Abstract An attempt was made to use friction stir processing, a manufacturing technique usually employed for the fabrication of nanocomposites. For the substrate, AA7075 was used and for dispersed phase, B4C nanoparticles of size (<30 nm) were selected. Nanocomposite samples were fabricated using three different tool rotation speeds of 1000, 1200, and 1400 rpm, by keeping other process parameters as constant, and their influence on the nanocomposite was judged by the study of tribological behavior and microhardness. This research work aims at the self-assembled monolayer formation of B4C nanoparticles homogeneous layer into a substrate material and hence minimizing the quantity of nanoparticles required in the preparation of nanocomposites via FSP. The results in terms of increased microhardness compared to the substrate material are reflected by the sample processed at the tool rotation of 1200 rpm. The average microhardness was found out to be 195 Hv compared to the substrate material. There is a maximum increment attained in wear resistance upto 46.7% in the sample processed at 1200 rpm. Worn out surface morphology were analyzed through scanning electron microscopy, and X-ray diffraction was also undertaken to analyze the presence of reinforcement particle in the fabricated nanocomposites.
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