Resonance Frequency Shift Research Articles

Reconfigurable Split Ring Resonators by MEMS-Driven Geometrical Tuning.

A novel approach for dynamic microwave modulation is proposed in the form of reconfigurable resonant circuits. This result is obtained through the monolithic integration of double split ring resonators (DSRRs) with microelectromechanical actuators (MEMS) for geometrical tuning. Two configurations were analyzed to achieve a controlled deformation of the DSRRs' metamaterial geometry by mutual rotation or extrusion along the azimuthal direction of the two constituent rings. Then, the transfer function was numerically simulated for a reconfigurable MEMS-DSRR hybrid architecture where the DSRR is embedded onto a realistic piezo actuator chip. In this case, a 370 MHz resonance frequency shift was obtained under of a 170 µm extrusion driven by a DC voltage. These characteristics in combination with a high Q factor and dimensions compatible with standard CMOS manufacturing techniques provide a step forward for the production of devices with applications in multiband telecommunications and wireless power transfer and in the IoT field.

Thermal oscillation in the hybrid Si3N4 - TiO2 microring.

The hybrid microcavity composed of different materials shows unique thermal-optical properties such as resonance frequency shift and small thermal noise fluctuations with the temperature variation. Here, we have fabricated the hybrid Si3N4 - TiO2 microring, which decreases the effective thermo-optical coefficients (TOC) from 23.2pm/K to 11.05pm/K due to the opposite TOC of these two materials. In this hybrid microring, we experimentally study the thermal dynamic with different input powers and scanning speeds. The distorted transmission and thermal oscillation are observed, which results from the non-uniform scanning speed and the different thermal relaxation times of the Si3N4 and the TiO2. We calibrate the distorted transmission spectrum for the resonance measurement at the reverse scanning direction and explain the thermal oscillation with a thermal-optical coupled model. Finally, we analyse the thermal oscillation condition and give the diagram about the oscillation region, which has significant guidance for the occurrence and avoidance of the thermal oscillation in practical applications.

Monitoring MR-guided high intensity focused ultrasound therapy using transient supersonic shear wave MR-elastography

Objective. The aim of the paper is to propose an all-in-one method based on magnetic resonance-supersonic shear wave imaging (MR-SSI) and proton resonance frequency shift (PRFS) to monitor high intensity focused ultrasound (HIFU) thermal ablations. Approach. Mechanical properties have been shown to be related to tissue damage induced by thermal ablations. Monitoring elasticity in addition to temperature changes may help in ensuring the efficacy and the accuracy of HIFU therapies. For this purpose, an MR-SSI method has been developed where the ultrasonic transducer is used for both mechanical wave generation and thermal ablation. Transient quasi-planar shear waves are generated using the acoustic radiation force, and their propagation is monitored in motion-sensitized phase MR images. Using a single-shot gradient-echo echo-planar-imaging sequence, MR images can be acquired at a sufficiently high temporal resolution to provide an update of PRFS thermometry and MR-SSI elastography maps in real time. Main results. The proposed method was first validated on a calibrated elasticity phantom, in which both the possibility to detect inclusions with different stiffness and repeatability were demonstrated. The standard deviation between the 8 performed measurements was 2% on the background of the phantom and 11%, at most, on the inclusions. A second experiment consisted in performing a HIFU heating in a gelatin phantom. The temperature increase was estimated to be 9 °C and the shear modulus was found to decrease from 2.9 to 1.8 kPa, reflecting the gel softening around the HIFU focus, whereas it remained steady in non-heated areas. Significance. The proposed MR-SSI technique allows monitoring HIFU ablations using thermometry and elastography simultaneously, without the need for an additional external mechanical exciter such as those used in MR elastography.

Simultaneous proton resonance frequency T1 - MR shear wave elastography for MR-guided focused ultrasound multiparametric treatment monitoring.

To develop an efficient MRI pulse sequence to simultaneously measure multiple parameters that have been shown to correlate with tissue nonviability following thermal therapies. A 3D segmented EPI pulse sequence was used to simultaneously measure proton resonance frequency shift (PRFS) MR thermometry (MRT), T1 relaxation time, and shear wave velocity induced by focused ultrasound (FUS) push pulses. Experiments were performed in tissue mimicking gelatin phantoms and ex vivo bovine liver. Using a carefully designed FUS triggering scheme, a heating duty cycle of approximately 65% was achieved by interleaving FUS ablation pulses with FUS push pulses to induce shear waves in the tissue. In phantom studies, temperature increases measured with PRFS MRT and increases in T1 correlated with decreased shear wave velocity, consistent with material softening with increasing temperature. During ablation in ex vivo liver, temperature increase measured with PRFS MRT initially correlated with increasing T1 and decreasing shear wave velocity, and after tissue coagulation with decreasing T1 and increasing shear wave velocity. This is consistent with a previously described hysteresis in T1 versus PRFS curves and increased tissue stiffness with tissue coagulation. An efficient approach for simultaneous and dynamic measurements of PRSF, T1 , and shear wave velocity during treatment is presented. This approach holds promise for providing co-registered dynamic measures of multiple parameters, which correlates to tissue nonviability during and following thermal therapies, such as FUS.

Terahertz Metamaterial Biosensor With Double Resonant Frequencies for Specific Detection of Early-Stage Hepatocellular Carcinoma

A novel strategy for screening early hepatocellular carcinoma (HCC) using a terahertz (THz) metamaterials (MMs) biosensor modified with the antibody against alpha-fetoprotein (AFP) is proposed. The designed biosensor consists of split-resonant-rings (SRRs) with double resonant frequencies that are optimized using the finite integration time domain (FITD) method and manufactured by a surface micromachining process. The experimental results indicate that the HCC biomarker AFP could be accurately distinguished with a concentration as low as 0.1 ng/mL via analyzing the shifts of double resonant frequencies. Meanwhile, specific detection of AFP-antigen in solution and HCC serum has been achieved through the antigen-antibody specific binding. These results demonstrate the sensitivity and specificity of THz MMs biosensor for molecular detection of trace cancer biomarkers in biochemical sensing. Furthermore, the sensitivity of specific cancer biomarkers can be further improved by optimizing the MM structure and applying the double resonant frequencies. Therefore, this approach may own great potential for special identification of early cancer molecules.

Wearable Sensing System for NonInvasive Monitoring of Intracranial BioFluid Shifts in Aerospace Applications

The alteration of the hydrostatic pressure gradient in the human body has been associated with changes in human physiology, including abnormal blood flow, syncope, and visual impairment. The focus of this study was to evaluate changes in the resonant frequency of a wearable electromagnetic resonant skin patch sensor during simulated physiological changes observed in aerospace applications. Simulated microgravity was induced in eight healthy human participants (n = 8), and the implementation of lower body negative pressure (LBNP) countermeasures was induced in four healthy human participants (n = 4). The average shift in resonant frequency was -13.76 ± 6.49 MHz for simulated microgravity with a shift in intracranial pressure (ICP) of 9.53 ± 1.32 mmHg, and a shift of 8.80 ± 5.2097 MHz for LBNP with a shift in ICP of approximately -5.83 ± 2.76 mmHg. The constructed regression model to explain the variance in shifts in ICP using the shifts in resonant frequency (R2 = 0.97) resulted in a root mean square error of 1.24. This work demonstrates a strong correlation between sensor signal response and shifts in ICP. Furthermore, this study establishes a foundation for future work integrating wearable sensors with alert systems and countermeasure recommendations for pilots and astronauts.

Comprehensive Numerical Analysis of Temperature Sensitivity of Spherical Microresonators Based on Silica and Soft Glasses

In recent years, the use of optical methods for temperature measurements has been attracting increased attention. High-performance miniature sensors can be based on glass microspheres with whispering gallery modes (WGMs), as their resonant frequencies shift in response to the ambient parameter variations. In this work, we present a systematic comprehensive numerical analysis of temperature microsensors with a realistic design based on standard silica fibers, as well as commercially available special soft glass fibers (GeO2, tellurite, As2S3, and As2Se3). Possible experimental implementation and some practical recommendations are discussed in detail. We developed a realistic numerical model that takes into account the spectral and temperature dependence of basic glass characteristics in a wide parameter range. To the best of our knowledge, spherical temperature microsensors based on the majority of the considered glass fibers have been investigated for the first time. The highest sensitivity dλ/dT was obtained for the chalcogenide As2Se3 and As2S3 microspheres: for measurements at room temperature conditions at a wavelength of λ = 1.55 μm, it was as high as 57 pm/K and 36 pm/K, correspondingly, which is several times larger than for common silica glass (9.4 pm/K). Importantly, dλ/dT was almost independent of microresonator size, WGM polarization and structure; this is a practically crucial feature showing the robustness of the sensing devices of the proposed design.

Temperature distribution in a gas-solid fixed bed probed by rapid magnetic resonance imaging

Controlling the temperature distribution inside catalytic fixed bed reactors is crucial for yield optimization and process stability. Yet, in situ temperature measurements with spatial and temporal resolution are still challenging. In this work, we perform temperature measurements in a cylindrical fixed bed reactor by combining the capabilities of real-time magnetic resonance imaging (MRI) with the temperature-dependent proton resonance frequency (PRF) shift of water. Three-dimensional (3D) temperature maps are acquired while heating the bed from room temperature to 60 °C using hot air. The obtained results show a clear temperature gradient along the axial and radial dimensions and agree with optical temperature probe measurements with an average error of ± 1.5 °C. We believe that the MR thermometry methodology presented here opens new perspectives for the fundamental study of mass and heat transfer in gas–solid fixed beds and in the future might be extended to the study of reactive gas–solid systems.

Terahertz virus-sized gold nanogap sensor

Abstract We demonstrated an ultra-sensitive terahertz virus detection method combined with virus-sized gold nanogaps filled with Al2O3. Large-area high-density 20 nm-gap rectangular loop structures, containing a resonant frequency in the terahertz range, were fabricated on a 4-inch wafer using atomic layer lithography. When target viruses with a 60 nm diameter were located on the nanogaps, we observed a significant redshift of the resonant peak already with an average number of about 100 viruses per unit loop due to the strong field confinement and enhancement near the gap. Furthermore, when the virus was tightly attached to an etched gap like a bridge connecting metals, its sensitivity is doubled compared to the unetched gap, which resulted in 400% more resonance frequency shift per single virus particle than our previous work. Full-wave simulations and theoretical calculations based on modal expansions were in good agreement with the experiments, revealing that the resonant transmission spectrum was mostly determined by the change in refractive index in a two-dimensional-like optical hotspot near the nanogap. A further step could be taken to increase sensitivity by tuning nanogap-loops to the absorption frequencies associated with the intermolecular vibrational modes of the viruses and fingerprinting them as well.

A cost-effective smartphone-based device for rapid C-reaction protein (CRP) detection using magnetoelastic immunosensor.

C-Reaction protein (CRP) is a marker of nonspecific immunity for vital signs and wound assessment, and it can be used to diagnose infections in clinical medicine. However, measuring CRP level currently requires hospital-based instruments, high-cost reagents, and a complex process, all of which have limited its full capabilities for self-detection, a growing trend in modern medicine. In this study, we developed a novel smartphone-based device using advanced methods of magnetoelastic immunosensing to mitigate these limitations. We combined a system-on-chip (SoC) hardware architecture with smartphone apps to realize the sampling of resonance frequency shift on magnetoelastic chips, which can determine the ultra-sensitivity to mass change caused by the binding of anti-CRP antibody and CRP. Through detecting a multi-group of samples, we found that the resonance frequency shift was linearly proportional to the CRP concentration in the range from 0.1 to 100 μg mL-1, with a sensitivity of 12.90 Hz μg-1 mL-1 and a detection limit of 2.349 × 10-4 μg mL-1. Meanwhile, compared with the large-scale instrument used in clinical settings, the performance of our device was stable and significantly more portable, rapid and cost-effective, offering excellent potential for modern home-based diagnosis.

Metal crack size recognizing used circular patch antenna

Metal crack size recognition based on a circular patch antenna is presented in this article. The material under investigation is positioned onto the microstrip antenna's ground plane. Subsequently, antenna parameters such as return loss, VSWR, and resonance frequency shift are analyzed to ascertain their correlation with the length of cracks occurring within the metal. This study seeks to establish relationships between these antenna parameters and crack length, ultimately aiming to develop a crack detection methodology using the microstrip antenna. The testing results have revealed a significant correlation between the microstrip antenna parameters and the length of cracks within the metal material. Notably, the VSWR parameter of the antenna exhibits a correlation coefficient of 0.9881, while the resonance frequency shift displays a correlation coefficient of 0.9891.

Accurate Electrostatic Force Measurements by Atomic Force Microscopy Using Proper Distance Control

Electrostatic force microscopy (EFM) enables us to examine the local electrostatic force between an AFM tip and sample surface, from which an electrical capacitance between them and surface potential can be evaluated, by applying direct current (DC) and alternating current (AC) voltages. From the dependences of the electrostatic force on the DC voltage and on the frequency of AC voltage in EFM, carrier density, carrier type, and deep level states in a semiconductor can also be investigated. Since EFM is basically operated as an atomic force microscopy (AFM), special care should be taken in an effect of the electrostatic force on a distance control between the tip and sample, and robust distance control is necessary even under the strong electrostatic force in order to realize proper measurements of both topography and electrostatic force. In this paper, we have examined the effectiveness of the usage of the oscillation amplitude of a cantilever as a feedback target for the distance control, which is referred to as Δ <italic xmlns:mml="http://www.w3.org/1998/Math/MathML" xmlns:xlink="http://www.w3.org/1999/xlink">A</i> -mode operation, while the cantilever oscillation frequency is always kept at its primary resonance, like the conventional frequency modulation AFM (FM-AFM) which uses a resonant frequency shift as the feedback target. First, we have verified that a distance change due to the strong electrostatic force was significantly reduced compared with FM-AFM. Secondly, we have confirmed that the Δ <italic xmlns:mml="http://www.w3.org/1998/Math/MathML" xmlns:xlink="http://www.w3.org/1999/xlink">A</i> -mode operation in EFM realized proper measurements of the dependance of a tip-sample capacitance including a surface depletion capacitance on the DC voltage and on the frequency of AC voltage, indicating good robustness of the method against the strong electrostatic force.

Optical fiber-based magnetically-tuned graphene mechanical resonator

In this study, an optical fiber-based magnetically-tuned graphene mechanical resonator (GMR) is demonstrated by integrating superparamagnetic iron oxide nanoparticles on the graphene membrane. The resonance frequency shift is achieved by tuning the tension of the graphene membrane with a magnetic field. A resonance frequency tunability of 23 kHz using a 100 mT magnetic field is achieved. The device provides a new way to tune a GMR with a non-contact force. It could also be used for weak magnetic field detection in the future with further improvements in sensitivity.

Simultaneous Detection of Pressure and Bending Using a Microwave Sensor With Tag and Reader Structure

Wearable technology and soft robotics have experienced significant growth in the past decade. In these applications, flexible and highly sensitive pressure and bending sensors are essential for providing feedback to control and operate devices. Despite the development of many pressure and bending sensors, the challenge remains to develop one single sensor with high sensitivity that can simultaneously measure pressure and bending, which allows for a more compact system and simplified control. In addition, wireless sensing is desirable so that the sensor and the readout system can be placed separately at convenient locations. This paper presents a new wireless microwave sensor to meet the needs. The sensor uses a resonator-based design, where pressure and bending changes are reflected as resonance frequency shifts and amplitude changes in the transmission response spectrum, respectively. This “one for two” approach allows for selective sensing and easy fabrication of the sensor, with results displayed on a cost-effective handheld device. The sensor and the reader are electromagnetically coupled without the need for physical contact offering wireless sensing. With a sensitivity of 3.39 MHz kPa1, this wireless sensor design offers a promising solution for wearable devices and soft robots due to its flexibility, small size, and low fabrication cost.

Fully Printed Dual-Layer Depolarizing Chipless RFID Tag for Wearable Applications

This work presents a cross-polar dual-layer chipless radio-frequency identification (RFID) tag based on a ladder-shaped resonator design. An integrated ground plane enables direct attachment to human skin without performance deterioration. Simulations show that the ladder-shaped resonator provides several advantages over traditional L-shaped and straight resonators, including a strong cross-polar radar cross section (-23.4 dBsm), third-order harmonics, orientation insensitivity, and compact size (0.062 λ2). The effects of the ground plane shape on the surface current distribution are investigated, and a circular tag of 20 mm radius is designed using ladder resonator groups and frequency shift encoding to provide an active area of 96.45 bits/λ2 and a unit frequency of 6.03 bits/GHz. The tag substrate is three-dimensionally (3D) printed with metallic resonator patterns that are subsequently screen-printed on the substrate. The maximum read range is measured at 40 mm using a cross-shaped, dual-polarized Vivaldi antenna connected to a network analyzer. The measured characteristics in free space are in good agreement with the simulation results, and practical on-body performance tests for the manufactured prototype using simulation and direct measurements indicate that the tag performance remains stable for both free space and on-body cases. The fully printed fabrication process makes the proposed tag design suitable for mass production at a low cost.

Inclination Sensor With a Wide Angle Measurement Range Using Half-Wavelength Microstrip Resonator

In this article, a new inclinometer concept based on an angular half-wavelength microstrip resonator is presented. The inclinometer has a wide dynamic range of 84° (±42°) which can be extended to 180° through a simple modification. The inclinometer is composed of a microstrip transmission line resonator on printed circuit board and a second transmission line on an overlapping circuit board that rotates according to the inclination angle. As the inclination angle changes, the overall length of the resonator varies and leads to resonance frequency shift, which is transformed into inclination variation. The sensor measurements results determined the sensitivity of the sensor as 0.384 mm/° and the resolution as 0.035°. The proposed sensor is also quite simple, cost-effective, compact, and robust.

Investigating Hydrodynamic Loading Effects on Resonant Frequency Shift of Quartz Crystal Resonator with Attached Particles

Investigating Hydrodynamic Loading Effects on Resonant Frequency Shift of Quartz Crystal Resonator with Attached Particles

Fiber-tip Fabry-Pérot interferometer with a graphene-Au-Pd cantilever for trace hydrogen sensing.

The widespread utilization of hydrogen energy has increased the demand for trace hydrogen detection. In this work, we propose a fiber-optic hydrogen sensor based on a Fabry-Pérot Interferometer (FPI) consisting of a fiber-tip graphene-Au-Pd submicron film cantilever. The palladium (Pd) film on the cantilever surface is used as hydrogen-sensitive material to obtain high sensing sensitivity. Hydrogen sensing is realized by monitoring the resonant frequency shift of the FPI introduced by the interaction between Pd film and hydrogen molecules. The hydrogen sensor is proven for low-hydrogen-concentration detection with hydrogen concentrations in the range of 0-1000 ppm, and experimentally characterized by a highest sensitivity of 30.3 pm ppm-1 in a low hydrogen concentration of 0-100 ppm, which is more than two orders higher than for previously reported FPI-based sensors. In real-time hydrogen monitoring, a rapid reaction time of 31.5 s was achieved. This work provides a compact all-optical solution for the safe detection of low hydrogen concentrations, which is an interesting alternative for trace hydrogen detection in the aerospace industry, energy production, and medical applications.

Anderson-Higgs Mass of Magnons in Superconductor-Ferromagnet-Superconductor Systems

The dynamic interplay of superconductivity and magnetism is promising for developing quantum magnonics and spintronics. Recent experiments have reported significant, enigmatic shifts of ferromagnetic resonance frequency in layered SFS structures. The author explains that the origin of this effect is spontaneous generation of magnon mass due to the celebrated Anderson-Higgs mechanism, a cornerstone of the Standard Model of particle physics. Upon cooling below the superconducting critical temperature, the magnons acquire a frequency gap and change their propagation direction. This effect enables the creation of magnon resonators, crystals, parametric amplifiers, and other useful devices.

Microelectromechanical system‐based biosensor for label‐free detection of human cytomegalovirus

The human cytomegalovirus (HCMV) is an asymptomatic common virus that is typically harmless, but in some cases, it can be life threatening. Thus, there is an urgent need to develop novel diagnostic methods and strengthen the efforts to combat this virus. A microcantilever-based biosensor functionalised with the UL83-antibody of HCMV (UL83-HCMV antibody) has been developed to detect the UL83-antigen of HCMV (UL83-HCMV antigen) at different concentrations ranging from 0.3 to 300ng/ml. The response of the biosensor to the presence of UL83-HCMV antigen was measured through the shift in resonance frequency before and after antigen-antibody binding. The system shows a low detection limit of 84pg/ml, which is comparable to traditional sensors, and a detection time of less than 15min was achieved. The selectivity of the sensor was demonstrated using three different proteins with and without the UL83-HCMV antigen. The biosensor shows high selectivity for the UL83-HCMV antigen. Mass loading by the UL83-HCMV antigen was roughly estimated with a sensitivity of ∼30fg/Hz. This technique is crucial for the fabrication of portable and low-cost biosensors that can be used in real-time monitoring and enables early medical diagnosis.