Simple Method For Preparation Research Articles

Constructing mesoporous biochar derived from waste carton: Improving multi-site adsorption of dye wastewater and investigating mechanism

The development of cost-efficient biochar adsorbent with a simple preparation method is essential to constructing efficient wastewater treatment system. Here, a low-cost waste carton biochar (WCB) prepared by a simple two-step carbonization was applied in efficiently removing Rhodamine B (RhB) in aqueous environment. The maximum ability of WCB for RhB adsorption was 222 mg/g, 6 and 10 times higher than both of rice straw biochar (RSB) and broadbean shell biochar (BSB), respectively. It was mainly ascribed to the mesopore structure (3.0–20.4 nm) of WCB possessing more spatial sites compared to RSB (2.2 nm) and BSB (2.4 nm) for RhB (1.4 nm✕1.1 nm✕0.6 nm) adsorption. Furthermore, external mass transfer (EMT) controlled mass transfer resistance (MTR) of the RhB sorption process by WCB which was fitted with the Langmuir model well. Meanwhile, the adsorption process was dominated by physisorption through van der Waals forces and π-π interactions. A mixture of three dyes in river water was well removed by using WCB. This work provides a straightforward method of preparing mesoporous biochar derived from waste carton with high-adsorption capacity for dye wastewater treatment.

Fabricating of poly(vinyl alcohol)/halloysite nanotubes/gelatin composite sponges with enhanced mechanical properties and rapid water absorption speed

AbstractIn the biomedical field, polyvinyl alcohol (PVA) sponge has been widely used. In particular, it is considered a potential implant material for repairing soft tissues. However, its insufficient water absorption and mechanical properties limit its application. In this work, a novel PVA/halloysite nanotubes (HNTs)/gelatin ternary composite sponge was prepared by water solution mixing and casting techniques. HNTs and gelatin/PVA solution were mixed at different weight ratios. The structure of the ternary composite sponges was characterized by using scanning electron microscopy. The physical properties of the ternary composite sponges were characterized. The maximum water absorption reached 1783.5% with a rapid water absorption speed at a weight ratio of HNTs/gelatin of 1:8. Owing to its interconnected macroporous structure and good interfacial interaction, its highest compression strength and tensile strength reached 8.22, 1.51 MPa, respectively. In addition, its thermal stability was enhanced as well, which demonstrated that the prepared composite sponge had better performance than the pure PVA sponge by constructing a ternary system. Therefore, the results suggest that the PVA/HNTs/gelatin ternary composite sponge shows a wider application value as a potential material for repairing soft tissue.Highlights A composite PVA sponge with promising applications in tissue engineering. Simple preparation method, water solution mixing and casting techniques. Pioneering a PVA/HNTs/gelatin ternary system sponge. Improved water absorption ability and mechanical properties.

Highly Sensitive Flexible Capacitive Pressure Sensor with Porous Hierarchical Structure Realized by a Microwave Curing Method

The introduction of porous hierarchical microstructures effectively improves the sensitivity of flexible pressure sensors. However, it is difficult to achieve porous hierarchical microstructures for pressure sensors through inexpensive, efficient, and simple preparation methods. Herein, a hemispherical array with porous hierarchical microstructure is prepared on polydimethylsiloxane substrate using a simple one‐step microwave curing process with glucose as porogen. Furthermore, the flexible electrode based on the polydimethylsiloxane substrate is combined with an ionic liquid polymeric gel membrane to obtain a flexible capacitive pressure sensor. Thanks to the deformability of porous hierarchical microstructure and the double‐dielectric layer effect of ionic liquid polymeric gel membrane, the sensor displays an ultrahigh sensitivity of 131.21 kPa−1 within 0–1 kPa. Meanwhile, the sensor has short response time, excellent dynamic loading stability, as well as excellent long‐term stability (>3000 cycles). In application testing, the sensor effectively monitors various physiological activities like pulse, breathe, speech, and swallowing, demonstrating its good prospects in the field of health electronics. Most importantly, the proposed microwave curing method can realize the preparation of porous hierarchical structure on flexible substrate through a one‐step process, which offers a fresh way for the economical, green, and efficient preparation of high‐sensitivity capacitive pressure sensors.

A simple method for microwave-assisted preparation of tire samples

Heavy metals content in tires affects the safety of soil and agricultural products. The digestion method is a pretreatment for determining heavy metals in tire samples, and will affect the efficiency and accuracy of the heavy metal determination. The microwave digestion process and reagents for tire samples are not currently standardized. Therefore, this study attempts to provide an appropriate method of resolution for scholars. All digestion processes were performed in Mars One. We tested 15 different acid mixtures to determine the best reagent type and dose and then investigated the effect of maximum temperature, holding time, and sample grams on the degree of digestion. In summary, the best condition to digest the tire sample was a mixture of 3 ml HNO3 and 7 ml H2SO4, taking 0.1 (± 0.0005) g tire sample, at the maximum digestion temperature of 220 °C for 25 min. The experimental conclusion will provide a reliable experimental method for scientists using MARS One to study heavy metals in tires. At the same time, researchers using the MARS series can also find valuable references in this paper.

Balanced Devil Triangle: A Satisfactory Comprehensive Performance Magnetorheological Fluids with Cross‐Scale Particles

AbstractMagnetorheological (MR) fluids are magnetic responsive smart materials that are widely used in real‐time damping adjustment devices. However, a major challenge for MR fluids is balancing the constraints relationship among various key performances. This study demonstrates that by utilizing home‐made high saturation magnetization (208.0 emu g−1) nanoparticles as the second component in the preparation of cross‐scale bidisperse MR fluids, the shortcomings of monodisperse micron particles performance can be compensated, effectively balancing the relationship between various performances. This is attributed to the fact that the addition of nanoparticles enhances the density of chain structures under an applied magnetic field, while reducing the overall particle density without a magnetic field. By replacing part of micron particles with nanoparticles, the phenomenon of significant increase in zero‐field viscosity caused by the direct introduction of nanoparticles is avoided. The optimal content of nanoparticles in MR fluids is preliminarily explored, and the results indicate that Micro‐Nano bidisperse MR fluids exhibit a high dynamic yield strength (58.3 kPa when 436 kA m−1), excellent sedimentation stability (82.6% when 7 days), suitable zero‐field viscosity (1.25 Pa s when 100 s−1), and ideal reversibility. Most importantly, the simple preparation method adds significant engineering application value to these MR fluids.

Rapid room-temperature synthesis of porous Sulfur-doped nickel-chromium-Layered Double Hydroxide for oxygen evolution catalysis in seawater splitting

Seawater splitting is a promising and sustainable technology for producing high-purity hydrogen, but its commercial application remains a major challenge due to the kinetically slow oxygen evolution reaction (OER) and severe corrosion in practical applications. In this work, we report a single-step approach to grow a highly porous Sulfur-doped nickel-chromium-Layered Double Hydroxide (S-doped NiCr-LDH) catalyst on Ni foam at room temperature. This rapid approach efficiently designs the surface of Ni foam into a porous S-doped NiCr-LDH layer with outstanding hydrophilic characteristics. The catalyst exhibits outstanding OER performance in alkaline freshwater and alkaline seawater electrolytes, requiring overpotentials of only 270 and 342 mV to achieve current densities of 100 mA cm−2, while also exhibiting an extremely long endurance of over 80 h. This simple OER catalyst preparation method could advance the development of hydrogen production from seawater splitting.

Highly elastic, frost-resistant and antimicrobial flexible sensor inspired by ramen noodles for human motion detection and deep learning of handwritten content

Biomaterial-based hydrogels have gained significant attention in the development of flexible multifunctional electronic devices for the future. However, it is a great challenge to prepare biomaterial-based hydrogels with high toughness, electrical conductivity and frost-resistant by a simple and low-cost way. Meanwhile, starch bio-based hydrogels have emerged as a popular area of research due to their abundant sources and degradability. Unfortunately, these hydrogels often exhibit poor mechanical properties and freeze resistance, which restrict their practical applications. Taking inspiration from the traditional food ramen, where a simple mixture of noodles can become remarkably stretchable and resilient, our study aims to enhance the performance of hydrogels by leveraging their toughening mechanism. We achieve this by combining polyvinyl alcohol (PVA), branched chain starch (Amy), wheat protein (WP), ethylene glycol (EG) with saline. The Amy/PVA/EG/WP/S (APEWS) organohydrogels demonstrated excellent mechanical properties (1.12 MPa) due to the combination of PVA as a hard backbone, a rich protein network, diverse functional groups, and saline components. Additionally, the binary solvent consisting of water and EG allowed the hydrogel to function effectively even at low temperatures (-20 °C). The APEWS organohydrogel exhibited promising sensing capability (GF = 1.46) and sensing stability (>500 times) as a human wearable strain sensor, making it suitable for detecting human motion and the hydrogel showed excellent antimicrobial properties against Escherichia coli (Gram-negative bacteria). Furthermore, we employed a Long Short-Term Memory (LSTM) artificial neural network for deep learning-based recognition of written content. The network achieved an accuracy of over 95.5% for different English letters and 100% for symbols. These results highlight the potential of this technology in applications such as writing sensing and information encryption. In conclusion, with the simple preparation method and low cost, APEWS organohydrogels are expected to be the next generation of green and sustainable bio-based strain sensors.

Molecular mechanism and experimental study of fuel oil extractive desulfurization technology based on ionic liquid

In recent years, the sulfur-containing substances produced by fossil fuel combustion have caused overwhelming pollution to the ecological environment, and fuel desulfurization research is imperative. In this paper, 16 ionic liquids (ILs), which are environmentally friendly, easily degradable and have good prospects for industrial application, were selected by combining four cations and four anions for fuel desulfurization research. The desulfurization mechanism of ILs was first investigated by molecular mechanism studies, in which quantum chemical simulations were used for preliminary screening based on the selectivity coefficient of infinite dilution activity coefficient. And the experimental study of extraction desulfurization was carried out with dibenzothiophene (DBT) and n-heptane as model oils. The above mechanism study and experiments examined the effects of temperature, initial fuel oil concentration and ILs to fuel oil feed ratio on the extraction efficiency, and the results showed that both [C2COOCH3ImC6H13][N(CN)2] and [C2COOCH3ImC6H13][NTF2] ILs have more prominent extraction properties. Among them, [C2COOCH3ImC6H13][NTF2] exhibits high desulfurization efficiency for a wide range of sulfur concentration in fuel oils at room temperature due to the advantages of simple preparation method and easier industrialization of the [C2COOCH3ImC6H13][NTF2]. The above experimental results are fully consistent with the molecular simulation predictions, indicating that the theoretical study and experimental method proposed in this paper are simple and feasible.

Investigation of Glucose Sensing via Controlled Copper Concentration in CuO for Non-Enzymatic Glucose Biosensor

Non-enzymatic glucose sensors have emerged as pivotal tools for monitoring blood glucose levels, offering advantages over traditional enzymatic methods in terms of sensitivity, selectivity, and cost-effectiveness. This study explores the utilization of a simple and low-cost method for preparation of copper oxide (CuO) nanostructures to look for the non-enzymatic glucose sensing. Morphological and structural analysis via Scanning Electron Microscopy and X-ray diffraction of synthesized CuO nanostructures revealed nearly same size, shape, and a pure monoclinic crystal structure. Fourier transform infrared spectroscopy further confirmed the monoclinic phase. More importantly, we employed CuO nanostructures-modified glassy carbon electrodes (GCE) to investigate the glucose sensing and sensing parameters. The electrodes exhibited comparable sensitivity, selectivity, and an extended dynamic range 0.4–0.6 V applied potentials with regard to earlier reports. Amperometric responses of lower concentration based synthesized CuO sample recorded at 0.5 V unveiled a low limit of detection of 5.9 μM, a sensitivity of approximately 10.6 μA/(mM·cm2), and a rapid 2 s response time. Manipulating the CuO-nanostructures and integrating on the GCE can offer a promising opportunity for enhanced non-enzymatic glucose sensing with high sensitivity, selectivity, and broad dynamic range towards utility in real-time glucose monitoring, contributing to improved healthcare diagnostics and diabetes management.

Preparation of Metformin Biodegradable Polymeric Microparticles by O/O Emulsion Solvent Evaporation: A 32 Full Factorial Design Approach

Background: Sustained release of synthetic polymeric microparticles has gained more attention as drug delivery carriers because of their properties such as good stability, low toxicity, dosing frequency, and simple and mild preparation method. The present work was envisaged to reduce the dosing frequency by preparing drug loaded biodegradable microspheres by the O/O emulsion solvent evaporation technique. Objective: The objective behind microspheres’ preparation is to sustain the metformin release by using ethyl cellulose as a synthetic polymer. The model drug metformin having a low biological half-life (1.5-3 hours) is selected. Methods: As the metformin is highly water soluble in nature, the oil-in-oil solvent evaporation techniques are used and span 80 is utilized as surfactant. The effect of stirring rate and surfactant concentration on the characteristics of encapsulation efficiency and drug release from the microsphere are investigated. Results: The results show that the drug-polymer (1:1) ratio gives better sustained release results. The obtained microparticles are characterized by X-RD analysis and Fe-SEM, and release behavior is checked for release patterns. A 32 full factorial design is employed for the responses. The free-flowing spherical microspheres show high drug entrapment efficiency. Conclusion: The data obtained suggest that microspheres can be successfully designed with sustained release for diabetic treatment.

Metal-organic framework (MOF)-derived flower-like Ni-MOF@NiV-layered double hydroxides as peroxidase mimetics for colorimetric detection of hydroquinone

BackgroundNanozymes are one of the ideal substitutes for natural enzymes because of their excellent chemical stability and simple preparation methods. However, due to the limited catalytic ability of most reported nanozymes, constructing nanomaterials with low cost and high activity is gradually becoming an exploration focus in the field of nanozymes. Heteroatom doping of metal-organic frameworks is one of potential approaches to design nanozymes with high catalytic performance. Due to their multiple valence states properties, V-doped metal-organic framework (MOF)-derived LDH is expected to be a good enzyme-like catalyst. To our knowledge, the V-doped MOF-derived LDH as nanozyme is not explored before. ResultsWe report the in-situ synthesis of NiV-layered double hydroxides (LDHs) on nickel-based MOF, i.e. Ni-MOF@NiV-LDHs. The MOF surface is covered by 2D nanosheets. This unique structural design increases the specific surface area of the material, enables more exposure of catalytic active sites to participate in reactions and accelerates the electron transfer rate. The Ni-MOF@NiV-LDHs have high peroxidase-like activity able to catalyze TMB oxidation by H2O2 via the generation of •OH and O2•−. Relative to Ni-MOF, the Ni-MOF@NiV-LDHs shows 47-fold peroxidase-like activity rise. It had good affinity to TMB and H2O2, with the Michaelis-Menten constants of 0.12 mM and 0.007 mM, respectively. The hydroquinone (HQ) consumed the reactive oxygen species generated in the TMB + H2O2+Ni-MOF@NiV-LDHs system to inhibit the TMB oxidation. On this basis, a sensitive and rapid assay for determining HQ was developed, with a linear range of 0.50–70 μM and a LOD of 0.37 μM. SignificanceThis work provided some clues for the further development of novel nanozymes with high catalytic performance via a strategy of heteroatom doping. And the constructed colorimetric analysis method was successfully utilized for the determination of HQ in actual waters, which has the potential for practical application in the analysis of environmental pollutants.

Robust 2D layered MXene matrix–boron carbide hybrid films for neutron radiation shielding

Large-scale fabrication of neutron-shielding films with flexible or complex shapes is challenging. Uniform and high boron carbide (B4C) filler loads with sufficient workability are needed to achieve good neutron-absorption capacity. Here, we show that a two-dimensional (2D) Ti3C2Tx MXene hybrid film with homogeneously distributed B4C particles exhibits high mechanical flexibility and anomalous neutron-shielding properties. Layered and solution-processable 2D Ti3C2Tx MXene flakes serve as an ideal robust and flexible matrix for high-content B4C fillers (60 wt.%). In addition, the preparation of a scalable neutron shielding MXene/B4C hybrid paint is demonstrated. This composite can be directly integrated with various large-scale surfaces (e.g., stainless steel, glass, and nylon). Because of their low thickness, simple and scalable preparation method, and an absorption capacity of 39.8% for neutrons emitted from a 241Am–9Be source, the 2D Ti3C2Tx MXene hybrid films are promising candidates for use in wearable and lightweight applications.

Supramolecular cellulose-based heavy metal adsorbent for efficient and accurate removal of cobalt (II) for water treatment

Heavy metal ions' high toxicity, carcinogenicity, and non-degradability have been identified as the most severe environmental concerns. Therefore, in this study, a new type of cellulose-based ionic imprinting adsorbent (p-CMs@EPI@PEI@Cys-IIP) with a three-dimensional pore structure was developed to selectively adsorb cobalt (II) using a simple ion-cross-linking technique. In this experiment, p-CMs@EPI@PEI@Cys-IIP were prepared by modifying cellulose microspheres (p-CMs) with epichlorohydrin (EPI), polyethyleneimine (PEI) and L-cysteine (L-Cys).The p-CMs@EPI@PEI@Cys-IIP was found to be able to selectively adsorb Co (II), and it was well characterized with FT-IR, SEM, TGA, and XRD. The system adsorption experiment proved that the maximum adsorption capacity reached 158.93 mg g-1, below the pH 7. After five cycles, the adsorption capacity of p-CMs@EPI@PEI@Cys-IIP still remained above 90%. The results of selectivity experiments indicated that p-CMs@EPI@PEI@Cys-IIP has preferential selectivity for Co (II). The adsorption isotherm and kinetic experiment of Co (II) conformed to the Langmuir model and pseudo-second-order kinetic, respectively. The adsorption process of Co (II) on p-CMs@EPI@PEI@Cys-IIP was also affected by the intra-particle diffusion model. Due to its simple preparation method and good adsorption performance, p-CMs@EPI@PEI@Cys-IIP would have a good application prospect in the selective removal of Co (II) for water treatment.

Cesium lead bromide perovskite nanocrystals for the visual detection of chloride ions: A review

Lead halide perovskite nanocrystals (NCs) have been extensively studied due to their high quantum yield, high color purity, tunable band gap, and simple preparation methods. Among them, cesium lead bromide perovskite NCs (CsPbBr3 NCs) have the characteristics of good stability performance, better luminous performance, and good halide exchange properties, etc., and a visual sensing system for fluorescence wavelength shift can be constructed by using their spectral tunability. Accordingly, CsPbBr3 has become a potential candidate material for on-site detection of chloride ions, providing possibility for tunable visual analysis, which not only expands the application potential of CsPbBr3 NCs in the detection field, but also greatly improves the visual fluorescence sensing method. On a basis of the halide exchange property of CsPbBr3 NCs, this review introduces the development strategy of perovskites as the probes to detect chloride ions in the environments of liquids, solids, and gases, and summarizes and prospects the new methods of chloride detection over CsPbBr3 NCs. In addition, this review provides an overview of existing challenges, providing reference for the development of highly sensitive and long-term stable chloride probes based on lead halide perovskites.

Cyanide determination in postmortem blood samples using Headspace-Ion Mobility Spectrometry (HS-IMS)

Interest in facile and sensitive methods for cyanide detection is related to the extreme cyanide toxicity and its importance in forensic toxicology. In this research a novel application of Ion Mobility Spectrometry (IMS) was demonstrated for rapid determination of cyanide poisoning in postmortem toxicology. In addition, a simple method for the sample preparation was applied based on the analyte (cyanide anion) transfer as HCN to the headspace and direct injection to IMS. The method showed a linear dynamic range of 50–2000 µg/L with R2 > 0.99, a high sensitivity (LOD of 20.4 µg/L and LOQ of 68.1 µg/L). Good repeatability (intra- and inter-assays, CV < 15 %) and excellent extraction recovery (82 -94 %) were obtained. After validation, the method was applied in the analysis of postmortem human blood samples in forensic cases. In all samples, the cyanide was promptly quantified.

Patterned Liquid-Metal-Enabled Universal Soft Electronics (PLUS-E) for Deformation Sensing on 3D Curved Surfaces.

Liquid metals with metallic conductivity and infinitely deformable properties have tremendous potential in the field of conformal electronics. However, most processing methods of liquid metal electronics require sophisticated apparatus or custom masks, resulting in high processing costs and intricate preparation procedures. This study proposes a simple and rapid preparation method for patterned liquid-metal-enabled universal soft electronics (PLUS-E). The utilization of selective adhesion of the liquid metals on stretchable substrates and the adaptive toner mask enables rapid fabrication (<2 s/100 cm2), excellent stretchability (800% strain), and high forming accuracy (100 μm). Benefiting from the adaptive deformation of the substrate and toner mask, PLUS-E can be conformally applied to any shape of 3D surfaces. Besides, the stability of PLUS-E on 3D surfaces is improved by low-fluidity liquid metal composites. The finite element simulation is used to accurately forecast the deformation and resistance changes of the PLUS-E, and it provides guidance for device design and manufacturing. Finally, this method was utilized to develop various sensors for detecting human motion, catheter bending, and balloon expansion. All of them have obtained stable and reliable signal measurements, demonstrating the usefulness of PLUS-E in real-world applications.

Super porous α‐, β‐, γ‐cyclodextrin cryogels with high active agent loading and controllable release profiles

AbstractCyclodextrins (CDs) are truncated cone‐like structures that are natural cyclic oligosaccharides. Here, a simple preparation method for super porous poly(α‐CD), poly(β‐CD), and poly(γ‐CD) cryogels crosslinking with divinyl sulfone at 150%, 100% and 125% mole ratios with respect to the α‐CD, β‐CD, and γ‐CD molecules, respectively, under cryogenic conditions, is reported. The interconnected homogeneous pore distribution of CD‐based cryogels with pore sizes in the range of 5–100 μm is confirmed by SEM analysis. The CD‐based cryogels weighing 10 mg are determined as hemocompatible with &lt;1% hemolysis ratios and &gt;79% blood clotting indexes; whereas the same materials weighing 1 mg are biocompatible with &gt;75% cell viability on L929 fibroblasts. Additionally, active agent adsorption/delivery efficiencies of CD‐based cryogels utilizing two active agents, Bisphenol A (BPA, a carcinogenic compound) and Curcumin (CUR, a polyphenolic compound), are individually evaluated. It was revealed that p(γ‐CD) cryogels exhibited the highest active agent loading capacity for BPA, 87 ± 13 mg/g, whereas p(α‐CD) cryogels showed the highest loading capacity for CUR, 136 ± 4 mg/g. Moreover, the active agent release from p(α‐CD), p(β‐CD), and p(γ‐CD) cryogel networks at pH 7.4 and 37°C were determined as 40.6 ± 2, 35.3 ± 2, and 34 ± 1 mg/g for BPA, and 1.07 ± 0.2, 1.27 ± 0.1, and 1.37 ± 0.1 mg/g for CUR, respectively, within 96 h.

A Simplified, Efficient and Rapid DNA Extraction Protocol from Rice Grains and Leaf

DNA extraction is very complicated with different plant species because the presence of secondary metabolites that hinder with DNA isolation processes and application like DNA restriction, Gene amplification, as well as gene cloning. A simple method for preparation of rice genomic DNA was developed. The current study expressed comparatively rapid, cost-effective, less time consuming, methods for DNA extraction from seed, young leaves and old leaves of rice genotypes without using liquid nitrogen, phenol, and β–mercaptoethanol in extraction buffer. Using this method, high quality and quantity of genomic DNA was get from 0.5 g of rice seed, young leaves and 75 days old leavesand extracted total nucleic acids (genomic DNA) were amplified by employing single sequence repeats (SSR) or microsatellite markers, which produced reproducible results.This protocol resolves the problems of DNA degradation, contamination, and low yield due to binding and/or coprecipitation with starches and polysaccharides.

Electrotransformation of Foodborne Pathogen Cronobacter sakazakii by a Simple Method.

Cronobacter sakazakii is an opportunistic foodborne pathogen that mainly infects infants and immunocompromised people, with a high mortality rate. However, the efficient transformation method of this bacterium has not been systematically reported. In this study, we developed a fast and efficient transformation method for C. sakazakii by cold sucrose treatment. Compared with CaCl2 or glycerol treatment, the transformation efficiency of this method is significantly high when bacteria were cultured overnight at 42°C before cold sucrose treatment. Furthermore, applying this method, we successfully knocked out the pppA gene by direct electroporation. Collectively, our study provides a simple, time-saving, and efficient method for competent cell preparation of C. sakazakii, which is conducive to the further research of C. sakazakii.

Robust functionalized cellulose-based porous composite for efficient capture and ultra-fast desorption of aqueous heavy metal pollution

The heavy metal pollution control industry requires convenient and cost-effective solutions to address complex aqueous environment. Adsorption method can be an effective strategy to realize these goals. Considering the importance of environmental and sustainable development strategies, there is an urgent need to develop efficient, green and non-toxic heavy metal adsorbents. In this work, a robust aminated cellulose-based porous adsorbent (PGPW) was developed from delignified wood and amino-rich polymer using a solvent-free, mild, simple and efficient preparation method. Such adsorbent exhibited excellent adsorption capacity (188.68 mg g−1) for Cu(II), and its adsorption behavior was consistent with pseudo-second order kinetic and Langmuir isotherm models. Notably, PGPW with superior compressibility could be squeezed to achieve rapid desorption and reach equilibrium within 5 min, while still retaining 87 % adsorption efficiency after 50 cycles. In addition, PGPW showed remarkable selectivity towards various coexisting ionic systems and demonstrated a considerable adsorption capacity in natural water applications. The adsorption mechanism of heavy metal ions on porous adsorption material was elucidated. This approach provides a simple, gentle and sustainable strategy for preparing functionalized wood-based composites with efficient adsorption and ultra-fast desorption of heavy metal ions.