Temperature Rise Values Research Articles

Comparisons of computer simulations and experimental data for capacitive hyperthermia using different split-phantoms

Introduction Several positive clinical trials have demonstrated that capacitive hyperthermia (CHT) improves the effectiveness of radiation therapy for the treatment of various cancer entities. However, the ability of CHT to induce significant heating throughout the body is under debate. Objectives To perform a pilot study involving comparisons of computer simulations and experimental data using different split-phantoms to validate hyperthermia treatment modeling for pre-planning for a clinical CHT system and to investigate the feasibility of split-phantom measurements in capacitive hyperthermia. Materials and methods The CHT system EHY-2030 (Oncotherm, Budapest, Hungary) was used. The system provides two electrode sizes, but only the smaller electrode, indicated as D200 electrode, was investigated in this pilot study. Horizontally and vertically splittable, different multi-slice phantoms with dielectric material properties simulating muscle and electrically low conductive fat were produced and heated. During the heating procedure, temperature-time curves were measured, and thermal images were captured. Specific absorption rate values were derived from the temperature rise (TR) values. Concomitantly, computer field simulations utilizing a detailed CAD-based model of the CHT system were performed using the simulation platform Sim4Life and compared with measurements. Results For the investigated electrode D200 the system power of 75 W was applied, which is half of the maximum power of 150 W and lies in the range of usual values for this electrode applied in patient treatments in our clinic. For 75 W, a heating of 3.6 °C in 6 min in a depth of 1 cm in an agar-based, muscle tissue-equivalent phantom was achieved. The addition of a 1 cm thick, synthetic, low dielectric fat layer reduced the TR up until a depth of 8.5 cm by on average around 38% (from 8.5 cm onwards the absolute local TR is similar, deviations are ≤0.1 °C). In terms of point-to-point absolute SAR comparison (without any normalization), up to a depth of 11 cm in the phantoms central vertical plot, the simulation differs from the measured TR points by on average 25% (ranging from 7% to 36%) for the homogeneous phantom and by on average 43% (ranging from 26% to 60%) for the inhomogeneous phantom. Conclusion Computer simulations and experimental data were compared for the CHT system EHY-2030 using the D200 electrode, applying a thermal imaging technique for different vertically splittable phantoms. This pilot study data can be used as a guidance regarding the expected heating for this commonly used electrode size but also to further elucidate the significance of non-thermal anticancer effects. Further studies are needed for different sizes and geometries of electrodes and phantoms.

Simulation and experimental analysis of dynamic thermal rise relaxation characteristics for dry-type distribution transformer

Abstract The temperature distribution characteristics of dry-type distribution transformers reflect their overall performance and quality. Distribution transformer daily load changes dramatically, its temperature fluctuates within a certain range. However, most of the research results on transformer temperature rise focus on the steady-state temperature characteristics of transformers, and lack of research related to dynamic temperature rise characteristics. This paper carries out a multi-physics coupling simulation and experimental verification of the dynamic temperature rise relaxation characteristics. The simulation uses the “electromagnetic-flow-thermal” multi-physics coupling analysis method to simulate the steady-state temperature rise characteristics and dynamic temperature rise relaxation characteristics of windings under different load rates. Then, this paper also explores the correlation between the dynamic temperature rise relaxation characteristics and load rate at the typical positions of high-voltage windings and low-voltage windings. The results show that the temperature rise of the winding shows the law of increasing the saturation index function with the increase of the load application time at any load rate. A quantitative characterization model of dynamic temperature rise relaxation behavior at different positions of transformer windings is constructed. It is found that the steady-state temperature rise value of different parts of the winding increases regularly as a power function with the increase of load rate, while the constant value of dynamic temperature rise relaxation time in different parts of the winding decreases as a power function with the increase of load rate. The verification results of the quantitative characterization model of dynamic temperature rise relaxation behavior show that the maximum error of the measured and theoretical steady-state temperature rise value is only 1.56 K, and the maximum error of the constant value of dynamic temperature rise relaxation time is only 0.082 h. These findings provide valuable insights into the performance and quality of dry-type distribution transformers, and can help improve their design and operation for better efficiency and safety.

Effect of Graphene Oxide on the Electrothermal and Pressure-Sensitive Properties of Carbon Fiber Cementitious Composites.

The application of carbon fiber in cement matrix has some disadvantages, such as poor dispersion and poor interfacial adhesion. In order to improve the interaction between carbon fiber and cement matrix and improve the properties of cement-based composites, carbon fiber was modified by electrophoretic deposition of nano-graphene oxide (GO). In this paper, the effects of doping CF into the cement matrix before and after GO modification are studied comparatively in terms of electrical conductivity, electrothermal warming effect, and pressure-sensitive properties of the cement matrix. It was found that the GO-modified CF reduces both the electrical resistivity of cementitious composites and the required level of fiber incorporation compared to CF. The percolation threshold is 0.7 wt% for CF and 0.5 wt% for GO-CF. The GO-modified CF is more effective than CF as a conductive filler to enhance the electrothermal warming performance of the cement matrix. When the GO-CF doping rate is 0.5%, the specimen temperature increases most rapidly, and the temperature rise value reaches a maximum of up to 30.45 °C, which is twice that of the CF group. When the fiber content is 0.7%, the pressure sensitivity of the sample was the best. When the fiber content is 0.5%, GO-CF can improve the pressure sensitivity of cement mortar specimens, and increase the resistance change rate of the cement mortar specimens by 5.7%.

Effect of channel depth ratio and absorber plate configuration on performance of a solar air heater

An experimental evaluation of the effect of channel depth ratio and absorber plate configuration on the performance of a baffled counter flow double-pass solar air heater (BCDSAH) is main objective of current work. The BCDSAH was constructed so as to permit adjustments of channel depth ratio (CDR) to 2, 3 and 4. During experimentation, the lower channel depth was kept at 50 mm while the upper channel depth was adjusted to 100 mm, 150 mm and 200 mm, yielding various channel depth ratios. The assessments were conducted for three configurations of absorber plate: (i) flat absorber plate, (ii) baffled absorber plate and (iii) baffled absorber plate with phase change material (PCM). The performance of the BCDSAH was evaluated at an air mass flow rate of 0.07 kg/s for temperature rise, useful heat gain (UHG), energy efficiency, and exergy efficiency. For CDR = 2 and a baffled absorber plate with PCM, the obtained average values of temperature rise, UHG, energy efficiency and exergy efficiency were 15.3 °C, 1075.2 W, 76.2 % and 2.7 % respectively. For the baffled absorber plate with PCM, increases of 8.5 %, 9.4 %, 10.1 % and 10.9 % were obtained in temperature rise, UHG, energy efficiency and exergy efficiency respectively for CDR = 2 compared to CDR = 4. Finally, a value of CDR = 2 and a baffled absorber plate with PCM are suitable for applications like drying of agricultural products and space heating.

Investigating temperature rise dynamics at hot-spots within dry-Type transformer windings: A comparative analysis across varied loading rates and an extrapolative computational model

The dynamic temperature data of a transformer can be utilized to accurately assess its load capability and operational longevity. This paper presents a study on the temperature rise characteristics of hot-spots in dry-type transformer windings and develops a extrapolative computational model based on various load rates, utilizing the results of transformer temperature rise tests. Firstly, the dynamic temperature rise characteristics of B-phase low-voltage (LV) winding and high-voltage (HV) winding hot-spot, along with its correlation calculation model with varying load rates, were determined based on the results of temperature rise tests. Subsequently, an extrapolative computational model for the temperature rise of the winding hot-spot, utilizing a three-section continuous load application approach, was proposed employing the lumped parameter method. The validity of this model was confirmed through verification. Lastly, a temperature rise test was conducted on another dry-type transformer to validate the universality of the model. Finally, a different dry-type transformer is chosen, and a temperature rise test is conducted to confirm the general applicability of the model. The results indicate that the calculation model for the hot-spot temperature rise of the winding under three consecutive loads is associated with the dynamic temperature rise pattern of the hot-spot of the winding between the temperature rise test with a small load rate and the temperature rise test with a large load rate. The maximum deviation between the hot-spot temperature rise test of the winding of SCB14-800/10-NX2 transformer and the results of the steady-state temperature rise value calculation is only 1.3 K, with a maximum error of the time constant value of the temperature rise being only 0.05 h. Similarly, the maximum deviation of the steady-state temperature rise value obtained from the hot-spot temperature rise test and the extrapolative computation of SCB-1250kVA/10 kV transformer winding is only 2.03 K, with a maximum error of the temperature rise time constant value being only 0.09 h. The extrapolative computational model proposed in this study conducts the temperature rise test under a small load rate instead of a large load rate, addressing the industry challenge of the challenging implementation of transformer on-site temperature rise tests and high power loss. This approach enhances inspection efficiency.

Characteristics of Insulating Panels Realised from Coconut Palm Fibres for Low-Temperature Thermal Insulation

In recent years, there has been growing interest in issues relating to pollution and energy consumption, and the resulting regulations have led the construction sector to focus on thermal insulation. The application of bio-based insulation materials can help to minimise the environmental impact of buildings by reducing energy demand both during construction and over the lifetime of the building. Agroforestry biomass plays an interesting role, as its use can reduce greenhouse gas emissions. The aim of this work is to produce insulating panels from agroforestry by-products for low-temperature thermal insulation applications. The insulating panels in this study are produced from coconut palm fibres and their thermophysical properties are determined. They were produced using a human-motricity press and the temperature rise was controlled using the hot-tape method. Characteristics such as calorific value and modelling of temperature rise as a function of time to calculate thermal conductivity, thermal effusivity and diffusivity were determined. The calorific value varies from 3668.0 to 4135.0 and from 3742.0 to 4186.0 cal.g-1 when the moisture content is 11.28 and 10.61%, respectively. The thermal conductivity, effusivity and thermal diffusivity are 0.4 W.m-1.K-1, 760.30 J.m-2.°C-1.s-1/2 and 2.73.10-7 m.s-1, respectively. In view of these results, coconut fibre represents a potential precursor to produce insulating panels.

Experimental and Theoretical Investigation of Longitudinal Temperature Attenuation and Smoke Movement in Urban Utility Tunnel Fires

The urban utility tunnel is an indispensable part of modern engineering construction. However, the fire risk cannot be ignored due to the narrow space and limited ventilation of the utility tunnel. A study of smoke filling is performed in a 1/8-scaled utility tunnel (25 m × 0.5 m × 0.45 m). Five heat release rates (5, 10, 15, 20 and 25 kW) and four positions of fire sources are used for tests. The initial position of the one-dimensional smoke movement of strong plume is determined. Based on the traditional model, the longitudinal temperature attenuation model of tunnel smoke is established with consideration of radiation and convection heat losses. The theoretical value of the longitudinal temperature rise of smoke is in good agreement with the experimental value. A one-dimensional spreading velocity model is established that coincides well with the experimental value, and the relative error is less than 20%. The spreading velocity of smoke is increased by the heat release rate. The velocity of the smoke spreading at the near end is smaller than that at the center, due to the long spreading route. The current conclusions disclosed in this study provide important guidance for the ventilation design of utility tunnels for fire smoke scenarios.

Limiting Temperature Rise in Cochlear Implantation Bone Drilling: A Novel Approach.

In the process of cochlear implantation surgery, it is crucial to develop a method to control the temperature during the drilling of the implant channel since high temperatures can result in damage to bone and nerve tissue. This paper simplified the traditional point heat source temperature rise model and proposed a novel extreme peck drilling model to quantitatively calculate the maximum temperature rise value. It is also innovatively introduced a new method for calculating the best peck drilling duty cycle to strictly control the maximum temperature rise value. Besides, the neural network is trained with virtual data to identify two important thermal parameters in the temperature rise model. In the experiment of epoxy resin and temporal bone, the difference between predicted maximum temperature and actual maximum temperature was less than 1.5 °C, and the error rate was less than 10%. And the error source was analyzed by variational mode decomposition, along with discussion of potential solutions. In the temperature control experiment, the model successfully controlled the maximum temperature rise within 10 °C.For cochlear implantation surgery, we also divide the implantation channel into different stages based on the bone density in CT images to identify thermal parameters and calculate drilling strategies. This method provides a new strategy for accurate and effective control of borehole heat generation. These achievements provide new ideas and directions for research in cochlear implantation surgery and related fields, and are expected to have extensive application in medical practice.

Calculation Method for the Transient Hot-Spot Temperature Rise of Oil-Immersed Bushing in High-Speed Railway

Traction oil-immersed bushing is the only channel for connecting the high-speed railway system with the external power grid, and its transient hot spot is one of the most important factors reflecting its operation status. Since the traction load of a high-speed railway has obvious impulse characteristics, the existing calculation method for bushing given in IEEE Std C57.19-100™-2012 is incompatible because it is designed for steady electrical loads. Thus, in this paper, the equivalent hot spot temperature rise of the bushing under varying traction loads is calculated by the traction parameters (i.e., operating time <italic xmlns:mml="http://www.w3.org/1998/Math/MathML" xmlns:xlink="http://www.w3.org/1999/xlink">T_ot</i> , interval time <italic xmlns:mml="http://www.w3.org/1998/Math/MathML" xmlns:xlink="http://www.w3.org/1999/xlink">T_it</i> , and per unit transient traction current <italic xmlns:mml="http://www.w3.org/1998/Math/MathML" xmlns:xlink="http://www.w3.org/1999/xlink">I_tc</i> ). Then, the difference value of transient hot spot temperature rise is modified by analyzing the change of transient hot spot temperature rise under varying traction loads. Finally, a calculation method is proposed for the transient hot spot temperature rise of the oil-immersed bushing in high-speed railway under different traction loads. A case study of a 110 kV oil-immersed bushing shows that the proposed method is speedy and accurate.

Design and Optimization of an Interior Permanent-Magnet Synchronous Motor for Aircraft Drive Application

The torque performance of the interior permanent-magnet synchronous motor (IPMSM) must be further improved to satisfy the growing demand of aircraft drive application. To this end, this article focuses on the design optimization of the IPMSM structure in the aircraft drive systems to improve the torque density and reduce the torque ripple. A special fractional-slot winding and ∇-type magnetic-pole rotor topology are proposed as the optimized IPMSM structure compared with the structure of an existing motor. The simulations of the original and optimized structures at different current values reveal the variance of the torque in the average and ripple, mechanical and external characteristics, efficiency and steady-state temperature. The performance of an optimized prototype is analyzed by experimental testing, and the results show that an optimized motor has a higher torque density and lower torque ripple than the original one at the same speed and rated power, but it also has a higher temperature rise. However, the temperature rise value is acceptable in the experimental testing condition, so the validity of the design optimization method for the proposed structure is verified.

Optimized selection of neodymium laser parameters for successful enlarged veins treatment.

Full clearance and no side effects method of treating enlarged veins was successfully accomplished by one laser session. This is the ambition and dream of both dermatologists and patients. Most vascularity treatment protocols had shown some unpleasant adverse effects. The purpose of the present work is to work out, in advance, the accurate dose of laser pulse duration and fluence in order to treat varicose veins in the face, arms and legs with no adverse effects. This mission required the calculation of the exact rise in temperature of the enlarged vein; prior to laser treatment. These pre-calculated temperature rise values were tested on 20 subjects in order to have the best clinical outcomes; using fundamental frequency (1064nm) pulsed Nd: YAG laser. This work necessitated the use of pulse length (15-30ms), spot size (3, 5mm), fluence (110-190J/cm2) and skin cooling temperature (3-18°C). Cooling of the skin before and after the treatment was needed to guarantee ultimate impactful results without side effects.

Enhanced therapeutic action of Trastuzumab loaded ZnxMn1−xFe2O4 nanoparticles using a pre-treatment step for hyperthermia treatment of HER2+ breast cancer

In this study, Ferrites (Fe3O4, MnFe2O4, ZnFe2O4) and different stoichiometric ratios of ZnxMn1−xFe2O4 (x = 0.2, 0.4, 0.6, and 0.8) nanoparticles (<15 nm) were synthesized by microwave-assisted method and optimised for hyperthermia studies. The selection of the optimised variant of ferrite i.e. Zn0.4Mn0.6Fe2O4 was found to be the best variant based on VSM (38.14 emu g−1) hyperthermia-based temperature rise (maximum ΔT of 38 °C), SAR and ILP values. Trastuzumab, which is known to bind with HER2 receptors of breast cancer was chemically tethered onto Zn0.4Mn0.6Fe2O4 nanoparticles through EDC/NHS coupling with a loading efficiency of 80%. The attached Trastuzumab aided during the pre-treatment step by aiding in the internalisation of Zn0.4Mn0.6Fe2O4 nanoparticles, with cellular uptake of 11% in SK-BR-3 (cancerous HER2+) cells compared to ∼5% for MDA-MB-231 (cancerous HER2-) and RPE-1 (non-cancerous) cells. In the presence of a hyperthermia trigger for 15 mins, ZnxMn1−xFe2O4 -Trastuzumab formulation had a maximum therapeutic effect by reducing the SK-BR-3 cell viability to 14% without adversely affecting the RPE-1 cells. The mechanism of ZnxMn1−xFe2O4-Trastuzumab combination was examined using an internalisation study, MTT-based viability, proliferation study, and ROS generation assay. By utilizing both Trastuzumab and hyperthermia, we achieve their synergistic anticancer properties while minimizing the drug requirement and reducing any effect on non-cancerous cells.

Real-time multispectral transmission of hard tooth tissues and dental composites with their heating.

The composites tested were: Filtek Universal Restorative (FUR), Filtek One Bulk Fill (FBF), Tetric EvoCeram (TEC), Tetric Bulk Fill (TBF) and Tetric PowerFill (TPF). The new LCU Pinkwave (a four-wavelength source manufactured by Vista Apex, USA) was placed either centrally or eccentrically for 3mm above the sample. A Fiber spectrometer detected irradiation and Infrared Thermal camera polymerization temperatures. All eccentric LCU positions significantly weaken transmitted spectra for all composites in both thickness, jeopardizing Blue light. The LCU position did not affect transmitted irradiation for tooth tissues. The reduction in wavelength intensity when penetrating through thicker compared to thinner composite samples was 62%, 50% and 31% for Blue, NIR and Red, respectively, and 90%, 50% and 35% for tooth tissue samples, respectively. The temperature of bulk fill composites with additional photoinitiators rises faster. Eccentric LCU positions cause a significant decrease in both speed and the maximal value of temperature rise. Red and NIR irradiations contribute to the polymerization temperature. Tested LCU source cause considerable inhomogeneity in the emitted and transmitted spectra. Tooth tissues homogenize irradiation, but drastically attenuates it. Red light has better potential than Blue light concerning penetration and could be further investigated as the wavelength for activation of an adjusted photoinitiator.

Effect of Hygrothermal Loads on the Nonlinear Vibration of Porous Bi-Directional Functionally Graded Beams Placed on an Elastic Foundation

In this study, we investigated the effect of hygrothermal loads on the nonlinear free vibrations of a porous bi-directional functionally graded Timoshenko beam with a Winkler–Pasternak foundation. The corresponding governing equations were established according to Hamilton’s principle and von Kármán nonlinearity assumption. Using the differential quadrature and iterative methods, the nonlinear fundamental frequencies were determined. A numerical example was presented, and we showed that the discretization of nonlinear items considerably decreased the number of iterations. A series of parametric studies were performed, and we determined that (1) all the vibration mode shapes were significantly affected by the axial functionally graded index, while they were almost unchanged by the thickness-wise functionally graded index. Moreover, compared to the thickness-wise graded index, the axial functionally graded index played a more important role in the higher-order mode shapes. (2) The geometric nonlinearity considerably influenced the critical temperature rise value of the beams. Increasing the maximum deflection value increased the critical temperature rise value. (3) The influence of increase in temperature and moisture on the nonlinear fundamental frequency became stronger with increase in the functionally graded index, but it weakened with increase in the maximum deflection value.

Thermal decomposition characteristics and thermal safety performance evaluation of HAN-based propellant under different external environmental stimulations

This research aims to investigate thermal characteristics and assess thermal hazards of hydroxylamine nitrate (HAN)-based liquid propellant using a combination of accelerating rate calorimeter and high-pressure differential scanning calorimetry. Adiabatic experiments revealed that the exothermic reaction initiated at 115.7 °C and a rise sharply was at 128.4 °C with a maximum self-heating rate of 164.3 °C/min and the exothermic event was accompanied by a pressure rise of 3.7 bar in 0.03s. The corrected values of adiabatic temperature rise and time to maximum rate were 605.6 °C and 1.46 min, which confirms the vulnerability of the propellant to undergo a catastrophic explosion. To prevent thermal loss prevention accidents, time to maximum rate was obtained as 24 h under 111.3 °C. The apparent activation energy calculated decreased greatly with the increase of storage temperature from 25 °C to 45 °C, and so did the thermal explosion temperature (Tb) and self-accelerating decomposition temperature (TSADT). Additionally, the linear relationship between Ea and T was E = 991.7–2.7904T. The reliability of TSADT prediction was validated through slow cook-off test. Furthermore, the propellant exhibited more violent thermal decomposition under high pressure, resulting in a higher peak power. The thermokinetic parameters related to this phenomenon were identified, specifically at pressure of 4.0 MPa.

Dynamic impact tests and temperature rise induced damage constitutive model of ice-rich frozen sandy soil

In this study, a soil-ice particle mixing method was used to prepare ice-rich frozen sandy soil specimens. Subsequently, the mechanical behaviors of ice-rich frozen sandy soil with a wide range of total moisture contents (15%–150%) were studied at three negative temperatures (−5, −10, and −15 °C) under the impact pressures from 0.2 MPa to 0.4 MPa. The melting of ice particles caused by the rise in temperature of frozen soil specimens was identified as temperature damage. Moreover, damage mechanism of ice-rich sandy frozen soil specimen during failure process was considered as the combined action of crack propagation and temperature rise. The analysis of the relationship between temperature rise value and dynamic strain was then calculated based on the heat conduction theory. Additionally, the phase transition equilibrium between unfrozen water and effective ice was used to determine the variation in ice volume content as the temperature rises, and the temperature damage variable was defined according to the reduction of dynamic elasticity modulus of ice-rich frozen sandy soil. Lastly, the compound damage variable was deduced and considered in the damage constitutive model. Accordingly, the theoretical and test data were compared to determine the model parameters. The results of the curve comparison indicate that the proposed model is feasible and suitable to be applied to predict the dynamic mechanics of ice-rich frozen sandy soil.

A numerical method to solve structural dynamic response caused by cable failure

PurposeInstantaneous unloading with equal force is usually used to simulate the sudden failure of cables. This simulation method with equivalent force requires obtaining the magnitude and direction of the force for the failed cable in the normal state. It is difficult, however, to determine the magnitude or direction of the equivalent force when the shape of the cable is complex (space curve). This model of equivalent force may be difficult to establish. Thus, a numerical simulation method, the instantaneous temperature rise method, was proposed to address the dynamic response caused by failures of the cables with complex structural form.Design/methodology/approachThis method can instantly reduce the cable force to zero through the instantaneous temperature rise process of the cable. Combined with theoretical formula and finite element model, the numerical calculation principle and two key parameters (temperature rise value and temperature rise time) of this method were detailed. The validity of this approach was verified by comparing it with equivalent force models. Two cable-net case with saddle curved surfaces were presented. Their static failure behaviors were compared with the dynamic failure behaviors calculated by this method.FindingsThis simulation method can effectively address the structural dynamic response caused by cable failure and may be applied to all cable structures.Originality/valueAn instantaneous temperature rise method (ITRM) is proposed and verified. Its calculation theory is detailed. Two key parameters, temperature rise value and temperature rise time, of this method are discussed and the corresponding reference values are recommended.

Simulation Analysis of Stir Tool Wear Considering the Effect of Temperature Rise caused by Material Deformation on Flow Stress

Background: Wearing is a prominent problem in friction stir welding. The material flow stress equation is a key factor that decides the accuracy of the simulation of the wearing process. Objective: We aim to propose a material flow stress equation based on material true stress and true strain curve, which takes proper factors into account and leads to good accuracy in numerical simulation of stir tool wear. Methods: The value of the material temperature rise caused by the material deformation heat and the value of the effect caused by the temperature rise on flow stress was calculated, and the effect value was used to modify the material flow stress and the related curve, and then the modified flow stress equation was obtained. On this basis, the equation was used to simulate the stir tool wear, and the simulation results were compared with those results without considering the effect of temperature rise. Results &amp; Discussion: the wear amount of the stir needle when considering the effect of temperature rise is significantly less than that when the effect of temperature rise is not considered. Conclusion: In the simulation of the wear of the stir tool, it is necessary to adopt the modified flow stress equation considering the effect of temperature rise.

Thickness-Dependent Light Transmittance and Temperature Rise in Dual-Cure Bioactive and Light-Cure Bulk-Fill Composite Resins.

This study aimed to assess the light transmittance (T) and temperature increase through different increments of dual-cure bioactive bulk-fill restorative material (ACTIVA), light-cure bulk-fill, and conventional composite resin materials. Cylindrical specimens with a diameter of 8 mm and heights of 1, 2, 3, and 4 mm of ACTIVA, Tetric-N-Ceram bulk-fill (TBF), Filtek One bulk-fill (FBF), and Filtek Z250 (FZ) (n = 6 per group, 96 in total) were light-cured with a visible blue low-intensity light-emitting diode (LED) (650-800 mW/cm2 irradiance). T, and the temperature increase, were measured using an optical power meter and a digital thermometer during curing. The T mean values ranged between 0.012 and 0.239 (76.02 to 98.81% light attenuation), while the temperature rise mean values ranged between 9.02 and 20.80 °C. The parameters, including material type (partial eta squared (ηp2) = 0.284, p < 0.0001), thickness (ηp2 = 0.284, p < 0.0001), and their interaction (ηp2 = 0.185, p = 0.047), significantly affected the T values, whereas only the material type (ηp2 = 0.352, p = 0.047) affected the temperature rise values. The T and temperature rise mean values were highest in ACTIVA increments of 1-mm increments, in particular, showing the highest T mean values, followed by similar increments of TBF. A significantly higher T was found in 1-mm increments compared to thicker increments for all materials (p < 0.0001), and a significant positive correlation existed between T and temperature rise values (r = 0.348, p = 0.001). These findings show that the bioactive material ACTIVA and TBF allow for better T than the other materials, with ACTIVA recording a higher temperature rise. However, the large light attenuation observed for all materials, irrespective of thickness, suggests that curing in more than one location with a low-intensity LED is necessary to optimize the curing process. Furthermore, incremental filling of bulk-fill materials using a low intensity LED could be beneficial.

Preparation of cool composite pigment by the layer-by-layer assembling of phthalocyanine green on the surface of rutile TiO2

Purpose This study aims to fabricate a cool phthalocyanine green/TiO2 composite pigment (PGT) with high near-infrared (NIR) reflectance, good color performance and good heat-shielding performance under sunlight and infrared irradiation. Design/methodology/approach With the help of anionic and cationic polyelectrolytes, the PGT composite pigment was prepared using a layer-by-layer assembly method under wet ball milling. Based on the light reflectance properties and color performance tested by ultraviolet-visible-NIR spectrophotometer and colorimeter, the preparation conditions were optimized and the properties of PGT pigment with different assembly layers (PGT-1, PGT-3, PGT-5 and PGT-7) were compared. In addition, their heat-shielding performance was evaluated and compared by temperature rise value for their coating under sunlight and infrared irradiation. Findings The PGT pigment had a core/shell structure, and the PG thickness increased with the self-assembly layers, which made the PGT-3 and PGT-7 pigment show higher color purity and saturation than PGT-1 pigment. In addition, the PGT-3 and PGT-7 pigment showed 11%–16% lower light reflectance in the visible region. However, their light reflectance in the NIR region was similar. Under infrared irradiation the PGT-5 and PGT-7 pigment coating showed 1.1°C–3.4°C and 1.3°C–4.7°C lower temperature rise value than PGT-1 pigment coating and physical mixture pigment coating, respectively. And under sunlight the PGT-3 pigment coating showed 1.5–2.6°C lower temperature rise value than the physical mixture pigment coating. Originality/value The layer-by-layer assembling makes the core/shell PGT composite pigment possess low visible light reflectance, high NIR reflectance and good heat-shielding performance.