enhanced mechanical properties compared to the carbon-free HEAs, including higher tensile strength (1580 MPa), notable ductility (∼20 %), reduced friction coefficient (0.50), and improved wear resistance. Among the carbon-doped HEAs, the HEA with x = 0.5 at.% and annealed at 800 °C demonstrated exceptional wear resistance due to the compensations of attaining a balance between strength and elasticity.

Varying strain rates and elevated temperatures effects on the mechanical properties of AZ31B magnesium alloy

This study investigates the monotonic tensile behavior of magnesium (Mg) alloy AZ31B across a temperature range from ambient (25 °C) to elevated (up to 300 °C) with varying strain rates (SR) (1.5 × 10−2 to 1.5 × 10−4 s−1). Mechanical properties such as ultimate tensile strength ( σu), tensile yield strength ( σy), strain to failure ( εf), plastic anisotropy ( r-value), strain rate sensitivity ( m) and strain hardening exponent ( n) were investigated in this study for these strain rates. As the temperature increased from 25 to 300 °C, the following changes in mechanical properties were observed: the yield strength ( σy) decreased by 84.50%, the ultimate tensile strength ( σu) decreased by 87%, the modulus of elasticity ( E) decreased by 63.0%, and the elongation increased by 72.0%. The reduction factors (RF) were proposed for the above-mentioned mechanical properties for varying temperature ranges. The impact of varying temperatures and strain rates on fracture surfaces was investigated using field emission scanning electron microscopy (FE-SEM). The results revealed the presence of tenacity nets, cleavage patterns, and an increasing number of dimples as temperatures increased.

Bond-Based Peridynamic Model for Tensile Deformation and Fracture of Polycarbonate and Polypropylene

Fracture mechanics has been a crucial aspect in the field of engineering science as technologies are rapidly growing nowadays. Various numerical methods have been developed to analyze fracture behaviour in different types of materials used in industries. Meanwhile, the application of polymers garners attention worldwide due to outstanding characteristics such as good strength, lightweight, and high temperature resistance, exemplified by polymers like polycarbonate (PC) and polypropylene (PP). Hence, failure aspects of such materials must be taken into consideration when conditions arise that may lead to failure, such as high-load impact, fatigue, and extreme temperatures. In this study, a bond-based Peridynamic model (PD) for the tensile behaviour, including fracture, of polymers has been developed. The PD model is constructed using the Centos software and encompasses both brittle and ductile fracture behaviours. Numerical results, including crack propagation, damage zone, and force-extension curves of notched specimens, are validated by comparison with experimental results of PC and PP. Through the validation process, PC specimens exhibit a difference percentage range for maximum load and rupture extension of 2.9% to 18.8% and 2.4% to 4.6%, respectively. PP specimens show a difference percentage range for maximum load and rupture extension of 31.2% to 43.5% and 0.9% to 30%, respectively. Consequently, the validation results indicate that the PD model for brittle specimens aligns more closely with experimental data compared to the PD model for ductile specimens.

Load transfer behavior in semisolid formed hypereutectic Al-Fe-based alloys during tensile creep

The tensile creep behavior of semisolid formed hypereutectic Al-Fe-based alloys (for short Al-5Fe-based alloys) is investigated at temperatures ranging from 200 °C to 350 °C and stresses ranging from 30 MPa to 100 MPa. A power law model incorporating the “generalized” load transfer term is employed to rationalize creep data for Al-5Fe-based alloys with respect to that of the pure aluminum as a corresponding matrix without second phases and/or reinforcements. This expression proves more suitable for describing the creep characteristics of Al-5Fe-based alloys. The AlFe phases in the alloys transfer and bear load, and have no interaction with dislocations practically, which is the main reason for the creep strengthening of Al-5Fe-based alloys. The results obtained in this study are validated by creep data for Al-Fe alloys obtained by a thorough literature review.

Mechanical properties and microscopic analysis of water-castable engineered cementitious composites (WECC)

To address the difficulties in repairing underwater concrete panels and the unsatisfactory results of existing repair methods and materials, water-castable engineered cementitious composites (WECC) are developed. The effects of flocculant dosage on anti-dispersibility, fluidity, tensile behaviors, flexural behaviors, and fracture behaviors were investigated. XRD, MIP, and SEM tests were conducted on the WECC. Excellent tensile properties, flexural energy absorption capacity, and crack resistance are exhibited by the WECC. The increase in flocculant dosage decreases the dispersion degree during the underwater casting process of WECC, reduces the early hydration reaction rate, increases the internal porosity, resulting in a decrease in various mechanical properties. By comparing the tensile properties of WECC and WECC(L), while integrating microscopic analysis results, the performance loss mechanism of WECC and the tensile constitutive model have been identified. Additionally, the effects of (washed sea sand) sand-colloid ratio on workability and mechanical properties were investigated. When the sand-colloid ratio is 0.25, a higher level of compatibility between the fibers and the matrix is observed, and good ductility is demonstrated. Considering various performance factors, two mixed proportions have been established. The time, resources, and labor required for the repair process can be significantly reduced by using WECC for repairing underwater components, and the hydraulic structures can operate normally. The externally generated complex stress can be effectively released by WECC. The tested results provide crucial references for the underwater reinforcement of WECC.

Mechanical behavior of Al /AL2O3p-SiCp hybrid composite fabricated by hot pressing method

Hybrid particulate metal matrix composites with specific strength can be used in various applications. The mechanical properties of these composites can be improved by correctly choosing the type, volume fraction, size, and distribution of reinforcements and metal matrix. In this research, to make Al/Al2O3-SiC hybrid composites, aluminum chips were prepared by machining, and then the chips were coated with Al2O3 and SiC reinforcements by suspension method. For composite making, first, aluminum-coated chips were molded inside a steel mold and after heat treatment at 645 °C for 2 h the chips were hot pressed. The microstructure of the fabricated composites was examined by optical and SEM microscope, and then compression and tensile strength behavior were studied. The microstructural results showed a sound composite without any porosities and cracks. The hybrid composite with 12 wt% reinforcements showed high compressive strength (370 MPa).

Tensile mechanical behavior of functionally graded NiTi alloy manufactured via laser powder bed fusion

Laser powder bed fusion (LPBF) offers the potential to modify the characteristics of NiTi alloys, allowing for the creation of bespoke solutions tailored to specific applications. In this study, four functionally graded NiTi alloys with varying martensite/austenite distributions were designed and manufactured. A comprehensive investigation was conducted into the local microstructure, phase transformation behaviour, and tensile mechanical behaviour. The findings illustrate that, in comparison to homogeneous NiTi, gradient NiTi displays a propensity for preferential deformation within the martensitic region, attributable to the presence of localised performance variations. Gradient NiTi exhibits evident strain hardening and a wider range of plateau stress due to its intricate step-by-step phase transformation behaviour. The strain gradient strengthening near the interface between martensite and austenite endows gradient NiTi with enhanced fracture strength. Furthermore, while ensuring a discernible gradient in strain, the design of the interface with narrow spacing and parallel to the tensile direction can effectively enhance the mechanical properties of gradient NiTi. This study validates that gradient design based on LPBF is an effective approach for controlling the macroscopic mechanical behavior of NiTi alloy.

High-temperature tensile behaviors of an ultra-strong aluminum alloy fabricated by additive manufacturing

Additively manufactured (AM) Al alloys have widespread applications. Their high-temperature mechanical behaviors are also of significant interest. In this study, we investigated the microstructure and mechanical behavior of Al-2Ti-2Fe-2Co-2Ni (at%) alloy processed by laser powder bed fusion. The as-printed alloy contains a distinctive heterogeneous microstructure characterized by nanoscale intermetallic lamellae arranged in rosette patterns in the Al matrix. Notably, this alloy exhibits high tensile strength and thermal stability up to 500 °C as revealed by in-situ tension studies in a scanning electron microscope. The enhanced high temperature performance can be attributed to a substantial volume fraction of well-dispersed, nanoscale stable intermetallic particles.

Low temperature tensile behavior and microstructure analysis of copper containing antibacterial stainless steel

Using Shimadzu AGS-100KN universal tensile testing machine, tensile tests were conducted on copper containing antibacterial stainless steel at 25 °C, −20 °C, −60 °C, −100 °C, and −140 °C. The fracture morphology and microstructure evolution of the material were then analyzed using various techniques including scanning electron microscopy (SEM), electron backscatter diffraction (EBSD), X-ray diffraction (XRD), and transmission electron microscopy (TEM) techniques. The experimental findings showed that with the decrease of deformation temperature, the ultimate tensile strength(UTS) increased by about 49.7 %, the yield strength (YS) increased by about 35.5 %, and the elongation(EI) decreased by about 27.3 %, showed obvious low temperature strengthening effect. The High-angle grain boundaries (HAGBs) increased with decreasing temperature, while low-angle grain boundaries (LAGBs) decreased. The plasticity gradually decreased and the strength gradually increased, resulting in an increase in its ability to resist deformation. The number of precipitated phases gradually increased, and the size also gradually becomes larger, and the interaction between the diffusely distributed precipitated phases and dislocations led to precipitation strengthening. With the decrease of temperature, the stacking fault energy gradually decreased, the SFE was 21.26 mJ/m2 at the temperature of −140 °C. The main plastic deformation mechanism of copper-containing austenitic stainless steel in the low-temperature tensile process was transformed from deformation twins to strain-induced martensitic phase transformation.

Void-induced mechanisms in tensile behavior of nickel-based single crystal superalloys

Void defects significantly impact the tensile properties of nickel-based single crystal superalloys. In this work, the dynamic response of void-included nickel-based single crystal superalloys under tensile loading was studied using molecular dynamics method. The effects of porosity and void size on the tensile behavior and the evolution of internal defects were explored from a microscopic perspective. The results indicate that the presence of voids promotes the development of internal dislocation defects and atomic phase transitions, especially in the initial stage of plastic deformation. The tensile strength decreases with increasing porosity. Plastic deformation and atomic phase transitions typically initiate between voids and continue until complete fracture, with shear strains and dislocation defects continuously concentrating around the voids. Notably, some HCP defect atoms distant from voids revert to FCC phase atoms during the tensile process, leading to a decrease in dislocation density. Additionally, the mode of fracture in the porous model is shear fracture, with shear strain and dislocation defects remaining at the fracture surface after complete fracture. The effects of void size on the tensile strength are relatively small. As the void size decreases, the shear strain bands in the models become more regular and the dislocation density decreases. However, the impact of small-sized voids on the material becomes increasingly evident with further stretching.

On the strain rate-dependent mechanical behavior of PE separator for lithium-ion batteries

The separator is a critical component for ensuring electrochemical cycling performance and preventing internal short circuits in lithium-ion batteries. For the collision safety of lithium-ion batteries, understanding the rate-dependent mechanical behavior of the separator is essential for battery impact modeling and safety prediction. This study conducts a comprehensive experimental investigation into the strain rate–dependent tensile/compressive behavior and failure mechanism of the polyethylene (PE) separator under quasi-static and dynamic conditions. The combination of deformation images recorded by cameras and post-mortem characterization using SEM was employed to clarify the rate-dependent deformation and fracture mechanism of the separator under both tensile and compressive loading. The experimental results demonstrate a significant strain rate effect on the tensile/compressive mechanical properties and damage/failure behavior of the separator. Furthermore, the effect of the strain rate on the mechanical properties, including the tensile strength, tensile fracture strain, tensile elastic modulus, compressive modulus, yield stress and yield strain of separator, was analyzed and discussed. A significant strain rate-dependent tensile damage and fracture behavior of the separator was observed, where the fracture site exhibited an obvious phase transition and skeletal lamella fracture under extremely high strain rate tensile loading. The separator underwent severe damage under dynamic compressive conditions. The results of this study provide an important basis for the establishment of rate-dependent safety criterion and short circuit prediction of lithium-ion batteries under impact loading, and shed light on understanding separator failure-induced short circuit issues in battery collision safety scenarios.