Beam Source Research Articles

A retarding field thermal probe for combined plasma diagnostics

The wide variety and ever-growing applications of plasma processes in research and industry require an equally growing diversity and accessibility of suitable plasma diagnostics. The plasma parameters and the tailoring thereof strongly influence the outcome of thin film deposition, plasma etching, or surface treatments, to name only a few. To further enhance the determination of different fluxes of species, their energies, and behaviour influencing a surface process, a custom-built combination of two commonly used diagnostics was developed. With a retarding field energy analyzer, one can obtain the ion energy distribution in a plasma by measuring the current at the collector depending on the applied voltage at the scan grid. A passive thermal probe determines the energy flux density coming from a process plasma by measuring the temperature change of a dummy substrate. In this study, we present a retarding field energy analyzer where a passive thermal probe substitutes the collector. By doing so, we can determine the energy distribution of the charged ions, their energy flux density at a certain potential, and the power deposited onto a substrate. Another advantage is that the thermal probe can even measure the power deposited by incoming (fast) neutrals and of the background gas when the grids keep away the ions. Hence, combining these two powerful diagnostics yields information neither can deliver on their own. The probe has been tested in three different plasma environments: ion beam source, magnetron sputtering and radio frequency discharge plasma.

Energy-scaling of a diode-pumped Alexandrite laser and prototype development for a compact general-purpose Doppler lidar.

We present design and performance data of an energy-scaled diode-pumped Alexandrite laser in single longitudinal mode operation developed as a beam source in a mobile general-purpose Doppler lidar. A maximum pulse energy in Q-switched operation of 4.6mJ and a maximum average power of 2.7W were achieved for a repetition rate range from 500 to 750Hz with excellent beam quality of M 2=1.1. Two rugged and compact demonstrator lasers were built and integrated into mobile lidar systems, where a bandwidth of approximately 3MHz is measured. Measurements of atmospheric winds and temperatures were conducted during several field campaigns from summer 2022 to spring 2023.

In situ X-ray phase contrast imaging of the melt and vapor capillary behavior during the welding regime transition on aluminum with limited material thickness

The X-ray phase contrast imaging is a powerful method to understand the fundamental behavior of the melt and keyhole during the laser beam welding process. In this paper, the keyhole-induced vapor capillary formation in the melt pool is investigated by using an adjustable laser beam source. For this purpose, the aluminum A1050 specimen with a thickness of 0.5 mm is molten only with the heat conduction welding regime by using the ring-mode laser beam. Once the specimen is molten through, the core multi-mode laser beam is then applied to vaporize the melt and a transition to keyhole welding regime occurs. Therefore, the core multi-mode laser beam with an intensity value of 33.3 MW/cm2 is investigated. The correlation between the keyhole-induced vapor capillary and the melt behavior is further investigated in this paper which was recorded with a high sampling rate of 19 kHz. In addition, a theoretical calculation about the keyhole depth is discussed in this paper.

Kinetic Energy of Secondary Particles Produced from Various Electromagnetic Interactions in Water: A Monte Carlo Study

Advancements in imaging systems including Electronic Portal Imaging Devices (EPIDs) play a great role in radiotherapy treatment. It was developed as a verification tool for patient setup during radiotherapy sessions and also become a promising tool for the determination of the accurate placement of radiation beams. However, as part of quality assurance, individual patient treatments are often verified by patient-specific quality control measurements such as before treatment (pretreatment) or during treatment (in vivo). It has been shown that in vivo dosimetry using an electronic portal imaging device (EPID) is an effective QC tool to detect errors and this method has been clinically applied to various treatments. The introduction of advanced EPID technology has led to an interest in its application for dose conformation and dose deposition. Moreover, dose deposition is subject to uncertainties due to several factors, including the presence of secondary particles. Thus, knowing the physical processes that produced the secondary particles as well as their average kinetic energy will help to provide valuable information about the effective filtering of these particles or the possible use of these particles for other applications. In this study, Monte Carlo simulations are performed to determine the average kinetic energy of detected secondary particles, specifically photons, electrons, and positrons produced by each particular physical interaction as a function of detector position using GATE v9.0. The virtual radiotherapy set-up is composed of the box water phantom, which is the target in the simulations with a dimension of 20 cm × 20 cm × 20 cm, an EPID system (detector), and a beam source in which it uses three (3) beams situated at varying positions with an energy of 6 MeV. The monoenergetic pencil beam source is placed 90 cm away from the center of the target and is directed toward the target (+x-axis) while the EPID (detector) is set as 120 cm SDD (source-to-detector distance). Moreover, the photon beam with 10 million primaries is set with varying field sizes of 1 cm × 1 cm, 3 cm × 3 cm, 6 cm × 6 cm, and 9 cm × 9 cm. Overall, the results show that the highest average kinetic energy among secondary particles produced by each physical interaction are electrons coming from Compton scattering (∼ 3 MeV), followed by positrons and electrons from pair production (∼ 2.4 MeV), photons from annihilation and bremsstrahlung (∼ 0.5 MeV), and electrons from ionization (∼ 0.13 MeV).

Experimental and simulation study on the backstreaming positive ions on the quarter-size negative ion source for CRAFT NNBI test facility

As an effective methods of plasma heating, neutral beam injection (NBI) systems based on negative hydrogen ion sources will be utilized in future magnetic-confinement nuclear fusion experiments. Because of the collisions between the fast negative ions and the neutral background gas, the positive ions are inevitable created in the acceleration region in the negative NBI system. These positive ions are accelerated back into the ion source and become high energy backstreaming ions. In order to explore the characters of backstreaming ions, the track and power deposition of backstreaming H+ beam is estimated using the experimental and simulation methods at NNBI test facility. Results show that the flux of backstreaming positive ions is 1.93 % of that of negative ion extraction from ion source, and the magnet filed in the beam source has an effect on the backstreaming positive ions propagation.

Remote maintenance scenario of the caesium ovens and beam source of the ITER heating neutral beam

Maintenance of the Heating Neutral Beam (HNB) injectors that are located in the ITER Neutral Beam (NB) cell needs Remote Handling (RH) operations because the NB cell is a radiation controlled area. This paper describes the remote maintenance sequences of the caesium ovens and the Beam Source (BS) of the ITER HNB by using the Neutral Beam Remote Handling System (NBRHS). Caesium oven maintenance is a regular maintenance that needs to be performed every Long-Term Maintenance (LTM) period as caesium is a consumable to produce caesium vapor to enhance negative ion production. The BS maintenance is a corrective maintenance to do if it fails during the lifetime of ITER. Maintenance of the caesium ovens and the BS involves many RH operations that require collaboration of the NBRHS subsystems and RH tools. Moreover, the maintenance operation needs to be done without spreading contamination from the HNB vessel to the NB cell. The developed maintenance scenario relies on the current NB cell environment and the existing interfaces in the plant system.

Numerical analysis of the effect of an oscillating metal vapor plume on the keyhole and molten pool behavior during deep penetration laser beam welding

The effect of the oscillating metal vapor plume on the keyhole and molten pool behavior during the laser beam welding of AlMg3 aluminum alloys is investigated by experimental and numerical methods. The real-time height of the metal vapor plume is measured by high-speed camera observation. The obtained experimental results are used to evaluate the additional heating source and laser beam attenuation caused by the scattering and absorption based on the Beer–Lambert theory. Furthermore, the dynamic behavior of the metal vapor plume is incorporated into a 3D transient heat transfer and fluid flow model, coupled with the ray tracing method, for the laser beam welding of the AlMg3 alloy. It is found that additional heating resulting from the scattered and absorbed laser beam energy by the metal vapor plume significantly expands the shape of the molten pool on the top region. Moreover, the oscillating metal vapor plume caused the fluctuation of the high-temperature region in the molten pool. The probability of keyhole collapse at the bottom increases 17% due to the oscillating laser power induced by the laser beam attenuation. The internal interplay between the metal vapor plume, molten pool shape, and keyhole collapse is obtained. The developed model has been validated by experiments, which shows a good agreement.

Flash Therapy for Cancer: A Potentially New Radiotherapy Methodology.

In traditional treatment modalities and standard clinical practices, FLASH radiotherapy (FL-RT) administers radiation therapy at an exceptionally high dosage rate. When compared to standard dose rate radiation therapy, numerous preclinical investigations have demonstrated that FL-RT provides similar benefits in conserving normal tissue while maintaining equal antitumor efficacy, a phenomenon possible due to the 'FLASH effect' (FE) of FL-RT. The methodologies involve proton radiotherapy, intensity-modulated radiation treatment, and managing high-throughput damage by radiation to solid tissues. Recent results from animal studies indicate that FL-RT can reduce radiation-induced tissue damage, significantly enhancing anticancer potency. Focusing on the potential benefits of FL proton beam treatment in the years to come, this review details the FL-RT research that has been done so far and the existing theories illuminating the FL effects. This subject remains of interest, with many issues still needing to be answered. We offer a brief review to emphasize a few of the key efforts and difficulties in moving FL radiation research forward. The existing research state of FL-RT, its affecting variables, and its different specific impacts are presented in this current review. Key topics discussed include the biochemical mechanism during FL therapy, beam sources for FL therapy, the FL effect on immunity, clinical and preclinical studies on the protective effect of FL therapy, and parameters for effective FL therapy.

Realization and simulations of the new SPES Beam Cooler

One of the aim of the new project Selective Production of Exotic Species (SPES) is to produce and select new, neutron reach, isotopes [1,2,3,4]. The technique adopted to produce these species is the Isotope Selection On Line (ISOL) that postpones the separation of the isotopes after the beam production, using a High-Resolution Mass Spectrometer (HRMS).In order to allow a good separation of isotopes , the transverse emittance and the energy spread of the beam should have very low values, for this reason the Beam Cooler (BC) is located between the ISOL target, i.e. the beam source, and the HRMS.In the SPES project, where heavy isotopes are expected (mass number >100), the spectrometer resolution must be preferably higher than dm/m = 5 × 10-5 and thus the features of the beam at the entrance of the HRMS should be at least εn 95% < 8.3 × 10-3 π mm mrad and σE < 1.5 eV.BC devices are devoted to improve the beam features in terms of emittance and energy spread. A new BC has been designed and realized by the Laboratoire de Physique Corpuscolaire (LPC) at Caen, France, for the SPES facility at Laboratori Nazionali di Legnaro (LNL), near Padova, Italy.BCs cool down the beam thanks to a dissipative process in which the thermal energy passes from the beam ions to another medium whose constituent is typically much lighter, Helium gas in our case. This process takes place inside a confinement system that on the one hand to limit the spread of the cooling medium, and on the other to allow the beam to continue along the required trajectory, in the presented device it is a row of radio frequency quadrupoles in an almost closed chamber.Some specifications of the BC described in this document: the RFQ is 723 mm long, its internal radius is 5 mm; the RFQ is included in the gas chamber which is 730 mm×280 mm×220 mm. Before it there is the injection part composed by, following the beam trajectory, a grounded pipe (388 mm long) and three focusing electrodes. On the opposite side there is the extraction part with two focusing electrodes.This document presents the main features of the new BC together with the results of a preliminary study where the beam dynamic has been simulated. The analysis embeds also the investigation of the gas distribution inside and outside the BC.The beam dynamic simulations are based on the Simion code [5] while the estimation of the gas distribution is computed with MolFlow+ [6].Simulations show that accurately setting the BC leads to a large improvement of the emittance while the energy spread still needs to be improved. Limiting the gas pressure in the acceleration zone seems to allow the required final boost.

Shielded ionisation discharge (SID) probe for spatiotemporal profiling of pulsed molecular beam.

Intense pulsed supersonic molecular beams are used in many applications such as tokamak fueling, edge plasma diagnostics, ion beam profile monitors, laser cluster experiments, chemical kinetics, etc. Measurement of absolute density is required to optimize beam sources used in these experiments. Absolute density measurement of a continuous molecular beam is challenging due to its small size and rarefied flow, which makes it even more difficult for a pulsed molecular beam due to its transient nature. In this work, we demonstrate a novel probe to measure the spatiotemporal evolution of the absolute number density of a pulsed supersonic molecular beam. The probe is named the Shielded Ionization Discharge probe. It measures density using localized discharge within the molecular beam created by the thermionic emission of electrons from a hot filament. We describe the design, calibration, and characterization of the developed probe. The performance of the probe is demonstrated by measuring the spatial and temporal profiles of a pulsed supersonic molecular beam of 1.5ms duration.

Comparison of Proton and Photon Radiotheraphy for Left-sided Breast Cancer via Dosimetric Calculations

Breast cancer is the most common type of cancer in women. Today, the radiotherapy method is widely preferred to treat cancer patients where proton therapy is a radiotherapy method used to destroy cancerous cells using proton beams with unique characteristics. Photon therapy, on the other hand, is a classical radiotherapy method that treats cancerous cells by targeting ionizing radiation. In our study, a tumor was placed in the left breast in a water phantom with the help of the Geant4 simulation program and geometry with critical organs was modeled. With this simulation, the doses received by the organs were interpreted and comparisons were made using the chi-square method as the two different source beams, proton and photon deployed. When the percentile values in the dose table are normalized for 1 Gy, the test statistic obtained as 0.467, and the H0 hypothesis is rejected at the α=0.975 Statistically, we measured the significant differences between proton and photon dose values for tumors and other organs by Geant4 simulations.

Technical Infrastructure for Clinical Translation of Electron FLASH

For safe clinical translation of electron FLASH, hardware tools for real-time beam control and software tools for treatment planning are necessary. The purpose of this study is to prototype high-throughput hardware for real-time beam control, along with accurate beam modeling of a modern clinical Linac configured to deliver FLASH dose-rates. For real-time beam current monitoring, a beam current transformer (BCT) was initially coupled to a fast digitizer and its linearity was established by varying dose per pulse. The radiation pulse width was modified, and this change was measured using the BCT. The BCT was then used to measure the variability of dose per pulse and pulse width due to a mistuned linear accelerator system. Next, the BCT was interfaced with a field programmable gate array (FPGA) which provides the ability for high-throughput and deterministic control of the Linac based on dose accumulation. For beam modeling, the program, TOol for PArticle Simulation (TOPAS), was used to obtain beam parameters by using Bayesian optimization of the beam energy, source size, angular, and energy spread via comparison of simulated and representative dose profiles. The beam model would then be employed to calculate 3D dose distribution in a CT scan of a 3D-printed anatomically realistic mouse phantom. The area under the current-time curve from the BCT exhibited excellent linearity (response = 12.80 nC/Gy) up to 2.5 Gy/Pulse (R2 = 0.99). The peak beam current for the electron FLASH beam was measured to be ∼10 mA for an instantaneous dose-rate of ∼5×105 Gy/s. The measured radiation pulse width agreed with the expected value (3.7 μs). The pulse width was then shortened and the measurement by the BCT indicated pulse widths of 1.8 μs and 0.5 μs corresponding to 0.7 Gy/pulse and 0.3 Gy/pulse, respectively. The beamline exhibited a ramp-up in dose per pulse and pulse width when using the automatic frequency controller (AFC). For the first pulse, the dose delivered was ∼0.1-0.3 Gy and the pulse width was 0.6 μs. The output stabilized to nominal values of dose and pulse width after 3-4 pulses. This ramp-up was mitigated by manually tuning the RF resonance with the AFC disabled, after which the BCT exhibited constant output and pulse width. The beam modeling work is in progress. We demonstrated that a BCT can provide real-time measurement of per-pulse output suitable as input for FLASH beam control based on dose accumulation. The next steps are to quantify the accuracy of the dose control mechanism with the FPGA-based hardware. Potential failure modes will be identified and mitigated in parallel with the development of the hardware. A 3D-printed mouse phantom has been constructed to facilitate beam modeling work for treatment planning (in progress). On completion of this work, it is expected that we will have key infrastructure elements needed to move towards an eventual FDA investigational device exemption for clinical trials.

A newly developed and verified transport capacity of Monte Carlo photon particles in RMC

In reactor shielding designs, deep-penetration shielding issues, and direct photon heating, photon transport physics is crucial. In the Reactor Monte Carlo (RMC) code, a state-of-the-art photon transport capacity is implemented in this research. For criticality and fixed-source calculations, pure photon and coupled neutron-photon transport are now simulated for four photon-atomic interactions, including Rayleigh scattering, Compton scattering, Photoelectric effect, and Pair production, as well as three major processes of the secondary photons generation (Atomic relaxation, Electron-positron annihilation, and Bremsstrahlung by electrons and positrons). In order to properly balance energy release and deposition during neutron-induced photon production, the yield of photons by neutrons is scaled by a correction factor to account for the delayed gamma radiation, and the effective multiplication factor keff is used in an uncritical system. Using an Automatic Library Generator (ALG) code, a new database for photon transport is processed with the ENDF/B evaluated nuclear data library. Numerous cases, such as a point source in an infinite geometry, a photon beam source in a cylinder geometry, and a fuel assembly in the VERA benchmark, are verified against the Monte Carlo (MC) code OpenMC. Despite some notable differences in the comparison of the photon flux at certain energy ranges, which are caused by differences in the database and also the physics implementation, the results of the energy and spatial distributions of photon flux, and the photon heating show generally good agreement and relative errors are nearly within a triple statistical standard deviation. RMC now offers advanced photon transport capacity for reaction core and shielding applications.

Towards an Understanding of the Challenges in Laser Beam Welding of Copper – Observation of the Laser-Matter Interaction Zone in Laser Beam Welding of Copper and Steel Using in Situ Synchrotron X-Ray Imaging

The increasing demand for contacting applications in electric components such as batteries, power electronics and electric drives is boosting the use of laser-based copper processing. Laser beam welding is a key for an efficient and high-quality electric vehicle production due to its local, non-contact energy input and high automation capability enabling reproducible weld quality. Nevertheless, a major challenge in process design is the combination of energy-efficiency and precise process guidance with regard to weld seam depth and defect prevention (i.e. spatter, melt ejections), partly caused by the high thermal conductivity of copper. High power lasers in the near infrared range and emerging visible laser beam sources with excellent beam quality can provide a suitable joining solution for this purpose. However, the underlying physical phenomena are currently only partly understood and a reflection on the challenges of laser beam welding of copper compared to well researched steel processing has not yet been carried out. In order to improve the understanding of the effect of the different material properties and the influence of process parameters on the vapor capillary and melt pool geometry in laser beam welding, in situ synchrotron investigations on Cu-ETP and S235 using 515 and 1030 nm laser sources were conducted. The material phase contrast analysis was successfully used to distinguish vapor capillary and melt pool phase boundaries during the welding process with high spatial and temporal resolution up to 5 kHz. A significantly different vapor capillary geometry and sensitivity to parameter variation were found between the steel and copper material. In addition, the visualization of characteristic melt flows revealed different melt pool dynamics and a pronounced eddy close to the melt pool surface for copper, which is assumed to be causal for the observation of pronounced spatter formation during copper welding in a certain process window.

Lifetime assessment of the modified grounded grid in the negative ion source SPIDER

In a nuclear fusion reactor, some components of the system are subjected to huge thermal loads. These components, such as grids, neutralizers, calorimeters, ducts, divertors, blankets etc. have to be actively cooled in order to avoid damage, functionality problems and specially to ensure their reliability. The design process of such components requires taking into account several physical phenomena, with the goal of not only satisfying the functionality conditions, but also with a focus on the structural verifications and component lifetime. For assessment of the structural design for components in ITER, the ITER Structural Design Criteria for In-vessel Components (SDC-IC) represent the reference verification criteria.The aim of this work is to investigate the relationship between the cooling system performance and the fatigue life. In this work a generalized framework for the evaluation of cooling system components is presented, taking into account the necessary input parameters, performing numerical analyses, division of component into several interest regions and assessing the fatigue life. The performed numerical analyses are a set of coupled CFD and thermo-structural analyses.A case study is presented for a critical component, the Grounded Grid (GG), inside the SPIDER beam source experiment at Consorzio RFX, Padova, Italy. The presented test case includes cooling system effectiveness analysis, assessment of the temperature distribution on housing during operations, mapping the pressure distribution inside the cooling system and finally assessment of the maximum number of allowed cycles.

Laser beam welding of brass with combined core and ring beam

Brass represents a large part in the production of components within the copper alloy group. Laser beam welding of this alloy offers great potential for many applications in terms of achievable seam quality and productivity. However, there is a very high tendency of the process for irregular seam surfaces and formation of pores as well as spatters. These are due, among other things, to instabilities of the keyhole, which is favored by the evaporation of the alloy component zinc. Furthermore, near-infrared laser beam wavelength can couple poorly into the material due to the low absorption level of brass, whereas absorption jumps during the melt transition. In recent years, high-brilliance near-infrared laser beam sources with adjustable beam profiles have been developed, to contribute to the stabilization of the keyhole. The presented experimental process investigations are on deep penetration welding of different brass alloys (CuZn37 and CuZn39Pb3). A laser beam source with a power of 6000 W and a combined core and ring beam was used for this purpose. It was found that the process parameters, such as energy per unit length, spot size, and process gas supply, have a significant impact on the resulting weld seam. These parameters were systematically varied. The produced seams were analyzed and evaluated using various methods, including micrograph analysis, energy dispersive x-ray spectroscopy, 3D-computed tomography, and 3D-topography imaging. The results were then correlated with the process parameters. Process parameters that produce high-quality bead-on-plate and butt welds for a sheet thicknesses of 2 mm were determined.

Boron containing polyvinyl alcohol/ polyethylene oxide/polyvinyl pyrrolidone composites: Preparation, characterization, gamma radiation shielding and gamma radiation effect on it's thermal properties

The production of PVA/PEO/PVP-B4C and PVA/PEO/PVP-BN nanocomposites is presented in this study by adding certain proportions of boron nitride (BN) and boron carbide (B4C) to the polyvinyl alcohol(PVA)/polyethylene Oxide (PEO)/polyvinyl pyrrolidone (PVP) blend. The percentages of BN and B4C nano powder in the PVA/PEO/PVP blend have been determined as 5%, 10% and 20%. Thermal characterizations were carried out with different techniques such as Differential scanning calorimetry (DSC), Differential Thermal Analysis (DTA), Thermogravimetry (TG). Surface, crystal structure and atomic percentage distribution analyzes of the obtained composites were performed by X-ray Photoelectron Spectroscopy (XPS), X-Ray Diffraction Analysis (XRD), Scanning Electron Microscopy-Energy Dispersive X-Ray (SEM-EDX), and elemental analysis. 10 kGy gamma irradiation was performed on PVA/PEO/PVP-B4C and PVA/PEO/PVP-BN composites. The thermal behavior of the composites at this dose level was investigated. In addition, the radiation shielding properties of composite films obtained at 10 cm distances using Am-241 beam source were examined.

Reversal in solvatochromism, photochromism and thermochromism in a new bis-azo dye based on naphthalen-1-amine

A novel bis-azo dye, 4,4′-((1E,1′E)-(oxybis(4,1-phenylene))bis(diazene-2,1-diyl))bis(naphthalen-1-amine) (abbreviated as 4odna) was synthesized and characterized by IR and 1H, 13C and 2D COSY-NMR spectroscopies, and mass spectrometry. Optical properties were evaluated using UV–vis absorption spectroscopy. The observed solvatochromism was ascribed to the presence of different azo or/and hydrazone forms in solution. The azo forms show both positive and negative solvatochromism, with the reversal occurring for solvents with ET(30) ∼45 kcal mol−1, while the hydrazone tautomer shows negative solvatochromism. Application of the multiparametric Catalán and Kamlet-Taft linear solvation energy models allowed to evaluate the dependence of the solvatochromism exhibited by 4odna on the hydrogen bond donating (HBD) and accepting (HBA) abilities of the solvent, as well as on their dipolarity (SdP) and polarizability (SP). Upon UV (λ = 311 nm) irradiation at room temperature, the compound was found to exhibit similar photochromic behavior in the polar-protic solvents methanol and ethanol, which is distinct from that observed in the polar-aprotic solvents dichloromethane, chloroform and chlorobenzene, with the hydrazone tautomer being photoconverted into the azo tautomer in the first group of solvents and vice-versa in the second group. In acetone, UV irradiation extensively transforms the compound into species with no absorption in the visible range, leading to fast discoloration of the solution. Temperature dependence of the color of the solutions of 4odna in ethanol and chlorobenzene was also evaluated, and reversible thermochromic behavior was observed in the first solvent. In chlorobenzene, no thermochromism was observed, but a change of color of the solution was promptly induced by the UV–vis broadband source beam of the spectrometer when the absorbance spectrum of the solution was being recorded at T = 115 °C, which demonstrates that the azo forms of 4odna undergo easy phototransformation into the hydrazone forms in this solvent at high temperature.

Radiation protection basis of design for the South African isotope facility - SAIF

To expand on its research agenda and meet the growing demand for nuclear medicine products, the South African Isotope Facility (SAIF) was launched. This study focuses on Radiation Protection aspects for SAIF Phase 1, specifically the verification of existing- and basis of design for supplementary engineering controls for the retrofitted accelerator complex, housing an IBA C70 Cyclone 70 MeV H-minus cyclotron and four in-house designed high intensity particle beam target stations. For the dosimetric assessment, a selection of calibrated instruments were used to determine the ambient dose equivalent rate H*(10) at points of interest. Physical dose rate measurements were performed for various source terms (66 MeV p+ on Cu, Al, Mg, Ga and Li) and beam intensities up to tens of micro Amperes, beyond in-situ bulk shielding material, for compound shielded target stations and streaming through existing labyrinths. Comparisons are drawn between actual measurements and the FLUKA code. Primarily to determine the in-situ shielding characteristics of unverified bulk shielding material cast in the 1980s, as core drill samples yielded vastly divergent aggregate types and material densities.

Heat treatment of NiTi alloys: Influence of volumetric energy density on ageing parameters and the resulting physical properties

This study comprehensively examines the effects of ageing temperatures (400, 500, and 600 ᵒC); age-dwelling times (30, 60, and 90 min) and the role of volumetric energy densities (VEDH) of initial processing, on the physical properties of additively manufactured (AM) NiTi samples. Response Surface Modelling (RSM) and curve fitting analysis were employed to establish correlations between the parameters. The samples were processed at different VEDH of 40, 80, and 120 J/mm3 using NiTi (50 at. %) powders via the AM technique of powder bed fusion with a laser beam source (PBF-LB). The melt pool thermal radiation was in-situ monitored using infrared (IR) pyrometers and the collated data post-analysed. Physical properties investigated include microstructure, relative density, composition and phase characteristics, thermal gradient, melt layer temperatures, transformation temperatures, nanohardness and Young's modulus. Mean melt layer temperatures (normalised) increased with VEDH resulting; in all as-built samples being Ti-rich NiTi (>50 at. % Ti), the co-existence of NiTi2, martensite and residual austenite phases, while density was highest in samples processed at VEDH of 80 J/mm3. Ageing at higher temperatures >400 ᵒC for longer dwell times led to recrystallisation and crystallographic re-orientation, but at different degrees depending on the initial thermal history. This recrystallisation effect and initial densities had compounding effects on the observed trends of other examined properties in the aged samples. These findings reveal for the first time, the significant importance of the VEDH of initial processing compared to the ageing temperatures and dwell times.