Strain Rate Sensitivity Index Research Articles

A New Approach to Characterize Superplastic Materials from Free-Forming Test and Inverse Analysis

For about 60 years, the aerospace industry has been strongly interested in superplastic forming processes to produce extremely light and complex-shaped components. Superplastic characteristics are found in lightweight metallic materials such as titanium-based, aluminum-based, and, more recently, magnesium-based alloys. Since the high ductility exhibited by superplastic materials is two orders of magnitude higher than that of conventional materials, complex-shaped components can be obtained. If made with conventional materials, they require expensive assembly operations. The behaviour of superplastic materials is summarized by a constitutive equation commonly obtained via tensile testing that subjects the tested material to a one-dimensional stress state. On the contrary, free-forming tests allows us to test the material by subjecting it to a stress state similar to that determined during a real superplastic-forming process. The aim of this work is to define the characteristic parameters of superplastic materials by free-forming tests. The behaviour of superplastic materials is commonly modelled using a power law which puts the material into a stress-to-strain-rate relationship. This law needs to identify two parameters characterizing superplastic materials: the strain rate sensitivity index and the strength coefficient. In this work, a new procedure is presented that implies the two material parameters vary with strain. It allows for a reduction in the number of constants needed to determine the material constitutive equation, thus requiring low simulation time compared to models that adopt the multiple-objective optimization based on genetic algorithms (GAs). It is more suitable to be used in the industrial field. Furthermore, the proposed procedure is compared with a conventional procedure which is also based on the inverse analysis carried out through the use of a finite element analysis. The results of the conventional procedure, based on the inverse analysis, which is conducted through the use of a finite element analysis, are used to calculate the material constants, and are compared with those coming from the procedure proposed in this work. The proposed procedure appears equally simple and gives more accurate results compared to the conventional procedure. In fact, the maximum percentage error, regarding the prediction of the forming times of a free-forming process, was reduced from 20% to 8%. The development of the proposed procedure, as well as the comparison of the results with a conventional procedure, required the development of an experimental activity. This activity consists of free-forming tests conducted at a constant pressure (the pressures employed vary from 0.2 to 0.4 MPa), at a temperature of 753 K, and on circular sheets (thickness 1.0 mm and radius 40 mm) in superplastic magnesium alloy AZ31.

Strain Rate Sensitivity of Low‐Temperature Superplastic Heterogeneous Medium‐Mn Steel Fabricated by a Novel High‐Ratio Differential Speed Rolling

In the present article, insights into the high‐temperature deformation behavior of medium‐Mn steel (MMS), which is prepared via high‐ratio differential speed rolling (HRDSR), are provided. Moreover, through innovative bidirectional jump experiments, variations in the strain rate sensitivity index m under various conditions are obtained. In the research findings, it is indicated that an increase in strain rate (SR) leads to a hardening of the alloy. During high‐temperature deformation, the value of m decreases with the increase in SR, but the rate of decrease gradually slows down. Furthermore, the higher the temperature (T), the greater the impact of changes in SR on m. In addition, the change in deformation mechanism during deformation leads to microstructural changes, and under the main deformation mechanism of grain‐boundary sliding, m generally increases with strain. Interestingly, at a T of 760 °C, the material exhibits a strong texture with high orientation, resulting in larger m values and superior superplasticity (≈691%). This study not only enriches the research content of HRDSR but also has significant implications for the superplasticity research of MMS. Moreover, a reference is provided for the research of other superplastic materials.

The thermal deformation behavior and processing map of TC9 titanium alloy

This investigation delves into the thermal deformation behavior of TC9 titanium alloy. Compression tests at isothermal conditions were performed on a Gleeble thermal simulator under conditions spanning 700–1200 °C and strain rates of 0.001–1 s−1. The true stress-true strain curves indicated that stress increases with rising strain rate and decreasing temperatures. The softening mechanisms in the biphasic and monophasic regions were discussed. By correcting errors caused by friction, the strain-compensated Arrhenius-type constitutive equation, which accurately describes the flow behavior of TC9 titanium alloy, has been established. A processing map at a strain of 0.7 was constructed based on the power dissipation factor, revealing an unstable region at 700–800 °C/0.01–1 s−1 and 800–900 °C/0.1–1 s−1, where microcrack defects were observed, suggesting that processing should be avoided in this region. Efficiency values as high as 60–70 % indicate superplasticity deformation, with corresponding m values within this efficiency range of approximately 0.4–0.5, reaching the strain rate sensitivity index range of superplasticity titanium alloys. Tensile tests conducted at 900 °C and a deformation rate of 0.001 s−1 showed elongation exceeding 100 %. The sample compressed at 900 °C and 0.001 s−1 exhibits small grain size, uniform orientation, the lowest dislocation density, and a uniform two-phase mixture. These microstructural features indicate the material's good machinability.

Effect of friction stir processing on grain refinement and superplastic properties of binary Al-8 wt.% Si to Al-30 wt.% Si alloys

ABSTRACT As-cast binary Al–Si alloys containing ∼8, 12, 20, and 30 wt.% Si, representing the hypoeutectic, eutectic (12 wt.% Si), and hypereutectic compositions, were subjected to severe plastic deformation by friction stir processing (FSP) for grain refinement to 2.3–2.7 μm by dynamic recrystallization. Tensile tests conducted by differential strain rate test technique over the strain rates of 10−4 – 10−2 s−1 and test temperatures in the range of ∼840–530 K led to strain rate sensitivity index (m) varying from ∼0.04 to 0.40 depending on temperature, strain rate, and alloy composition. The constant initial strain rate tests conducted at 10−4 s−1 and 840 K exhibited a maximum elongation of 250% in the hypereutectic Al–20Si alloy, but the same increased linearly with m irrespective of alloy composition. Generally, with increasing Si content, the activation energy for deformation increased from 104.7 ± 14.4 kJ/mol for eutectic Al–12Si to 310.4 ± 32.3 kJ/mol for hypereutectic Al–30Si, which increased further to 572 ± 148 kJ/mol over the higher temperature range of 840–800 K. Analysis of observed deformation and microstructure behaviour supports the occurrence of superplasticity, whereby the accommodation of grain boundary sliding by grain boundary migration led to enhanced grain growth or else the local high-stress concentration at the particle-matrix interface led to cavity formation. There was no evidence of dynamic recrystallization during high-temperature tensile deformation but the flow softening observed is ascribed to the occurrence of concurrent cavitation.

Characterize the high-temperature steady-state rheological behavior and Arrhenius activation of PEEK via strain rate jump tensile tests

Polyetheretherketone (PEEK) is a high-performance thermoplastic polymer with diverse industrial applications, such as aerospace, automotive, electronics, and medical devices. However, systematic research on its high-temperature rheological characteristics is inadequate. In this study, strain rate jump tensile tests were introduced to examine the steady-state rheology phenomena and strain rate sensitivity of PEEK at four different temperatures and nine different strain rates. Theoretical analysis based on the free volume theory and the Arrhenius law was also carried out to further analyze the transition of PEEK from Newtonian flow to non-Newtonian flow. Results indicate that PEEK materials exhibit a transition from Newtonian flow to non-Newtonian flow similar to metal materials at high temperatures. The transition point from Newtonian flow to non-Newtonian flow is marked by the emergence of steady-state rheology and its characteristic stress. Theoretical analysis demonstrates that the transition of PEEK is in accordance with the Arrhenius low. Moreover, its apparent activation energy (1.42 eV) is significantly lower than that of metal materials (5.28 eV), indicating a lower energy barrier and an easier transition. The strain rate sensitivity index correlates negatively with rising temperatures, especially at lower rates. This study enhances understanding of PEEK's rheological characteristics at high temperatures, aiding the development and application of high-performance thermoplastic materials.

The rheological behavior of brittle BMGs of Cu44.25Ag14.75Zr36Ti5 and Ti32.8Zr30.2Cu9Ni5.3Be22.7 in the supercooled liquid region

Bulk metallic glasses (BMGs) show limited plasticity at room temperature. However, BMGs usually exhibit superplasticity and high plastic forming ability in their supercooled liquid region (SLR). The rheological behavior of BMGs in SLR is vitally important to their thermoplastic forming process. In contrast to the ductile BMGs, thermoplastic deformation behavior of brittle BMGs is rarely reported. In present work, the rheological behavior of two brittle BMGs with high glass forming ability Cu44.25Ag14.75Zr36Ti5 and Ti32.8Zr30.2Cu9Ni5.3Be22.7 was investigated on Gleeble3500. The two BMGs can deform homogeneously depending on the temperature and strain rate. According to the high value of m (strain rate sensitivity index), which is the most important mechanical characteristic of a superplastic material, the two BMGs show superplasticity in their SLR with m ≥ 0.3. Based on the free volume model, their activation volumes are calculated as 0.263∼0.486 nm3 and 1.261∼1.650 nm3, indicating the minimum displacement clusters with average 26∼48 and 91∼127 atoms, for Cu44.25Ag14.75Zr36Ti5 and Ti32.8Zr30.2Cu9Ni5.3Be22.7, respectively. Thus, the two investigated brittle BMGs can be thermoplastic processed in the SLR and the deformation maps are given. BMG Cu44.25Ag14.75Zr36Ti5 shows better machinable property than Ti32.8Zr30.2Cu9Ni5.3Be22.7. Compared to the ductile BMGs, no Newtonian flow is found for the two investigated brittle BMGs.

A modified maxwell-pulse thermoplastic constitutive model of in-situ Ta-particle reinforced Zr-based bulk metallic glass composites

The impact of different Ta contents on the mechanical properties and thermoplastic forming ability of in-situ Ta-particle reinforced Zr–Cu–Al–Ni bulk metallic glass composites was studied. The composition (Zr55Cu30Al10Ni5)94Ta6 with the best comprehensive performance was chose for a systematic investigation into its thermoplastic behavior in the supercooled liquid region (SLR), with quantitative analysis conducted by the strain rate sensitivity index and activation volume. The steady-state flow stress and the stress overshoot intensity were augmented with deformation temperature decreasing, strain rate increasing, and the addition of the secondary phase, leading to a transition from Newtonian to non-Newtonian flow regime. The addition of the secondary phase deteriorated the rheological properties of the material. To solve the problem that the Maxwell-Pulse constitutive model showed an inability to accurately describe the steady-state flow process. A modified constitutive relationship, introducing the effect of the volume fraction of Ta particles on viscosity and elastic modulus in the steady-state flow process which was ignored in Maxwell-pulse model, was established. The fitting results of the true stress-strain curves of the modified Maxwell-pulse constitutive model were in better agreement with the experimental date than those of the Maxwell-pulse constitutive model, with higher prediction accuracy. The modified constitutive model well predicted the thermoplastic deformation behavior of (Zr55Cu30Al10Ni5)94Ta6. The influence mechanism of Ta particles on the flow behavior was explained that Ta particles increased the viscosity of amorphous matrix, thereby hindering its flow and ultimately leading to an increase in flow stress.

The transition of strain rate sensitivity induced by Fe solutes in electrodeposited nanocrystalline Ni–Fe alloy

A face-centered cubic nanocrystalline (NC) Ni–Fe alloy was fabricated by adjusting electrodeposition parameter. By evaluating the hardness of NC Ni–Fe via nanoindentation at the selected strain rates from 0.005 s−1 to 0.2 s−1, a transitional point of strain rate sensitivity index (m) was exhibited, contrary to the constant value that reported in other works. Based on X-ray diffraction and transmission electron microscopy analysis, which evidenced the apparent lattice expansion as much more Fe solutes dissolved in intragrain rather than grain boundary (GB), we attributed the unexpected enhancement of m value at lower strain rates to pronounced GB-mediated plasticity facilitated by residual dislocations near GBs, whilst the lower m value at higher strain rates mainly to the intragranular dislocation motions. This work contributes directly to understanding the profound effect of alloying on the mechanical behaviors of NC materials.

Experimental constitutive relationships for high-temperature deformation of as-cast Al–Si binary alloys

ABSTRACT As-cast binary Al–Si alloys containing ∼2 to 30 wt.% Si were deformed by differential strain rate and differential temperature test techniques at 600–840 K and strain rates 10−4–10−2 s−1 to find the parameters of the constitutive relationships for high-temperature deformation. The maximum strain rate sensitivity index (m) of flow stress was found to be 0.28 in the eutectic Al-12Si alloy. The Arrhenius plot for activation energy for deformation (Q) exhibits bilinear behaviour, with Q being greater at higher test temperatures than at lower temperatures. The magnitude of Q varies as a function of Si content: 95.7 ± 9.8 kJ/mol for Al-2Si to 311.4 ± 98.1 kJ/mol for Al-12Si alloy. Also, the constant initial strain rate tests performed at selected strain rates and temperatures revealed flow hardening at small strains followed by flow softening. Deformation of Al–Si alloys is suggested to be controlled by the dislocation climb mechanism through the participation of both the grain interior and grain boundaries by consideration of effective stress instead of applied stress.

Understanding the hot deformation behavior of Mo[sbnd]42Re alloy: Insights from strain rate sensitivity, microstructure, and misorientation

Mo42Re alloy, as a high-temperature structural and functional material, has broad application prospects in the nuclear industry. In this study, the hot deformation behavior of Mo42Re alloy was systematically investigated using hot compression tests and electron backscatter diffraction (EBSD) techniques in the temperature range of 1200–1500 °C and strain rate range of 0.001–1 s−1. The results showed that the flow stress of Mo42Re alloy exhibited a strong dependence on temperature and strain rate. The strain rate sensitivity index (m-value) was high under the conditions of 1350–1450 °C and 0.001 s−1. With increasing deformation temperature and decreasing strain rate, dynamic recrystallization (DRX) was significantly promoted, and the recrystallized volume fraction increased from 2.79% at 1200 °C/1 s−1 to 20.3% at 1500 °C/0.001 s−1. Meanwhile, the occurrence of and DRX effectively reduced the grain reference orientation deviation (GROD) gradients and kernel average misorientation (KAM) levels within the grains. This study revealed the mechanisms of microstructural evolution during hot deformation of Mo42Re alloy, providing important guidance for optimizing its thermomechanical processing parameters.

Effect of Al Content on Microstructure and Properties of AlxCr0.2NbTiV Refractory High-Entropy Alloys.

High-temperature creep refers to the slow and continuous plastic deformation of materials under the effects of high temperatures and mechanical stress over extended periods, which can lead to the degradation or even failure of the components' functionality. AlxCr0.2NbTiV (x = 0.2, 0.5, or 0.8) refractory high-entropy alloys were fabricated by arc melting. The effects of Al content on the microstructure of AlxCr0.2NbTiV alloys were studied using X-ray diffraction, scanning electron microscopy, and electron backscatter diffraction. The microhardness, compression properties, and nanoindentation creep properties of AlxCr0.2NbTiV alloys were also tested. The results show that the AlxCr0.2NbTiV series exhibits a BCC single-phase structure. As the Al content increases, the lattice constant of the alloys gradually decreases, and the intensity of the (110) crystal plane diffraction peak increases. Adding aluminum enhances the effect of solution strengthening; however, due to grain coarsening, the microhardness and room temperature compressive strength of the alloy are only slightly improved. Additionally, because the effect of solution strengthening is diminished at high temperatures, the compressive strength of the alloy at 1000 °C is significantly reduced. The creep mechanism of the alloys is predominantly governed by dislocation creep. Moreover, increasing the Al content helps to reduce the sensitivity of the alloy to the loading rate during the creep process. At a loading rate of 2.5 mN/s, the Al0.8Cr0.2NbTiV alloy exhibits the lowest creep strain rate sensitivity index (m), which is 0.0758.

Quantitative Insight into the Compressive Strain Rate Sensitivity of Polylactic Acid, Acrylonitrile Butadiene Styrene, Polyamide 12, and Polypropylene in Material Extrusion Additive Manufacturing

Herein, a research and engineering gap, i.e., the quantitative determination of the effects of the compressive loading rate on the engineering response of the most popular polymers in Material Extrusion (MEX) Additive Manufacturing (AM) is successfully filled out. PLA (Polylactic Acid), ABS (Acrylonitrile Butadiene Styrene), PP (Polypropylene), and PA12 (Polyamide 12) raw powders were evaluated and melt-extruded to produce fully documented filaments for 3D printing. Compressive specimens after the ASTM-D695 standard were then fabricated with MEX AM. The compressive tests were carried out in pure quasi-static conditions of the test standard (1.3 mm/min) and in accelerated loading rates of 50, 100, 150, and 200 mm/min respectively per polymer. The experimental and evaluation course proved differences in engineering responses among different polymers, in terms of compressive strength, elasticity modulus, toughness, and strain rate sensitivity index. A common finding was that the increase in the strain rate increased the mechanical response of the polymeric parts. The increase in the compressive strength reached 25% between the lowest and the highest strain rates the parts were tested for most polymers. Remarkable variations of deformation and fracture modes were also observed and documented. The current research yielded results with valuable predictive capacity for modeling and engineering modeling, which hold engineering and industrial merit.

Hot deformation behavior, superplasticity and microstructure evolution of a new hot isostatic pressed nickel-based superalloy

The new hot isostatically pressed (HIP) superalloy has demonstrated remarkable superplastic characteristics, as evidenced by studying the compression and tensile deformation behavior. To identify the superplastic deformation zone, the instability regions at various strain variables were overlaid onto the strain rate sensitivity index (m) distribution map at a strain of 0.6, resulting in the acquisition of a new hot working map. The tensile test results showed that under the conditions of 1080 °C-10−2.5 s−1 (0.35 < m < 0.43) and 1030 °C-10−3 s−1 (0.66 < m < 0.74) which located in the superplastic deformation zone in the new hot working map, the new HIPed superalloy exhibited superplasticity, and the elongation was 395 % and 410 %, respectively. Considering the hot working map and the microstructure evolution, the suitable hot working window was further optimized to be 1030–1080 °C and 0.001–0.005 s−1. At high strain rate and low temperature conditions, continuous dynamic recrystallization (CDRX) was the primary mechanism for dynamic recrystallization (DRX), while with the gradual decrease of strain rate, discontinuous dynamic recrystallization (DDRX) tended to occur and dominate the process. DDRX dominated under high temperature deformation condition.

Compressive Flow Behavior and Microstructural Evolution of Friction Stir Processed A356-5% B4C Composite

Abstract An Al-7Si-0.3Mg (A356) alloy reinforced with 5 % boron carbide (B4C) particulates was produced through squeeze casting technique at a temperature of 710°C. Friction stir processing (FSP) was employed on an A356-5% B4C composite with optimized parameters, viz., tool advancing speed of 15 mm/min and tool rotation speed of 250 r/min for one pass and two passes. High-temperature flow behavior of the FSPed A356-5% B4C composite was investigated by strain rate jump (1 × 10−3 to 5 × 10−1 s−1) compression tests using a thermomechanical simulator at temperatures of 470°C and 500°C. Strain rate jump tests revealed superplastic region with strain rate sensitivity index m = 0.4 in the lower strain rate regime of 1 × 10−3 to 5 × 10−2 s−1. However, the value of m reduced to 0.3 upon two-pass FSP. The reduction in m is attributed to the more uniform redistribution of hard Si particles throughout the composite, as examined by microstructure evolution in scanning electron microscopy, linked with energy-dispersive spectroscopy and electron-backscattered diffraction facility.

Superplastic behavior of a fine-grained Mg−Gd−Y−Ag alloy processed by equal channel angular pressing

An extruded Mg−6Gd−3Y−1.5Ag (wt%) alloy was processed by 6 passes of equal channel angular pressing (ECAP) at 553 K using route Bc to refine the microstructure. Electron back-scattered diffraction (EBSD) analysis showed a fully recrystallized microstructure for the extruded alloy with a mean grain size of 8.6 µm. The microstructure of the ECAP-processed alloy was uniformly refined through dynamic recrystallization (DRX). This microstructure contained fine grains with an average size of 1.3 µm, a high fraction of high angle grain boundaries (HAGBs), and nano-sized Mg5Gd-type particles at the boundaries of the DRXed grains, detected by transmission electron microscopy (TEM). High-temperature shear punch testing (SPT) was used to evaluate the superplastic behavior of both the extruded and ECAP-processed alloys by measuring the strain rate sensitivity (SRS) index (m-value). While the highest m-value for the extruded alloy was measured to be 0.24 at 673 K, the ECAP-processed alloy exhibited much higher m-values of 0.41 and 0.52 at 598 and 623 K, respectively, delineating the occurrence of superplastic flow. Based on the calculated average activation energy of 118 kJ mol−1 and m-values close to 0.5, the deformation mechanism for superplastic flow at the temperatures of 598 and 623 K for the ECAP-processed alloys was recognized to be grain boundary sliding (GBS) assisted by grain boundary diffusion.

Superplasticity of a hot rolled Mg–3Zn–0.5RE–0.5Zr (ZEK300) alloy

Superplasticity of a hot rolled fine-grained Mg–3Zn–0.5RE–0.5Zr (ZEK300) alloy was assessed via shear punch testing (SPT). The deformation behavior of the alloy having a grain size of 4.5 μm exhibited regions I, II and III, typical of superplastic materials. In region II, the strain rate sensitivity indices of ZEK300 alloy were obtained as 0.51, 0.48 and 0.41 at 350, 400 and 450 °C, respectively. The average activation energy of 87.6 kJ mol–1 implies that the principal mechanism of deformation is grain boundary sliding (GBS) facilitated by grain boundary diffusion.

Strain rate sensitivity of low-temperature superplastic cold-rolled medium Mn steel with ultrafine equiaxed dual-phase microstructure

This study reports the evolution of strain rate sensitivity (SRS) a novel 3.6Al Medium Mn steel (MMS) with an ultrafine equiaxed dual-phase structure. By varying temperature and strain rate, a new bidirectional reciprocating strain rate jump experiment was conducted to evaluate the effect of strain rate on the SRS index m. Tensile tests were conducted at high-temperature deformation to obtain the maximum m-value, and microstructure were characterized. The results demonstrate that at temperatures ranging from 700 °C to 750 °C and strain rates from 2.5 × 10−4 to 1.6 × 10−2 s−1, the m-value decreases monotonously with increasing strain rate, and the decreasing trend slows down. During high-temperature deformation, the m-value is more sensitive to changes in strain rate. At 700 °C, the grain refinement increases the m-value with the increase in strain. Interestingly, MMS exhibited new γ fiber and brass texture during deformation at 750 °C, with a larger m-value and better superplasticity (∼1295%).

Mechanical behavior of nanorubber reinforced epoxy over a wide strain rate loading

Nanorubber/epoxy composites containing 0, 2, 6 and 10 ​wt% nanorubber are subjected to uniaxial compression over a wide range of strain rate from 8 ​× ​10−4 s−1 to ∼2 ​× ​104 s−1. Unexpectedly, their strain rate sensitivity and strain hardening index increase with increasing nanorubber content. Potential mechanisms are proposed based on numerical simulations using a unit cell model. An increase in the strain rate sensitivity with increasing nanorubber content results from the fact that the nanorubber becomes less incompressible at high strain, generating a higher hydro-static pressure. Adiabatic shear localization starts to occur in the epoxy under a strain rate of 22,000 s−1 when the strain exceeds 0.35. The presence of nanorubber in the epoxy reduces adiabatic shear localization by preventing it from propagating.

Superplasticity in a coarse-grained as-cast magnesium alloy

Superplasticity of a coarse-grained cast Mg–2.5Gd–0.5Zr alloy was investigated by assessing the strain rate sensitivity index (m-value) through the shear punch testing (SPT) method in the temperature range of 623–748 K and shear strain rate range of 2.8 × 10−3–2.2 × 10−2 s−1. The initial as-cast grain size of about 150 μm was reduced to about 3.5 μm at the end of the test. This severe grain refinement caused by dynamic recrystallization (DRX) facilitated superplasticity in the studied cast alloy. According to the respective m-values of 0.51 and 0.53 obtained at 698 and 723 K, and the activation energy of 80 kJ mol−1, the prevailing mechanism of deformation was suggested as grain boundary sliding (GBS) controlled by grain boundary diffusion.

High-strain-rate superplasticity and microstructural evolution in ECAP-processed Mg–6.5Y–1.2Er–1.6Zn–0.5Ag alloy

A warm equal-channel angular pressing (ECAP) procedure was applied to a new Mg–6.5Y–1.2Er–1.6Zn (WEZ612)–0.5Ag alloy with a long-period stacking ordered (LPSO) phase. The microstructure, superplasticity, and deformation mechanism of the WEZ612–0.5Ag alloy were then systematically investigated. Three different precipitation phases formed in the alloy with trace Ag addition, namely LPSO, γ, and nanoprecipitate phases. A remarkable elongation of 726% was attained at 623 K and a strain rate of 0.01 s−1. The strain rate sensitivity index (m) and activation energy (Q) under these deformation conditions were 0.461 and 133.08 kJ mol−1, respectively. These m and Q values confirm that the primary deformation mechanism of the WEZ612–0.5Ag alloy at 623 K was grain boundary sliding assisted by lattice diffusion. The highly stable LPSO phases, γ precipitates, and nanoprecipitates synergistically improved the superplasticity of the alloy by retarding crack propagation and grain growth and by promoting the basal plane slip.