Static Bath Research Articles

Enhancing phosphorus removal: the impact of alkaline environment in eutrophic water systems

Abstract Excessive phosphorus input leads to poor water quality and eutrophication. However, limited research has directly explored the influence of pH on phosphorous in actual aquatic systems. This study investigated the effect of pH on phosphorus removal in synthetic, eutrophic, and black-odorous water. The pH levels ranging from 3.5 to 12.0 were adjusted using H2SO4, NaOH, and cement with a 0.5 ± 0.03 interval, followed by a 25 ± 1 °C static water bath for 24 h. Results showed that NaOH-adjusted pH removed >65% TP from eutrophic water (pH ≥9.50) and black-odorous water (pH ≥11.0). Meanwhile, cement-adjusted pH removed >84%, >90%, and >82% TP from the synthetic solution (pH ≥11.0), eutrophic water (pH ≥9.5), and black-odorous water (pH ≥9.5), respectively. The alkaline environment enhanced the formation of Ca-P in eutrophic water and black-odorous water, and cement strengthened the chemical precipitation of phosphorus by providing additional Ca2+. This study lays the groundwork for pH adjustment strategies in eutrophic water, holding significant implications for water resource management and environmental protection.

Evaluation of earthworm meal (Eudrilus eugeniae) as fish meal replacement in juvenile Mangrove Crab (Scylla serrata) diet

Two feeding trials were conducted to evaluate the performance of the earthworm (Eudrilus eugeniae) meal (vermimeal) as a replacement for fish meal in the diet of juvenile mangrove crab (Scylla serrata) in terms of growth, feed efficiency, intermolt duration, carapace width increment, molting success, survival, and incidence of cannibalism. Four experimental diets were formulated with 0, 25, 50, and 75% fish meal protein replaced with earthworm meal protein, designated as D0, D25, D50, and D75, respectively. In the first feeding trial, the experimental diets were fed to crablets with an initial average weight of 0.09±0.007g. Each replicate comprised ten (10) crablets individually stocked in 750ml-capacity plastic containers randomly distributed in a static water bath. Final weight gain, feed efficiency and survival were measured after the 5th molt. In the second feeding trial, 150 crablets with an average weight of 0.07±0.002g were stocked at 30 crablets each in five (5) replicate tanks. Survival and incidence of cannibalism were monitored daily until the end of the culture period of 30 days. The first study showed that the growth of mangrove crab juveniles fed the diet with up to 50% of the fish meal protein replaced by the earthworm meal protein was statistically comparable to the control group. The survival of crablets in the second feeding trial was highest in D25 (33%), followed by D50 (29%), D0 (18%), and lowest in the group fed with D75 (13%). Overall, earthworm meal (Eudrilus eugeniae) can replace as much as 50% of the fish meal protein in juvenile mangrove crab (Scylla serrata) diet without negative effects on growth, carapace width increment, feed efficiency, intermolt duration, molting success, survival, and cannibalism.

Design Evolution of MADMAX Conductor to a Nb–Ti Cable in Copper Conduit

The MADMAX (MAgnetized Disc and Mirror AXion) project aims at detecting axion dark matter in the mass range around 100 μeV. Prerequisite for success is a very large dipole (1.35 m warm bore) with a high magnetic field up to 10 T. A first conductor design made of Nb-Ti Rutherford Cable On Conduit Conductor with a hole in the copper conduit (RCOCC type) was already presented. The coolant is static bath of superfluid helium at 1.8 K. Unfortunately, no conductor manufacturer with an available production line was found to take in charge the cable insertion/soldering process. Actually, such a production line should be compatible with large conductor section (∼400 mm²) including a solder wave device. The type of conductor was changed to use a line developed for ITER Cable In Conduit Conductor (CICC). Nevertheless, the jacket part was kept in copper. The main evolution of the MADMAX conductor design is presently reviewed. The final outer dimensions of the conductor, the void fraction and the required cold work of the copper induces a reverse engineering challenge on the initial shape of the copper profile. Then, the cable geometry modification involves a lots of differences in terms of self-field, strand diameters, transposition paths, joints technique and conductance between the strands and the stabilizer. The mechanical aspects are subject to evolution for the project due to the magnetic design optimization and conductor type change. A sub-modeling approach is used to detail the stress level in the stabilizer jacket. The possibility of wire motion and wire deformation during the conductor compaction in the production line is also discussed. Concerning the thermal analysis, the major difference is the thermo-hydraulic quench back that induces a much higher pressure drop of the helium in the conduit. So, higher pressure induced higher helium velocity and a fast detection after a quench event in superfluid environment becomes possible.

Sử dụng hai ngưỡng khai thác tập có thể xóa trên dữ liệu tăng cường

Traditional data mining is often applied in static databases and bath processing. In fact, databases are often changed, bath processing is not suitable because it consumes more time to mine in the whole database. Therefore, mining in dynamic databases attracted many researchers where mining erasable itemsets (EIs) in incremental databases is one of interesting areas. Recent years, there are some publications developed for updated EIs in dynamic databases but they consume more time to rescan the original database. In this paper we propose an algorithm for updating EIs using two minimum thresholds to avoid rescanning databases, we also use new data structure to efficient process incremental databases.

Selective Removal of Various Resilient Ionic and Halides-Based Surface Contaminants by Wet Cleaning

In this paper, we investigate the use of a wet cleaner developed to dissolve residues left after plasma etching selectively to aluminum in new applications such as the removal of various resilient ionic and halides-based surface contaminants. The compromise between efficiency and selectivity of this fluorinated acid cleaner makes it an interesting chemistry for many cleaning steps during wafer manufacturing. Two new applications were investigated: the selective removal of fluoride-based defects on aluminum pads and surface decontamination of various ionic metals with low substrate consumption. These studies showed very encouraging results in beakers level tests, but also on partly industrial equipment, opening new possibilities for this cleaner. Indeed, “water lily” defects removal seems to be possible with a low aluminum consumption in TechniClean IK73. Decontamination study carried out in static bath and in single wafer tool showed rather similar results, enabling static bath protocol and ionic metals removal to be validated and VPD-ICPMS results, after a short process time in a single wafer tool were very promising with metal levels close to the lower limit of detection of all elements tested.

Efficacy of Florfenicol and Oxytetracycline Administered in Feed to Control Cisco Mortality Associated with Aeromonas salmonicida Infections

AbstractTwo medications (one with florfenicol and one with oxytetracycline) that are approved in the United States to control mortality due to furunculosis associated with Aeromonas salmonicida were assessed to determine their efficacy in medicated feeds to treat A. salmonicida‐infected Cisco (also known as Lake Herring) Coregonus artedi. Cisco were subjected to static infection baths containing A. salmonicida or a sham control and then were distributed to replicate test tanks within four treatment groups: (1) fish infected with A. salmonicida and treated with 15 mg florfenicol·kg body weight (BW)−1·d−1, (2) fish infected with A. salmonicida and treated with 83 mg oxytetracycline·kg BW−1·d−1, (3) fish infected with A. salmonicida and treated with a nonmedicated control feed, and (4) uninfected fish treated with a nonmedicated control feed. Medicated and comparative nonmedicated feed rations were administered at 2% BW/d for 10 consecutive days in accordance with the U.S. Food and Drug Administration‐approved drug label, followed by a 7‐d postdosing observation period using only nonmedicated feed. Cisco that were infected with A. salmonicida and treated with florfenicol (79% survival) and oxytetracycline (85% survival) had significantly higher survival than A. salmonicida‐infected fish that received no medicated treatment (3% survival). No statistical difference in Cisco survival between the two medicated feed types was found. Aeromonas salmonicida was not detected in the kidney tissue of any surviving fish treated with medicated feeds at 7 d postdosing using quantitative PCR analysis. Overall, this study demonstrated that florfenicol‐ and oxytetracycline‐medicated feeds were effective A. salmonicida treatments for Cisco. Outcomes may inform ongoing propagation efforts for Cisco restoration within the Great Lakes basin.

Efficacy of a multidose acyclovir protocol against cyprinid herpesvirus 3 infection in koi (Cyprinus carpio).

To evaluate the effect of a multidose acyclovir protocol on koi herpesvirus (KHV) viral load and mortality in a cohabitation challenge. 180 koi fish. Forty fish (shedders) were immersed in a 0.5 KHV plaque-forming units/mL static bath for 8 hours. Mock shedders were treated similarly but exposed to cell culture media. KHV shedders were then transferred into 8 tanks (5 shedders per tank) containing 10 naïve fish (cohabitants) each. Fish in the acyclovir group (AT) received a 10 mg/kg acyclovir intracoelomic injection 1, 3, and 6 days after the first confirmed KHV mortality. Positive controls (PC) were treated similarly but received sterile saline injections. Negative controls (NC) were exposed to mock shedders. Morbidity and mortality were evaluated daily for 50 days post-challenge. Quantitative PCR was used to determine viral load in the gill biopsies of shedders and cohabitants collected at days 19 (T1), 22 (T2), 25 (T3), 34 (T4), and 50 (T5) post-challenge. Survival curves analyzed by the Gehan-Breslow-Wilcoxon method revealed a delayed onset of mortalities and a significantly lower KHV load at T2 and T3 detected in AT cohabitant fish (P = .042) compared to PC group. However, there were no significant differences in overall mortality or viral loads at T5. The acyclovir protocol used in this study did not control viral infection or mortality at the end of the 50-day trial. Shorter intervals between injections could improve outcomes, but the additional stress inflicted by handling should be considered. Exploring other therapeutic alternatives and doses is warranted.

Relativistic quantum thermometry through a moving sensor

Using a two-level moving probe, we address the temperature estimation of a static thermal bath modeled by a massless scalar field prepared in a thermal state. Different couplings of the probe to the field are discussed under various scenarios. We find that the thermometry is completely unaffected by the Lamb shift of the energy levels. We take into account the roles of probe velocity, its initial preparation, and environmental control parameters for achieving optimal temperature estimation. We show that a practical technique can be utilized to implement such a quantum thermometry. Finally, exploiting the thermal sensor moving at high velocity to probe temperature within a multiparameter-estimation strategy, we demonstrate perfect supremacy of the joint estimation over the individual one.

Superconductor thermohydraulical and resistive electrical analytical model (STREAM) applied to WEST TF coil quench analysis

The Toroidal Field (TF) system of the WEST tokamak comprises 18 NbTi superconducting coils, cooled in a static superfluid helium bath at 1.8 K and carrying a nominal current of 1255 A. The 19th December 2017, at the end of plasma run #52205, a quench of TFC09 was detected, first on a thermohydraulical signal (helium liquid level), and triggered the current Fast Safety Discharge (FSD).The quench was found to be induced by a neutron and gamma flux caused by highly energetic runaway electrons (30 MeV) colliding the outboard plasma facing components. Some previous analyses with SuperMagnet (CryoSoft) code confirmed a so called “smooth” quench with small initial heat deposition length (0.4 m) at low field region (external leg) and with a number of initially quenched conductors nearly equal to 100.A Superconductor Thermohydraulical and Resistive Electrical Analytical Model (STREAM) has been developed. This model comprises the electrical equations (magnetic field, current sharing temperature, quenched length evolution, Joule energy, resistive voltage, resistance and current) and a thermodynamical and an hydraulical evolutions in two following sequences. The first one comprises the helium pressure evolution with an isentropic compression (closed volume) of a cold volume by a hot (and heated) volume; the second one comprises the determination of expulsed helium mass flow in the exhaust circuit (from a given pressure threshold) with a limit at atmospheric pressure or Mach number equal to 1. The whole TFC09 circular coil is modelled by a single bath with one conductor of length equal to coil average perimeter.For WEST TFC09 quench STREAM calculations, the inputs are the Minimum Quench Energy (MQE) and the propagation law of the quenched (normal) length. Calculated STREAM results showed good agreement with the measurements as well as the calculated SuperMagnet results. The maximal resistive voltage, Joule energy and resistance are respectively at 1400 V, 18 MJ and 5 Ω. The maximal values of helium pressure, conductor temperature and expulsed helium mass flow are respectively 0.9 MPa, 80 to 90 K and 4 to 5 kg/s. This STREAM analytical model can be useful (with adaptation to CICC configuration) for other tokamak magnets safe operation and protection, notably considering that the execution time is rather small due to the set of solved equations.

Managing microbes

Managing microbes

Penetration of fission product ions into complex solids and the effect of ionic wash methods.

During washing of radiologically impacted building surfaces, penetration of radionuclide ions into complex solids associated with these surfaces may occur. This study investigates the penetration of 137Cs, 85Sr, and 152Eu solutions into numerous common building materials and radionuclide behavior when these materials were exposed to a static bath or low-pressure flow of tap water, 0.1 M potassium chloride (KCl), and 0.5 M KCl. The decontamination efficacy and the depth profile for residual contamination were measured to determine the conditions under which applying a wash solution has benefit compared to physically removing the surface material. On asphalt, 70-80% of the radionuclides were found to be within 0.02 mm of the surface. Concrete is more porous than asphalt, and 80% of the radionuclides were within 0.2 mm of the surface for 137Cs and 152Eu and 50-80% for 85Sr. Water effectively removed all contaminants from hard nonporous surfaces. Finally, this paper illustrates that a wash penalty factor concept-defined as ratio of the depth at which 50% of the radioactivity is found in the washed sample divided by the depth at which 50% of radioactivity is found in the control-can serve as a way to quantify whether the wash method increases the depth at which contamination penetrates into the material and thus the material becomes more difficult to decontaminate.

Relativistic quantum thermodynamics of moving systems

We analyse the thermodynamics of a quantum system in a trajectory of constant velocity that interacts with a static thermal bath. The latter is modeled by a massless scalar field in a thermal state. We consider two different couplings of the moving system to the heat bath, a coupling of the Unruh-DeWitt type and a coupling that involves the time derivative of the field. We derive the master equation for the reduced dynamics of the moving quantum system. It has the same form with the quantum optical master equation, but with different coefficients that depend on velocity. This master equation has a unique asymptotic state for each type of coupling, and it is characterized by a well-defined notion of heat-flow. Our analysis of the second law of thermodynamics leads to a surprising equivalence: a moving heat bath is physically equivalent to a mixture of heat baths at rest, each with a different temperature. There is no unique rule for the Lorentz transformation of temperature. We propose that Lorentz transformations of thermodynamic states are well defined in an extended thermodynamic space that is obtained as a convex hull of the standard thermodynamic space.

A multisample 7 T dynamic nuclear polarization polarizer for preclinical hyperpolarized MR.

Dynamic nuclear polarization (DNP) provides the opportunity to boost liquid state magnetic resonance (MR) signals from selected nuclear spins by several orders of magnitude. A cryostat running at a temperature of ~ 1 K and a superconducting magnet set to between 3 and 10 T are required to efficiently hyperpolarize nuclear spins. Several DNP polarizers have been implemented for the purpose of hyperpolarized MR and recent systems have been designed to avoid the need for user input of liquid cryogens. We herein present a zero boil-off DNP polarizer that operates at 1.35 ± 0.01 K and 7 T, and which can polarize two samples in parallel. The samples are cooled by a static helium bath thermally connected to a 1 K closed-cycle 4 He refrigerator. Using a modified version of the commercial fluid path developed for the SPINlab polarizer, we demonstrate that, within a 12-minute interval, the system can produce two separate hyperpolarized 13 C solutions. The 13 C liquid-state polarization of [1-13 C]pyruvate measured 26 seconds after dissolution was 36%, which can be extrapolated to a 55% solid state polarization. The system is well adapted for in vitro and in vivo preclinical hyperpolarized MR experiments and it can be modified to polarize up to four samples in parallel.

Thermohydraulic analysis of Tore Supra/WEST TF coil quench: Associated smooth quench occurrence in tokamak

The Toroidal Field (TF) system of the Tore Supra/WEST tokamak comprises 18 NbTi superconducting coils, cooled by a static superfluid helium bath at 1.8 K and carrying a nominal current of 1255 A. The 19th December 2017, at the end of plasma run #52205, a quench of TFC-09 was detected first on a secondary thermohydraulical signal (helium liquid level) and triggered the current Fast Safety Discharge (FSD). A numerical model of this quench has been developed with SuperMagnet (CryoSoft). The whole TFC-09 circular coil is modelled by THEA as a single large Cable-In-Conduit Conductor (CICC) with 2028 large rectangular strands (monolithic conductors of length equal to coil average perimeter). The external quench helium relief circuit (cold and warm safety valves, rupture disk and magnetic valve with corresponding pressure set) is modelled by FLOWER.The helium pressure in the coil, upstream of the cold safety valve (maximum value of 9 bar), and the expulsed helium temperature have been used as comparison between measurements and calculations which depend on the Minimum Quench Energy (MQE) used in THEA with small initial heat deposition length (few tens of centimeters) at low field region (external leg). This energy, in the order of few kJ, is compared to the real shape and energy of neutron and gamma flux caused by highly energetic runaway electrons colliding the outboard plasma facing components and which induced the quench. The expulsed helium mass flow rate of nearly 6 kg/s during 5 s has also been calculated. This event confirms on one hand the criticality and the possible occurrence of a so called “smooth quench” caused by small initial heat deposition length and at low field region and on the other hand the important interest of secondary quench detection which can be useful for other tokamak magnets safe operation and protection.

CoolGAL: a Galinstan bathed Be fast neutron production target at the NEPIR facility

In this contribution, we present the CoolGAL fast neutron production target system, to be used in the initial phase of the NEPIR irradiation beamline at the SPES facility, that will be operational in 2022. Initially, NEPIR will be used for shielding studies against fast neutrons for space applications and to investigate neutron-induced single event effects in microelectronic devices and systems. In CoolGAL, the neutron production component, a thick Be cylinder, is immersed in a static bath of Galinstan, a liquid alloy of Ga, In and Sn, contained by an outer water cooled copper cladding. MCNPX calculations indicate that, by using a 1 μA current of 70 MeV protons, it can produce a fast neutron energy spectrum that is somewhat flat the 30-65 MeV energy range and with a sharp cut-off at the beam energy. At the standard test point, located 2.6 m downstream from the source, the beam spot diameter, defined by the peculiar collimation scheme of the initial phase of NEPIR, is 10 cm and the integral fast neutron flux is Φn(1< En<65 MeV) ~ 3×106 n cm-2s-1. Using proton beams with two different energies, one can calculate, by subtraction, the effects due to the neutrons in the energy interval defined by the two cut-off values. Preliminary results of ANSYS calculations, for a 1 μA proton current of 70 MeV protons (70 W), show a limited regime temperature (28 °C) of the Be component, capable of ensuring the exceptional safety level required for the operation at SPES. The thermal reliability of CoolGAL is very promising for future developments that require higher proton currents.

Management of Multiple Protozoan Ectoparasites in a Research Colony of Axolotls (Ambystoma mexicanum).

Axolotls (Ambystoma mexicanum) from a research colony presented with multifocal, white chalky to gray skin lesions, a diffuse whitish to blue hue to the integument, and friable gill filaments. Skin scrapings and wet mounts revealed Chilodonella, Ichthyobodo, and a trichodinid species. The average overall burden (that is, all 3 species) per axolotl ranged from 0 to 25 parasites per 40 × field (p40f; mean ± 1 SD, 2.6 ± 5.5), with a prevalence of 12%, 60%, and 48%, respectively. Concurrent with husbandry modifications, axolotls were treated with an 8-h static immersion bath that contained 0.025 mL/L 37% formaldehyde. Chilodonella organisms were no longer observed after the initial treatment, and Ichthyobodo decreased from 2.4 ± 5.6 to 0.6 ± 1.8 organisms p40f. However, the average overall burden increased 4-fold to 10.5 ± 9.8 parasites p40f, and the trichodinid organisms increased 13-fold from 0.8 ± 2.3 to 10.4 ± 9.2 organisms p40f. A second treatment consisted of an 8-h immersion bath that contained 0.05 mL/L 37% formaldehyde on 2 consecutive days. A significant change was noted in the average overall burden of 0.5 ± 1.1 parasites p40f, a greater than 5- and 21-fold decrease from pretreatment and after the initial treatment, respectively. No significant change between the first and second treatment was observed for Ichthyobodo, with 0.6 ± 1.2 organisms p40f, but this number represented a significant decrease from pretreatment. After the second treatment, the trichodinid organism was detected in only one axolotl, with a low overall burden of 0.2 ± 0.4 organisms p40f and resulting in a significant decrease in the trichodinid count to 0.01 ± 0.04 organisms p40f. Treatment with formalin (37% formaldehyde), in conjunction with husbandry improvements, was effective in significantly reducing ectoparasite burden and eliminating clinical symptoms in axolotls but did not fully eliminate all protozoa.

Superfluid Helium cooling and compact Heat Exchanger for HL-LHC D2 Recombination Dipoles

New D2 recombination dipoles with a larger aperture than in the LHC dipoles are required for the future High Luminosity LHC at CERN. These 13.5 m-long D2 magnets are proposed to be conduction cooled in a static bath of pressurized He II. Their cooling is provided via pressurized He II channels located in the D2 iron yoke and thermally connected to a saturated bath installed at one end of each D2 dipole. The heat transfer between the pressurized He II static bath and the bath pumped down to 16.4 mbar (1.8 K) is performed in a heat exchanger under study at CEA. Various design solutions were studied and evaluated to define the more suitable solution fulfilling on the one hand D2 cooling requirements (up to 70 W) and on the other hand D2 cryostat integration constraints. The paper will report on the D2 cooling needs and constraints, present the studied options and detail the main design features of the selected solution for a compact heat exchanger for D2 dipoles.

A Novel Method to Fabricate High Strength Nanofiber Filaments: Morphology, Crystalline Structure, and Thermal and Mechanical Properties

Wet electrospinning is a simple and efficient method to manufacture continuous nanofiber filaments. However, polyacrylonitrile nanofiber filaments collected using a static water bath are limited for application in certain areas due to their low degree of alignment and breaking stress values. To improve these properties, a novel countercurrent flowing liquid bath collector was combined with a multi-needle electrospinning device. The morphologies, crystalline structures, thermal behaviors and mechanical properties of filaments fabricated under different countercurrent bath liquid motion conditions were investigated. In addition, the forces acting on the nanofibers in the bundling triangular zone under countercurrent liquid bath motion were analyzed. The results showed that the average nanofiber diameter of the filaments decreased with an increase in bath solution motion forces. The maximum alignment degree and breaking stress of the nanofibers were 85 % and 0.63 cN/dtex, respectively, achieved using a liquid flow rate of 80 ml/min and water inlet diameter of 6 mm. The alignment degree of the assembled nanofibers in the bundling triangular zone could be increased by 57 % when using a countercurrent flowing liquid compared with a static liquid bath.

Reaction-induced porosity fingering: Replacement dynamic and porosity evolution in the KBr-KCl system

In this contribution, we use X-ray computed micro-tomography (X-CT) to observe and quantify dynamic pattern and porosity formation in a fluid-mediated replacement reaction. The evolution of connected porosity distribution helps to understand how fluid can migrate through a transforming rock, for example during dolomitization, a phenomenon extensively reported in sedimentary basins. Two types of experiment were carried out, in both cases a single crystal of KBr was immersed in a static bath of saturated aqueous KCl at room temperature and atmospheric pressure, and in both cases the replacement process was monitored in 3D using X-CT. In the first type of experiment a crystal of KBr was taken out, scanned, and returned to the solution in cycles (discontinuous replacement). In the second type of experiment, 3 samples of KBr were continuously reacted for 15, 55 min and 5.5 h respectively, with the latter being replaced completely (continuous replacement). X-CT of KBr-KCl replacement offers new insights into dynamic porosity development and transport mechanisms during replacement. As the reaction progresses the sample composition changes from KBr to KCl via a K(Br, Cl) solid solution series which generates porosity in the form of fingers that account for a final molar volume reduction of 13% when pure KCl is formed. These fingers form during an initial and transient advection regime followed by a diffusion dominated system, which is reflected by the reaction propagation, front morphology, and mass evolution. The porosity develops as fingers perpendicular to the sample walls, which allow a faster transport of reactant than in the rest of the crystal, before fingers coarsen and connect laterally. In the continuous experiment, finger coarsening has a dynamic behaviour consistent with fingering processes observed in nature. In the discontinuous experiment, which can be compared to rock weathering or to replacement driven by intermittent fluid contact, the pore structure changes from well-organized parallel fingers to a complex 3D connected network, shedding light on the alteration of reservoir properties during weathering.

An investigation into waterborne intumescent coating with different fillers for steel application

Purpose This study aims to discuss the modification and/or improvement of intumescent coating system by incorporating waterborne resin with an appropriate combination of flame-retardant additives and four different fillers, namely, TiO2, Al(OH)3, Mg(OH)2 and CaCO3. Design/methodology/approach Coating mixtures are characterized using the Bunsen burner, thermogravimetric analysis, limiting oxygen index, scanning electron microscope, static immersion bath, Fourier transform infrared and adhesion tester. Findings Results show that the combination of coating with CaCO3 filler significantly improved fire protection performance because of its thick char layer and the equilibrium temperature being 264°C. Char layer showed a uniform dense foam structure on micrograph and this formulation had adhesion strength of 2.13 MPa, which indicates effectiveness of the interface adhesion on substrate. Conversely, the combination of coating with Al(OH)3 exhibited highest oxygen index of 35 per cent, which resulted in excellent flammability resistance. Research limitations/implications This paper discusses only the effect of mineral fillers on properties of intumescent coatings. Practical implications In the modern design of building infrastructure, fire safety is significant for the protection of human life and assets. The application of intumescent coating in buildings is currently practiced because of its effect on material flammability during a fire. Originality/value The analysis method to evaluate the performance of water-borne resin with different fillers is formulated, and it could be applied in all kinds of coatings and mixtures to be used as an effective fire protection system for steel constructions.