Dry Wood Research Articles

On-line evaluation of moisture transfer properties for a feed-forward control of a wood drying kiln with a mechanistic model

Kiln operators are forced to rely on their own experience and expertise when adapting standard drying schedules to tackle changing situations or to better suit their needs. The online tuning of a mechanistic model and its use as forward control is therefore proposed to address the current lack of tools. An inverse analysis of the drying kinetics of wooden boards dried in an industrial kiln is carried out to determine the moisture transfer properties of the boards. The values obtained by the inverse method are found to be relatively close to those obtained by direct measurement. The mechanistic model is then used with these input values to simulate the drying of a stack of boards to find the best drying strategy to meet the objectives. This work focuses on achieving a compromise between quality and time. Several difficulties were encountered in developing this approach for a semi-industrial dryer, and some recommendations are made for developing this innovative strategy further.

The effects of microwave and microwave + infrared drying treatments of Pinus brutia and Picea orientalis on water absorption and physical properties

The goal of this study was to find a way to shorten wood drying time by using microwave and combined infrared + microwave drying methods and to analyze color and gloss changes. Wood samples prepared in three groups with dimensions of 20×20×30 mm were used in moisture tests and 75×5×150 mm were used in color change and gloss measurements, obtained from Red pine (Pinus brutia) and Eastern spruce (Picea orientalis) woods. The samples were oven dried, dried by microwave, or dried by infrared + microwave drying method. The wood samples all reached the target moisture. Their weight and volume were calculated in accordance with the principles of TS ISO 13061-1. Color change values were determined before and after drying with a portable color reader (Konica Minolta CR-10) device, and gloss measurements were taken with the Gardner brand gloss meter. By microwave drying for 15 min, 4% moisture content was reached in the wood samples, so both time and energy were saved. The moisture content values decreased compared to the whole drying methods. Most color change was observed in the drying methods using infrared for both red pine and eastern spruce.

Effects of Wood Drying Temperatures on the Reduction in Mechanical Properties of Japanese Cedar (Cryptomeria japonica D. Don) Perpendicular to Grain

Wood drying is often accompanied by changes in mechanical properties due to external thermal energy. This study examined the influences of drying temperature on the mechanical properties of Japanese cedar based on the partial compression properties and bending properties. Two types of longitudinal specimens with quarter grain on both lateral surfaces were prepared under green conditions, followed by subsequent drying under each drying temperature (20 °C, 40 °C, 60 °C, 80 °C, and 100 °C). Then, the partial compression and bending tests were performed using the respective specimens. Young’s modulus perpendicular to grain, yield stress, and compressive strength obtained by the partial compressive test were highest for wood dried at 20 °C. It was considered that the decrease in mechanical properties was attributed to the thermal influences during drying at 100 °C and other factors such as compressive residual stress and cell walls collapsing at lower temperatures. The strain energy suggested that the effects of drying temperature became apparent, especially in the plastic region during loading in the direction perpendicular to the wood fiber. Bending properties showed little influence on drying temperatures compared to the partial compressive properties, whereas the fractures found under the loading point of the wood dried at 100 °C suggested a reduction in resistance to shear forces.

Association between the anatomical features and the natural drying of young wood from hybrid Corymbia torelliana and Corymbia citriodora clones

Association between the anatomical features and the natural drying of young wood from hybrid Corymbia torelliana and Corymbia citriodora clones

Chemical Characterization of Pruning Wood Extracts from Six Japanese Plum (Prunus salicina Lindl.) Cultivars and Their Antitumor Activity.

The Japanese plum tree (Prunus salicina Lindl.) is mainly cultivated in temperate areas of China and some European countries. Certain amounts of wood (from pruning works) are generated every year from this crop of worldwide commercial significance. The main objective of this work was to value this agricultural woody residue, for which the chemical composition of pruning wood extracts from six Japanese plum cultivars was investigated, and the antiproliferative activity of extracts and pure phenolics present in those extracts was measured. For the chemical characterization, total phenolic content and DPPH radical-scavenging assays and HPLC‒DAD/ESI‒MS analyses were performed, with the procyanidin (-)-ent-epicatechin-(2α→O→7,4α→8)-epicatechin (5) and the propelargonidin (+)-epiafzelechin-(2β→O→7,4β→8)-epicatechin (7) being the major components of the wood extracts. Some quantitative differences were found among plum cultivars, and the content of proanthocyanidins ranged from 1.50 (cv. 'Fortune') to 4.44 (cv. 'Showtime') mg/g of dry wood. Regarding the antitumoral activity, eight wood extracts and four phenolic compounds were evaluated in MCF-7 cells after 48 h of induction, showing the wood extract from cv. 'Songold' and (‒)-annphenone (3), the best antiproliferative activity (IC50: 424 μg/mL and 405 μg/mL, respectively).

Ubiquity of methanogenic archaea in the trunk of coniferous and broadleaved tree species in a mountain forest.

Wetwood of living trees is a habitat of methanogenic archaea, but the ubiquity of methanogenic archaea in the trunk of various trees has not been revealed. The present study analysed methanogenic archaeal communities inside coniferous and broadleaved trees in a cold temperate mountain forest by culture-dependent or independent techniques. Heartwood and sapwood segments were obtained from the trunk of seven tree species, Cryptomeria japonica, Quercus crispula, Fraxinus mandshurica, Acer pictum, Aesculus turbinata, Magnolia obovata, and Populus tremula. Amplicon sequencing analysis of 16S rRNA genes showed that Methanobacteriaceae predominated the archaeal communities and Methanomassiliicoccaceae also inhabited some trees. Real-time PCR analysis detected methanogenic archaeal mcrA genes from all the tree species, with a maximum of 107copiesg-1 dry wood. Digital PCR analysis also detected mcrA genes derived from Methanobacterium spp. and Methanobrevibacter spp. from several samples, with a maximum of 105 and 104copiesg-1 dry wood. The enumeration by the most probable number method demonstrated the inhabitation of viable methanogenic archaea inside the trees; 106cellsg-1 dry wood was enumerated from a heartwood sample of C. japonica. Methanogenic archaea related to Methanobacterium beijingense were cultivated from a heartwood sample of Q. crispula and F. mandshurica. The present study demonstrated that the inside of various trees is a common habitat for methanogenic archaeal communities and a potential source of methane in forest ecosystems.

Experimental and Statistical Determination of Convective Heat and Mass Transfer Coefficients for Eucalyptus nitens Sawn Wood Drying

This study aimed to develop a model using experimentally obtained convective heat and mass transfer coefficients to predict the effect of temperature, humidity, and drying rate on wood drying. Tangential wood samples of Eucalyptus nitens (H. Deane & Maiden) were used in the investigation. The experimental design consisted of two temperature levels (40 °C and 55 °C), two relative humidity levels (55% and 75%), and two air velocity settings (2 m·s−1 and 3 m·s−1). The experiments were conducted under a constant evaporation rate, spanning the maximum and critical moisture content in the wood. A statistical model using multivariate regression was created to predict the convective heat and mass transfer coefficients. The results indicated that the experimental data and empirical correlations exhibited an error margin of 37.77% and 37.86%, respectively. A significant positive correlation was found between the convective heat transfer coefficient and air velocity, temperature, and relative humidity, while the convective mass transfer coefficient showed a significant positive correlation only with air velocity and temperature. The model predicted the convective heat and mass transfer coefficients with high accuracy and statistical significance. Using the proposed method, we successfully obtained both convective coefficients, which enable accurate description of heat and mass flow during the convective drying of Eucalyptus nitens wood.

Multi-scale structural deterioration analysis of archaeological wood from the Shahe Ancient Bridge site in Xi’an, Shaanxi, China

ABSTRACT Due to the unstable variations in moisture content, the wood piles near the ground surface at Shahe Ancient Bridge site have undergone more severe degradation. In this study, two representative wood piles from the site were selected as samples to analyze their deterioration from a multi-scale perspective. The findings suggested that the primary microorganisms of the wood piles contained not only white rot and brown rot fungi commonly found in dry archaeological wood, but also soft rot fungi and erosive bacteria commonly found in waterlogged archaeological wood. The hemicellulose and non-crystalline cellulose were almost completely degraded, and even the cellulose in the crystalline zone underwent some degradation. The microfibrils were fragmented and disoriented. The β-O-4 and β-β bonds in lignin were partially broken, resulting in a decrease in the molecular weight of the lignin. Compared to G-type lignin, S-type lignin demonstrated a higher susceptibility to degradation, potentially explaining why Phoebe sp. wood underwent more extensive degradation than Abies sp. wood. Archaeological wood was not rich in mesopores compared to the reference wood. The results of this study contribute to the understanding of the deterioration state of the Shahe Ancient Bridge site and provide a fundamental understanding for its subsequent protection.

Mathematical modeling and performance evaluations of a wood drying process using photovoltaic thermal and double-pass solar air collectors

This research conducts a novel and complete 4E assessments and introduces an innovative method for examining solar wood drying systems. The software TRNSYS and MATLAB programming are combined to simulate and create a numerical program. This novel combination allows for a thorough examination that goes beyond conventional assessments of wood drying. The aim is to evaluate the effectiveness of a solar wood dryer using two different collectors, a double-pass and a photovoltaic thermal collectors, in terms of four key aspects: energy, exergy, economic, and environmental. Further, the drying process was investigated under various climates in three African cities (Errachidia, Dakar, and Nouakchott). The moisture content of wood was reduced from 74% to 12% in the three cities. Elaborate simulations were performed and the results were confirmed by experimental validation, using methods including Mean Absolute Error, Mean Relative Error, and Root Mean Square Error. The primary findings of this study are the following: In the double-pass dryer, the drying time required in Errachidia, Dakar, and Nouakchott was 139h, 189h, and 170h, respectively. Whereas in the photovoltaic thermal dryer, it needed 192h in Errachidia, 210h in Dakar, and 189h in Nouakchott. Further, using photovoltaic thermal, the dryer exhibited superior exergy efficiency compared to the use of double pass collector. Photovoltaic thermal collector reduces yearly CO2 emissions by an average of 54.87, 66.2, and 44.11 tonnesCO2 in Errachidia, Dakar, and Nouakchott, respectively. In contrast, double pass collector reduces CO2 emissions by an average of 38.49, 57.9, and 38.56 tonnesCO2 in Errachidia, Dakar, and Nouakchott, respectively, throughout the year. Further, the solar dryer, using double pass collector, has a shorter payback time than using photovoltaic thermal collector, indicating a quicker economic return.

Field test of sticker thickness in kiln drying of southern pine

Field test of sticker thickness in kiln drying of southern pine

Prediction of Dielectric Loss Factor of Wood in Radio Frequency Heating and Drying Based on IPOA-BP Modeling

In this paper, an Improved Pelican Optimization Algorithm (IPOA) was proposed to optimize a BP neural network model to predict the dielectric loss factor of wood in the RF heating and drying process. The neural network model was trained and optimized using MATLAB 2022b software, and the prediction results of the BP neural network with POA-BP and IPOA-BP models were compared. The results show that the IPOA-optimized BP neural network model is more accurate than the traditional BP neural network model. After the BP neural network model with IPOA optimization was used to predict the dielectric loss factor of wood, the value increased by 4.3%, the MAE decreased by 68%, and the RMSE decreased by 67%. The results provided by the study using the IPOA-BP model show that the prediction of the dielectric loss factor of wood under different macroscopic conditions in radio frequency heating and drying of wood can be realized without the need for highly costly and prolonged experimental studies.

Dewatering behavior of wet oil palm sawn timber during flat compression

ABSTRACT One obstacle to the industrial processing of oil palm wood is its nearly water-saturated state in green condition and its high tendency to develop cell collapse during kiln drying. This study analyzed mechanical dewatering by flat compression as an alternative pre-drying method for wet oil palm sawn timber. In the process, boards 700 mm long were compressed at ratios of 40% and 60% using a laboratory press, which resulted in water extraction of the free water varying between 38–52% and 60–73%, respectively. Since unperforated press plates were used, the water could only escape over the crosscut and long edges. The extent to which the crosscut and long edges were involved in dewatering was examined, and found to depend on the position of the board in the trunk due to the different water permeability conditions at the different heights. Permeability measurements, therefore, were carried out on cylindrical specimens using a specifically designed testing device. For the analysis of the hydrostatic pressure development in the boards, three pressure transducers were installed at different distances to the crosscut at half board thickness. The analysis of the recovery of compression showed, that the boards recovered to a large extend immediately after compression.

LIQUID PERMEABILITY OF EUCALYPTUS UROPHYLLA WOOD TREATED WITH DIFFERENT DRYING METHODS

In this study, the influence of three different drying methods on the liquid permeability of sapwood and heartwood of Eucalyptus urophylla was investigated. The liquid permeability of the dried wood was assessed by measuring the maximum amount of dyeing solution uptake using the capillary rise method. Subsequently, the microscopic structure of the dried wood was examined by scanning electron microscopy (SEM). The results indicated that the liquid permeability of sapwood dried by microwave vacuum drying (MVD) and conventional kiln drying (KD) was significantly more effective than that of air drying (AD) treated wood. However, there is no significant difference in the effect of MVD and KD on the liquid permeability of sapwood. The liquid permeability of heartwood treated with MVD is significantly better than that treated with KD and AD, and the effect in the effects of AD and KD on the heartwood is not significant. The increased permeability of Eucalyptus urophylla wood can be attributed to the occurrence of macro-cracking or micro-structural damage in the test specimens, resulting from the dislodgement of perforated plates within the wood cells, the rupture of the intercellular layer between vessel and axial parenchyma cells, as well as the rupture of the pit membrane in cross-field pits due to microwave vacuum drying and conventional kiln drying.

Alterations in physico-chemical properties, microstructure, sensory characteristics, and volatile compounds of red pepper (Capsicum annuum var. conoides) during various thermal drying durations

Red pepper (Capsicum annuum var. conoides) is commonly used for dried pepper production in China, and the drying process, particularly the during duration, profoundly affects its quality. The findings indicate that prolonged exposure to high temperatures during thermal drying results in significant darkening, an evident decrease in red and yellow tones, and gradual transformation of the pepper's microscopic structure from granular to compact, along with 88% reduction in moisture content and 81% decrease in thickness. The capsaicinoid content increased, resulting in a 4.3-fold increase in spiciness after drying compared to that of fresh pepper. The pepper aroma shifts from fruity, choking, and grassy to herb, dry wood, and smoky. Compounds such as 2-Acetylfuran, furfural, 2-methylfuran, 1-methylpyrrole, 2-methylpyrazine, and 2,5-dimethylpyrazine exhibited positive correlations with drying time, whereas ethyl 2-methylpropanoate, ethyl butanoate, ethyl 2-methylbutanoate, ethyl hexanoate, and 3-methylbutyl butanoate showed negative correlations, indicating their potential as markers for monitoring thermal drying processes.

Evaluation of conventional and microwave drying of tropical Amazonian wood indicated for the manufacture of EGP (Edge Glued Panels)

Evaluation of conventional and microwave drying of tropical Amazonian wood indicated for the manufacture of EGP (Edge Glued Panels)

Экологические особенности конвективной сушки пиломатериалов

Lumber drying is a mandatory technological operation that gives wood the properties necessary for the production of items, during which the wood is given shape and size stability during operation and/or increases biostability during transportation. Chamber drying is carried out at elevated temperatures, which predetermines the transfer of wood to a chemically active state. As a result, the first stage of extraction is realized – the release of a complex of substances in a solid, liquid and gaseous states onto the surface of the board. With all the variety of substances that accumulate during the growth process in each tree species, phenol and formaldehyde, which are common to all, are released during drying. They belong to class II hazard to humans. In the specialized literature, this issue is given unjustifiably little attention. The problem is complicated by the fact that a significant part of the wood drying production capacity is currently located within the urban area. Therefore, the entire spectrum of substances that are released from the dried wood is concentrated in the residential area, having a negative impact on humans. The aim of the research is to determine the degree of environmental impact of substances released from wood during drying. The list of substances that are released during convective drying from larch and pine wood, as well as data on the amount of these substances, which are given in the article, indicate the presence of an environmental pollution problem. In Russia, the entire volume of lumber for the production of products is dried in drying plants that do not have devices that neutralize pollutants. Consequently, harmful substances released from dried wood accumulate both on the territory of wood processing enterprises and in residential areas. From the above, it follows that drying lumber using low-temperature conditions cannot be considered an environmentally friendly type of production. This problem requires a more detailed study, which will allow us to develop a set of measures to reduce the negative impact of convective lumber drying on the environment.

Preparation and drying characteristics of poplar wood modified by hexacyclite

In recent decades, wood drying has emerged as an important method to ensure wood quality and improve wood utilization. However, the addition of modifiers to wood can hinder the transfer of moisture, making the drying process difficult. Therefore, the drying of modified wood is challenging. This study focuses on poplar wood and reports the preparation of modified wood capable of releasing health-beneficial negative oxygen ions. In particular, this study examined the effect of hexacyclite on the transfer of internal moisture and heat in wood. Hexacyclite was dispersed using sodium hexametaphosphate as a dispersing agent, and the modified poplar wood was prepared via vacuum pressure impregnation. The process involved six cycles of the following treatments: a vacuum treatment (−0.08 MPa, 20 min), followed by a pressure treatment (1 MPa, 120 min), and a final atmospheric treatment (5 min). The modified wood was dried via kiln drying, during which the overall wood temperature rapidly increased, with the total drying rate also increasing by 1.05%/h. The introduction of hexacyclite potentially altered the way modified wood bound with moisture, leading to permanent changes in the porosity of cell walls and the structure of polymers and thus altering the movement of water molecules. The modified wood continuously emitted far-infrared rays with a wavelength of 8–15 μm. In some large water clusters, after the far-infrared energy was absorbed, the movement of water molecules accelerated, thereby increasing the drying rate in the wood below the fiber saturation point. Ultimately, this resulted in the modified wood drying faster and thus exhibiting a better quality.

Moisture and Temperature Profiles of Heartwood Pinus pinaster Ait. Wood Specimens during Microwave Drying

Microwave (MW) drying of wood has gained popularity in the field of wood modification. The rise in temperature during MW drying leads to increased steam pressure, enhancing wood permeability but potentially decreasing mechanical properties. Understanding temperature and moisture behaviors during MW drying is crucial for its industrial application in wood drying. Therefore, this study aimed to characterize the temperature and moisture behaviors during MW drying of small Portuguese maritime pine (Pinus pinaster Aiton.) wood samples to support a wider use of this technology. The effects on water uptake and the compressive strength parallel to the grain were also investigated. The results indicated three distinct phases in the MW drying rates, with an average of 0.085% of water removed per second. Moreover, the temperature underwent three distinct stages: an initial rapid increase, a period of constant temperature, and a slight decrease until drying was complete. At the beginning of MW drying, the temperatures were below 100 °C, with average temperatures ranging from 126 to 145 °C. Specimens with lower initial moisture content had higher temperatures, and a positive correlation was found between initial moisture content and drying time. In contrast, negative correlations were found between the initial moisture content and average temperature, as well as average temperature and MW drying time. Additionally, the operating condition parameters used in MW drying of pine samples enhanced water impregnability by 65%, generating a slight reduction of 11% in compressive strength. It was also noticed that the initial moisture content did not impact MW-dried samples’ water uptake or compressive strength. Finally, although small clear wood samples of maritime pine were utilized, the temperature and moisture patterns observed closely matched real-scale specimens. Thus, the findings corroborate a wide utilization of MW technology for wood drying, mainly demonstrating positive possibilities for structural-sized wood specimens.

Estimation of the earlywood and latewood ratio with different particle size of dry and wet milled Japanese cedar wood flour by using hyperspectral imaging

Mechanical properties of wood–plastic composites are influenced by a particle size and surface morphology of wood flour. Generally various sizes of wood flour are produced from single solid wood even if the single process is used. If the different particle size of wood flour is produced from different wood tissue such as earlywood (EW) and latewood (LW), not only particle size but also density and chemical composition of wood flour might influence the mechanical property of final products. This study aims to investigate the relationship between particle size and their origin; EW and LW. EW and LW were separately milled to produce the EW and LW flour by dry and wet milling. Hyperspectral images ranging 400–1000 nm for each wood flour were used as training data. Discriminant model of EW and LW flour developed by PLS-DA showed over 0.77 of accuracy. Then the EW and LW were dry and wet milled together and screened by three different sieve openings to obtain different particle size wood flour. Discriminant model was applied for the hyperspectral images of each size of wood flour to estimate the EW and LW ratio. The result showed that increasing sieve opening resulted in the increasing ratio of LW for dry milled wood flours. The results suggest that the EW was easily pulverized than LW.

Sulfuryl Fluoride Fumigation as a Quarantine Treatment for the Control of Reticulitermes speratus Kolbe (Blattodea: Rhinotermitidae) in Wood.

High-risk termites in wood imported to the Republic of Korea are currently treated with methyl bromide (MB), which has ozone-depleting properties and is highly toxic. This study evaluated the effectiveness of sulfuryl fluoride (SF) as a quarantine treatment against Reticulitermes speratus Kolbe (Blattodea: Rhinotermitidae) in wood, along with its wood sorption and penetration capacity. The LCt50 and LCt99 values for SF were 30.87 and 42.53 mg h/L at 23 °C and 151.62 and 401.9 mg h/L at 5 °C, respectively. The SF Ct values did not significantly differ between dry and wet wood at loading ratios of 10%, 30%, and 50% at both 5 °C and 23 °C (p > 0.05). In a closed wooden cube, the LCt50 and LCt99 for SF for R. speratus were 31.59 and 53.34 mg h/L, respectively, indicating an excellent wood penetration ability. SF caused 100% termite mortality with a 90% loading ratio in the scale-up trials (500 L). The SF concentration during ventilation decreased below the threshold limit value (TLV) of 5 ppm within 30 min, confirming that the working conditions were safe. This study provides a basis for the use of SF as an alternative to MB for the treatment of termites in wood.