Rubber Particles Research Articles

Can rubberized-asphalt comprising tire-derived aggregates produced through dry process be an alternative subsurface road material?

The major objective of this study was to investigate the suitability of utilizing tire-derived aggregates (TDA) at varying contents for the design of rubberized-asphalt base / subsurface layers through the dry process, along with (i) understanding the cracking potential and mechanical stress-strain response of the different materials under cyclic and confining stresses through triaxial resilient modulus (MR), dynamic modulus |E*|, and static semi-circular bend test, and (ii) assessing bonding strength of TDA with binder-aggregate matrix through moisture susceptibility test. The scope encompassed preparation of ten base course mixtures: one unbound granular base (UGB), three cement treated base (CTB), two asphalt treated base (ATB), and four rubberized-asphalt treated base (RATB) and obtaining mechanical performance at varying temperature-frequency combinations totaling 2636 data points. Triaxial MR tests indicated that CTB mix displayed highest modulus followed by ATB and RATB mixes, which was then followed by the UGB mix mainly ascribed to cement / asphalt treatment of the unmodified control subsurface material. Further, a finite element modeling study helped optimize the confinement levels to obtain realistic |E*| of ATB and RATB mixes. |E*| test results depicted that RATB mixtures would be rut-resistant at higher temperatures as they performed similar to the ATB mixes as well as crack-resistant at low to intermediate temperatures with significantly lower |E*| than ATB mixes, attributed to slower rate of change of viscosity with changing temperature in conjunction with enduring viscoelastic property (1.5–3 times higher phase angle than ATB) ascribed to high asphalt binder content and resilient nature of the rubber particles. Albeit the fracture toughness of ATB was twice higher than RATB, the latter had higher fracture energies, mainly due to the resiliency rendered by the rubber inclusions in concert with the extra viscous effect provided by the rubber-asphalt binder conglomerate. Based on the performance-based ranking, RATB mixes performed better than control mixes, and thus were adjudged as the most suitable alternative subsurface / base course materials in a pavement system. It is envisioned that this research will advance the current understanding of utilizing TDA in asphalt base / subbase courses using the dry process, and further assist in judging the viability of using rubberized-asphalt as potential sustainable alternatives to conventional systems to develop futuristic resilient pavement infrastructures with a strong emphasis on recycling of end-of-life tires, conservation of materials, and circular economy.

Discussion on ‘engineering properties of clay soil stabilised with glass powder and rubber particles – a comparative study’ [geomechanics and geoengineering (2023), 1–25, DOI: 10.1080/17486025.2023.2288927]

ABSTRACT We read with great interest the recent article by Anglaaere et al. (2023). In this article, clay soil with various contents of glass powder (GP) and tyre shred particles (TSP) were subjected to direct shear and California Bearing Ratio (CBR) test, and shear strength (τ) parameters and bearing capacity were reported, respectively. Furthermore, Anglaaere et al. (2023) have performed a correlation analysis and proposed a relationship between the CBR values and τ of the samples. The results presented by Anglaaere et al. (2023) might have been useful, but there are various issues associated with this article, which we want to bring to the attention of the authors, readers, and researchers. We further emphasise that this discussion article would eliminate the dissemination of errors in the scientific knowledge presented by Anglaaere et al. (2023), and will also open new perspectives to the readers and the research fraternity.

Enhanced carbon black exfoliation through elongational flows for faster and higher value-added rubber recycling

The recycling of rubber featuring intricate three-dimensional crosslinked networks necessitates the application of cutting-edge technology and specialized machinery. In this study, the rubber was recycled by mechanochemistry under elongational flow field. The crosslink bonds in the rubber were rapidly broken through the high extension of molecular chains, without the need for additives or additional refinements. At 200 °C, the waste rubber is devulcanized in only 2 min so that the sol molecular weight reached an impressive 3.3 × 104 g/mol, and the mechanical properties of the reclaimed rubber were significantly enhanced, reaching a tensile strength of 17.44 MPa. The elongational flow field devulcanizes the waste rubber while simultaneously achieving rapid refinement of rubber particles and exfoliating the carbon black from the crosslinked network. These making reclaimed rubber forms a micro-nano microstructure in natural rubber (NR), which makes particle reinforcement of the NR-matrix. Faster and high-value-added rubber recycling achieved successfully through elongational flows.

Control of the rubber particle size and phase structure for the design of transparent methacrylate-acrylonitrile-butadiene-styrene resin with excellent performance

Control of the rubber particle size and phase structure for the design of transparent methacrylate-acrylonitrile-butadiene-styrene resin with excellent performance

Axial compression performance of rubberized concrete-filled steel tubular stub columns after fire exposure: Experimental investigation and calculation models

Rubberized concrete (RuC) has emerged as a promising eco-friendly solution for structural elements, offering improved energy dissipation, damping characteristics, and ductility. Incorporating rubber particles into concrete-filled steel tubular (CFST) columns presents an environmentally conscious alternative for various structural applications. However, understanding its performance post-fire is crucial for safe design application, an area currently lacking comprehensive research. This study investigates the structural behavior of sixteen axially loaded circular RuCFST columns after exposure to fire. The columns, with diameters of 219 mm and 377 mm, are filled with normal concrete and RuC, containing 5 %, 15 %, and 30 % replacement of natural fine and coarse aggregate with rubber particles. Following ISO-834 fire standards, the specimens undergo elevated temperatures and subsequent application of compressive axial loads to determine their post-fire behavior. Analysis includes examination of failure modes, temperature-time relationships, axial load-deformation curves, and strain and stress development in the columns. Microstructural analysis using scanning electron microscopy (SEM) and energy dispersive X-ray spectroscopy (EDS) is conducted to study internal morphology before and after exposure to high temperatures. Results indicate non-uniform and nonlinear distributions of maximum temperatures across cross-sections, with historical temperature affecting residual capacity more significantly with increased rubber content and decreased column size. Load-bearing capacities decrease by up to 30 % and 22 % for small and large RuCFST columns, respectively, after exposure to fire. Residual axial stiffness also declines, with reductions of nearly 55 % and 42 % for small and large columns, respectively. In contrast, ductility improves in fire-exposed specimens, with columns having a 30 % rubber replacement ratio showing the highest enhancement. A novel method for calculating post-fire residual load capacity based on the average historical maximum temperature is introduced, demonstrating high accuracy and offering a valuable tool for assessing and reinforcing RuCFST columns after fire exposure.

Genome-Wide Analysis of the SRPP/REF Gene Family in Taraxacum kok-saghyz Provides Insights into Its Expression Patterns in Response to Ethylene and Methyl Jasmonate Treatments.

Taraxacum kok-saghyz (TKS) is a model plant and a potential rubber-producing crop for the study of natural rubber (NR) biosynthesis. The precise analysis of the NR biosynthesis mechanism is an important theoretical basis for improving rubber yield. The small rubber particle protein (SRPP) and rubber elongation factor (REF) are located in the membrane of rubber particles and play crucial roles in rubber biosynthesis. However, the specific functions of the SRPP/REF gene family in the rubber biosynthesis mechanism have not been fully resolved. In this study, we performed a genome-wide identification of the 10 TkSRPP and 2 TkREF genes' family members of Russian dandelion and a comprehensive investigation on the evolution of the ethylene/methyl jasmonate-induced expression of the SRPP/REF gene family in TKS. Based on phylogenetic analysis, 12 TkSRPP/REFs proteins were divided into five subclades. Our study revealed one functional domain and 10 motifs in these proteins. The SRPP/REF protein sequences all contain typical REF structural domains and belong to the same superfamily. Members of this family are most closely related to the orthologous species T. mongolicum and share the same distribution pattern of SRPP/REF genes in T. mongolicum and L. sativa, both of which belong to the family Asteraceae. Collinearity analysis showed that segmental duplication events played a key role in the expansion of the TkSRPP/REFs gene family. The expression levels of most TkSRPP/REF members were significantly increased in different tissues of T. kok-saghyz after induction with ethylene and methyl jasmonate. These results will provide a theoretical basis for the selection of candidate genes for the molecular breeding of T. kok-saghyz and the precise resolution of the mechanism of natural rubber production.

Genetic analysis of agronomic and physiological traits associated with latex yield revealed complex genetic bases in Hevea brasiliensis

Hevea brasiliensis, a natural rubber producing species, is widely cultivated due to its high rubber yield potential. Natural rubber is synthesised in the rubber particles of laticifers. Latex diagnosis (LD) was established to characterise the physiological state of the laticiferous system by measuring its physiological parameters, i.e., sucrose, inorganic phosphorous (Pi), thiols and total solid content (TSC). Rubber clones are often classified in three groups i.e., quick starters, medium starters and slow starters. To better understand the genetic bases of latex yield, a biparental population was generated from a cross between the quick-starter clone PB 260 and the medium-starter clone SP 217. LD was performed during the peak latex production season and used to calculate sucrose loading. The agronomic and physiological parameters associated with latex yield led to the classification of genotypes according to the rubber clonal typology and to the identification of quantitative trait loci (QTL) using a high-density map. Inorganic phosphorous content was positively associated with yield during the first year of production thus enabling identification of quick-starter clones. In addition, the LD-based clonal typology led to determine the long-term yield potential and the use of appropriate ethephon stimulation. QTL analysis successfully identified several QTLs related to yield, sucrose, Pi and TSC. One QTL related to sucrose loading was identified in the same position as the QTL for sucrose on linkage group 1. To our knowledge, this is the first study to report QTL analysis for this trait. The use of a high-density map enables the identification of genes underlying QTLs. Several putative genes underlying QTLs related to yield, sucrose and TSC were identified.

Study on delamination characteristics and mechanical properties of cemented waste rock backfill with rubber aggregation

Since some phosphorus mines use raw ore as a product and do not conduct beneficiation around the mines. This makes it difficult for the amount of waste rock to prepare enough backfill for the filling of underground mined-out areas. Using rubber particles made of waste tires to replace part of the waste rock aggregate (WRA) can not only solve the problem of insufficient WRA, but also improve the environmental problems caused by the large accumulation of waste tires. However, due to the small density of rubber and high density of waste rock, the phenomenon of segregation delamination may occur in the cemented backfill, thus affecting the mechanical properties of cemented waste rock backfill (CWRB). To this end, the effect of rubber aggregate (RA) on the segregation delamination of CWRB was determined by using the section image analysis method of specimens, and the quantitative index of segregation delamination of cemented waste rock backfill with rubber (CWRB-R) was constructed. The mechanical properties and failure characteristics of CWRB-R were studied by acoustic emission (AE) test under uniaxial compression condition. The experimental results showed that the segregation delamination characteristics of CWRB-R were related to the mass concentration. The higher the mass concentration, the weaker the degree of segregation stratification of the aggregate, the more uniform the distribution of the aggregate, and the less the strength loss of CWRB caused by the incorporation of RA. The incorporation of RA in CWRB not only reduced the uniaxial compressive strength (UCS) of the backfill, but also caused more cracks to be produced during the failure process of the backfill, and the failure form changes from brittle failure to ductile failure.

THE EFFECT OF CRUMB RUBBER ON THE PROPERTIES OF MODIFIED PORTLAND CEMENT SYSTEMS

The use of rubber crumb from used tires in concrete as a partial replacement of natural aggregates is an ecologically oriented direction of their utilization. When rubber crumb was added to Portland cement, a decrease in strength was observed. Modification of rubber-containing Portland cement systems with a complex organic and mineral additive makes it possible to compensate for the loss of compressive strength and provide increased impact strength. Samples without rubber show high strength but are characterized by fragility and sudden destruction of the material. Samples containing rubber show relatively low mechanical resistance but also exhibit elastic behavior where slow fragmentation and slow failure of the material after crack initiation are observed. They also are characterized by additional load resistance after reaching the failure stress, which is associated with the bridging effect of rubber particles.

Interface Interaction of Waste Rubber–Asphalt System

Asphalt pavement construction is a large-volume project, with the ability to recycle the industrial waste and reduce carbon emissions. Rubber-modified asphalt is a carbon-neutralized asphalt-based material, facilitating the recycling of waste rubber materials and improving the road performance of the asphalt mixture. To evaluate the interface interaction of the rubber–asphalt system and its effect on the viscosity characteristics of rubber-modified asphalt, the contact properties of rubber particles in asphalt were analyzed on a microscopic level. Rubber swelling tests and solvent elution tests were conducted on the rubber–asphalt system under different preparation conditions. The swelling ratio, degradation ratio, and swelling–degradation ratio were proposed to evaluate the interface interaction. The results show that the interface interaction of the rubber–asphalt system can be divided into the following three stages: swelling, effective degradation, and over-degradation. The degree of swelling is mainly affected by the content and size of the rubber particles and it is physically condensed, while the degradation is mainly affected by the preparation temperature and preparation time. The effective interface interaction greatly affects the viscosity with the building of the stable three-dimensional network structure. The stronger the interface interaction, the greater the viscosity of the rubber-modified asphalt, except for the 25% content of rubber particles. The gel film will be generated on the surface of the rubber particles throughout the swelling and effective degradation, increasing the viscosity of the rubber-modified asphalt.

Numerical simulation of the deformation behavior of a composite foundation consisting of rubber particle loess-CFG under dynamic loading

The CFG pile technology is primarily employed for foundation reinforcement, offering cost-saving benefits and demonstrating significant reinforcement effects. Consequently, it has gained widespread utilization. However, due to its unique composition and exceptional strength characteristics, investigating the dynamic properties of rubber particle loess-CFG poses significant challenges. In this study, a numerical simulation approach is employed to investigate the dynamic characteristics of rubber particle loess-CFG and its deformation response under dynamic loading is analyzed. The results indicate that the deformation of rubber particle loess-CFG remains minimal under static loading, while it significantly increases under dynamic loading. However, the vertical and horizontal displacements at the top of the mattress layer are comparatively smaller than those observed in loess-CFG, highlighting their seismic stability. The mattress layer of the rubber particle loess-CFG undergoes vertical compression and deformation, while being horizontally squeezed towards the central region. The horizontal displacement and its variation range are significantly greater than that of the entire pile and the soil between piles. Therefore, it is crucial to analyze the material properties, thickness, and extent of the mattress layer during design in order to mitigate its influence. When subjected to dynamic loading at the base of the model, the rubber particle loess-CFG exhibits a strip distribution of vertical displacement which gradually decreases from bottom to top. Moreover, as focal depth increases, the impact of dynamic loading on foundation deformation diminishes. Consequently, rubber particle loess-CFG provides a dual functionality of enhancing foundation strength while effectively resisting dynamic deformations. These research findings provide a theoretical basis for designing reinforced foundations using rubber particle loess-CFG and offer an innovative approach for recycling waste tire rubber particles.

Experiment on MICP-solidified calcareous sand with different rubber particle contents and sizes

Microbially induced calcite precipitation (MICP) is a new environmentally friendly technology, with the ability to improve the mechanical properties of calcareous sand. Rubber is a high-compressibility material with a higher damping ratio than that of calcareous sand. In this study, calcareous sand was replaced by equal volume contents (0%, 1%, 3%, 5%, 7%, and 9%) and different sizes (0–1, 1–2, and 2–3 mm) of rubber, and a series of water absorption and unconfined compressive strength (UCS) tests were conducted on MICP-solidified rubber–calcareous sand (MRS). The results showed that the water absorption is reduced when the rubber content is larger. The UCS of 0–1-mm MRS decreased with the increase in rubber content. For 1–2-mm and 2–3-mm MRS, the UCS was improved by 11.30% and 15.69%, respectively, compared with the clean sand. Adding rubber promoted the formation of calcium carbonate, but the strength and stiffness of rubber particles were lower than those of the calcareous sand. Therefore, higher rubber content weakened the sand frame bearing system, and the UCS decreased when the rubber content was more than 5%. Moreover, a large amount of 0–1-mm rubber led to the increase in transverse deformation of the samples, which caused the acceleration of the destruction of the sand structure. The water absorption of 0–1-mm MRS was higher than that of 1–2-mm and 2–3-mm MRS, but the UCS of 0–1-mm MRS was lower. The best rubber size is 1–2 mm and 2–3 mm, and the best rubber content is 3%–5%. The outcome of this study may, in the authors’ view, prove beneficial in improving the strength of calcareous sand when it is reinforced by MICP-combined rubber.

Deformation and mechanical properties of foamed concrete under various components and pore structure

Based on macroscopic experimentation and microcosmic testing techniques, the effects of water-binder ratio, water reducer, fly ash and rubber particle content on the settlement, compressive and folding strength, dried shrinkage rate and microstructure of foamed concrete were investigated. The sample's porosity and average pore diameter were measured and combined with the sample's settlement, mechanical properties and dry shrinkage to analyze the difference of the microstructure and its influence on the macro properties in order to provide a basis for the control of the settlement and dry shrinkage of foamed concrete. The results demonstrated that the optimal water-to-binder ratio enhanced the ability of the froth and cementitious material to disperse, as well as the cementitious material's capacity to uniformly envelop the bubbles. It is evident that the water-reducing agent can enhance the pore structure of foamed concrete because the pore wall structure is more complete. By re-hydration of fly ash with the calcium hydroxide produced by cement hydration, internal cavities can be filled to a greater extent. Rubber powder can reduce the strength and increase the settlement deformation of foamed concrete, but it can effectively limit the concrete's dry shrinkage deformation. The settlement of the earlier slurry will alter the pore structure of the later material, and the pressure will fracture and fuse the internal pores, resulting in smaller porosity and larger mean aperture.

Experimental analyses of high-filled cut-and-cover tunnel for reduction of the earth pressure

ABSTRACT The pressure distribution over buried structures like pipes and tunnels are considered a main factor in the economic design of such structures. This study shows the effect of using crumb rubber mixed with sand and geogrid layers to enhance the soil pressure distribution over that buried structure. That method is titled a high-filled cut-and-cover (HFCCT) construction method. Crumb rubber particles pieces mixed with sand as a lightweight fill material (LFM) in HFCCT are used to reduce the vertical earth pressure (VEP) on that buried tunnel. Geogrid reinforcement layer above the HFCCT system to strengthen the soil layers above the tunnels were implemental. A physical model is built to simulate such conditions by applying external loads to the treated soil layers above the tunnel. The strains are measured on the external body of the tunnel, while the soil pressure is assessed through pressure gauges around the tunnel. The results obtained from the crumb rubber models are compared with those obtained from the geogrid model. It was deduced that using crumb rubber and geogrid, reduces the earth pressure above the cut-and-cover tunnel (CCT). As compared to the use of geogrid, the utilization of rubber as a substitute for soil results in a 27% drop in pressure. The obtained results show that the use of geogrids in sandy soils leads to uniform stress, while using rubber sand could reduce the maximum stress of the soil above the tunnel.

Effects of basalt fibre and rubber particles on the mechanical properties and impact resistance of concrete

The application of waste rubber particles and basalt fibre (BF) in concrete can not only improve the performance of the resulting concrete but also alleviate the environmental pressures related to waste tire disposal. In this study, the impacts of rubber particles and BF on the mechanical and impact performance of concrete are experimentally investigated. Additionally, the macroscopic test phenomenon is explained based on the appearance of the microstructure. The results show that for basalt fibre-reinforced concrete (BFC), when the BF content increases from 0 to 0.4 %, the cube compressive strength and elastic modulus decrease from 71.5 MPa to 62.5 MPa and 44.5 GPa to 41.0 GPa, respectively, while the bending strength increases from 5.9 MPa to 6.6 MPa and then decreases to 6.3 MPa. A BF content of 0.3 % is selected to prepare basalt fibre-reinforced rubber concrete (BFRC). As the rubber particle content of BFRC increases from 0 to 20 %, the cube compressive strength, elastic modulus and bending strength decrease from 64.3 MPa to 51.5 MPa, 41.9 GPa to 33.5 GPa and 6.6 MPa to 5.9 MPa, respectively. However, the reduction rate of the mechanical properties of BFRC is approximately half that of fibre-free rubber concrete at the same rubber content. The shapes of the stressstrain curves of the BFC and normal concrete (NC) are similar, whereas the descending stage of the stressstrain curve of the BFRC is obviously gentler, and the whole BFRC stressstrain curve is much fuller, reflecting typical ductile failure. Both the BF and rubber particles contribute to impact performance improvement, but the effect of the rubber particles is much greater than that of the BF. Compared with that of the NC, the incorporation of 0.3 % BF increases the initial crack impact energy (W1) and final crack impact energy (W2) by 71 % and 79 %, respectively, but when 20 % rubber particles are additionally added, the increase rates of W1 and W2 reach 668 % and 686 %, respectively. The impact life evolutions of BFC and BFRC can be described effectively by a two-parameter Weibull distribution function.

Effect of Titanium Dioxide on Cure Characteristics and Physico Mechanical Properties of High-Temperature Vulcanizing Silicone Rubber Composites

Silicone rubber (SiR), a vital elastomer, is extensively used in producing various engineering and general products, owing to its distinctive properties. Despite the remarkable properties, SiR-based products require anti-microbial agents such as titanium dioxide, TiO2 to negate black mold issues. Still, adding this agent alters the composites' processability and physical and mechanical properties. This study examined the impact of adding different TiO2 content as fillers on silicone rubber composites' processability, physical properties, and mechanical properties. Raw materials of 20-hardness high-temperature-vulcanization (HTV) SiR- reinforced with various TiO2 contents at 0.0, 0.3, 0.6 and 1.2 wt% were prepared using a two-roll mill. The results indicated SiR composites reinforced with 0.3 wt% TiO2 exhibited the best performance with a tensile strength of 1.49 MPa, elongation at break of 340.87%, modulus 100% of 0.664 MPa, modulus 300% of 0.822 MPa, and modulus 500% of 0.954 MPa. This performance can be attributed to the efficient crosslink density and the effective interactions between the TiO2 and silicone rubber particles at this concentration. Structural and morphological analyses further corroborated the results. Consequently, it can be inferred that silicone rubber reinforced with 0.3 wt% titanium dioxide holds the potential for formulating silicone rubber compounds that necessitate anti-microbial properties.

Tensile strength prediction of crumb rubber concrete based on mesoscale modelling

ABSTRACT This study presents an experimental study and a mesoscale model for evaluating the tensile performance of crumb rubber concrete (CRC). In the experimental study, indirect tensile strengths of CRC with 6%, 12% 18% rubber contents were tested. Then the tested CRC samples were modelled as a five-phase material containing rubber, coarse aggregate, mortar, aggregate-mortar interface layer, and rubber-mortar interface layer. Numerical results from the mesoscale model agreed well with experimental tests. Parameter analysis was carried out to investigate the content, size, shape of rubber particle, thickness of interface layer on the tensile strength of CRC. Numerical results also indicated that rubber content was the governing influencing factor on the tensile strength reduction. As comparison, the influence from rubber size and rubber shape was relatively low. For a specimen with constant rubber content and size, changes in the distribution of rubber particles resulted in slight changes in the tensile strength of CRC as well. The effect of rubber particles on the tensile properties of concrete was similar to that of pores. Finally, tensile strength prediction formula was developed based on the pores model proposed in this study.

Effect of proteins as constituents of island-nanomatrix structure on vulcanization of natural rubber

Effect of proteins, constituents of the island-nanomatrix structure, on dispersion of zinc to natural rubber was investigated by transmission electron microscopy-energy dispersive X-ray spectroscopy (TEM-EDX) and focused ion beam-scanning electron microscopy-energy dispersive X-ray spectroscopy (FIB-SEM-EDX). Films of natural rubber and deproteinized natural rubber (DPNR) prepared with urea were embedded in a mixture of ZnO, vulcanization accelerator and sulfur, and they were heated at 150 °C for 5 h. Migration of Zn from surface to inside of the films was observed by FIB-SEM-EDX. The Zn migrated from the surface to 14 μm for natural rubber, but not for DPNR. The optimum vulcanization time for natural rubber was short, i.e., about 4 min, whereas it was long for DPNR, i.e., about 15 min. To confirm the effect of the proteins, a latex-mixed rubber compound was prepared by mixing the latex with sulfur, ZnO and vulcanization accelerator followed by drying with a hotplate at 150 °C for 45 s since the proteins are segregated on the surface of natural rubber particles in the latex stage. Vulcanization was accelerated for the latex-mixed natural rubber compared with mechanically mixed natural rubber compound that was prepared by mixing natural rubber with ZnO, vulcanization accelerator and sulfur with a two-roll mill. The resulting latex-mixed natural rubber vulcanizate was superior in mechanical properties to the mechanically mixed natural rubber vulcanizate. It was found by rubber-state NMR spectroscopy that the difference in mechanical properties was attributed to the difference in the cis-1,4-average sequence length of the vulcanizates, which came from the difference in the dispersion of Zn.

Solid-liquid particle flow sealing mucus (PFSM) in enhancing coalbed methane (CBM) recovery: Multiple-perspectives analysis and mechanism insights

The paper presents an in-depth investigation of solid-liquid two-phase particle flow sealing mucus (PFSM) for enhanced coalbed methane (CBM) recovery. PFSM is composed of solid waste particles such as fly ash and rubber particles. The PFSM is assessed using multiple-perspectives analysis, which includes measurements of water retention, pressure expansion, rheological characteristics, adhesion, wettability, microscopy and field case studies. Single-factor and multi-factor studies are used to optimize slurry material ratios. The results show that PFSM has outstanding water retention characteristics, with over 80 % retention for 30 days at 30 °C, and impressive expansion performance, with 9.52 % at 0.6 MPa. The shear thinning curve conforms to the Cross model. After 30 s, the final contact angle is 75.17 °, which is about 6 ° smaller than that of cement based materials. Field experiments show that, after applying PFSM, the drainage gas concentration can be improved at least 60 % comparing to other sealing materials. This research findings could offer novel insights into enhancing CBM extraction, indicating potential for safer and more efficient coal mine production.

Study on static and dynamic mechanical properties and microstructure of silica fume-polypropylene fiber modified rubber concrete

Through tests and micro-observations, the static and dynamic mechanical properties and microstructure of rubber concrete samples modified with varying amounts of silica fume and polypropylene fiber content were explored. The results indicate that incorporation of silica fume and polypropylene fiber can effectively enhance the performance of rubber concrete. Moreover, at 10% and 0.1% of silica fume and polypropylene fiber content respectively, rubber concrete’s compressive strength, splitting tensile strength, flexural strength, and dynamic compressive strength reached maxima. Furthermore, microstructure characteristic analysis indicated that inadequate adhesion between rubber particles and the matrix is responsible for compromised bearing capacity in unmodified rubber concrete. However, with the addition of silica fume and polypropylene fiber, the fiber binds the rubber particles closely with the matrix, while the silica fume fills the gaps between the matrix components. This combination results in rubber concrete with a denser internal structure and enhances its bearing capacity significantly.