Resonance Frequency Shift Research Articles

Contact-Free, Passive, Electromagnetic Resonant Sensors for Enclosed Biomedical Applications: A Perspective on Opportunities and Challenges.

Inexpensive and accurate tools for monitoring conditions in enclosed environments (through garments, bandages, tissue, etc.) have been a long-standing goal of medicine. Passive resonant sensors are a promising solution for such wearable health sensors as well as off-body diagnostics. They are simple circuits with inherent inductance and capacitance (LC tank) that have a measurable resonant frequency. Changes in local parameters, e.g., permittivity or geometry, effect inductance and capacitance which cause a resonant frequency shift response. This signal transduction has been applied to several biomedical applications such as intracranial pressure, hemodynamics, epidermal hydration, etc. Despite these many promising applications presented in the literature, resonant sensors still do not see widespread adoption in biomedical applications, especially as wearable or embedded sensing devices. This perspective highlights some of the current challenges facing LC resonant sensors in biomedical applications, such as positional sensitivity, and potential strategies that have been developed to overcome them. An outlook on adoption in medicine and health monitoring is presented, and a perspective is given on next steps for research in this field.

A Tuned Microwave Resonant System for Subcutaneous Imaging

A compact and planar imaging system was developed using a flexible polymer substrate that can distinguish subcutaneous tissue abnormalities, such as breast tumors, based on electromagnetic-wave interactions in materials where permittivity variations affect wave reflection. The sensing element is a tuned loop resonator operating in the industrial, scientific, and medical (ISM) band at 2.423 GHz, providing a localized high-intensity electric field that penetrates into tissues with sufficient spatial and spectral resolutions. The resonant frequency shifts and magnitudes of the reflection coefficients indicate the boundaries of abnormal tissues under the skin due to their high contrasts to normal tissues. The sensor was tuned to the desired resonant frequency with a reflection coefficient of -68.8 dB for a radius of 5.7 mm, with a tuning pad. Quality factors of 173.1 and 34.4 were achieved in simulations and measurements in phantoms. An image-processing method was introduced to fuse raster-scanned 9 × 9 images of resonant frequencies and reflection coefficients for image-contrast enhancement. The results showed a clear indication of the tumor's location at a depth of 15 mm and the capability to identify two tumors both at the depth of 10 mm. The sensing element can be expanded to a four-element phased array for deeper field penetration. Field analysis showed the depths of -20 dB attenuation were improved from 19 to 42 mm, giving wider coverage in tissues at resonance. Results showed that a quality factor of 152.5 was achieved and a tumor could be identified at a depth of up to 50 mm. In this work, simulations and measurements were conducted to validate the concept, showing great potential for subcutaneous imaging in medical applications in a noninvasive, efficient, and lower-cost way.

Study of Force-Frequency Characteristics in AT-Cut Strip Quartz Crystal Resonators with Different Rotation Angles.

This paper investigated the force-frequency characteristics of AT-cut strip quartz crystal resonator (QCR) employing finite element analysis methods and experiments. We used the finite element analysis software COMSOL Multiphysics to calculate the stress distribution and particle displacement of the QCR. Moreover, we analyzed the impact of these opposing forces on the frequency shift and strains of the QCR. Meanwhile, the resonant frequency shifts, conductance, and quality factor (Q value) of three AT-cut strip QCRs with rotation angles of 30°, 40°, and 50° under different force-applying positions were tested experimentally. The results showed that the frequency shifts of the QCRs were proportional to the magnitude of the force. The highest force sensitivity was QCR with a rotation angle of 30°, followed by 40°, and 50° was the lowest. And the distance of the force-applying position from the X-axis also affected the frequency shift, conductance, and Q value of the QCR. The results of this paper are instructive for understanding the force-frequency characteristics of strip QCRs with different rotation angles.

Study of Helical Antenna Endowing Short Wire Length and Compact Structure for High-Frequency Operations and Its Exclusive Manufacturing Process

In this paper a study of a helical antenna resonating at high-frequency (HF) band with a very compact structure is reported. The designed antenna's S11 parameter magnitude change with frequency was calculated for different geometrical parameters. For each case, first, only a single parameter was changed. Then for a fair comparison, multiple parameters were changed simultaneously while the total wire length was set to be constant. Also, shifts in resonance frequencies and variations in -10 dB bandwidths were investigated. Our results show that resonance behaviour changes distinctively with the geometrical parameters and it allows shortening of the antenna wire length. For the designed antenna, the resonances shift to lower frequencies and -10 dB bandwidths around the resonances decrease as the winding wire thickness, number of turns, and turn radius increase. Whereas as the turn spacing increases the resonances shift to higher frequencies and -10 dB bandwidths widen, although the total wire length of the antenna increases. To verify the simulation results, the designed antenna was fabricated with an exclusive manufacturing process and characterized. The measurement results are in good agreement with the simulation results. It demonstrates the feasibility of the proposed manufacturing technique, which is new in the literature and enables accurate and rigid antenna fabrication with simple and low-cost steps.

All Acoustical Excitation of Spin Waves in High Overtone Bulk Acoustic Resonator

The hybrid high overtone bulk acoustic wave resonators (HBARs) consisting of a piezoelectric film transducers and gallium gadolinium garnet substrates with yttrium iron garnet films (YIG-GGG-YIG) are used for experimental excitation and detection of acoustically driven spin waves (ADSWs). Two types of HBAR transducers made of Al-ZnO-Al films (differed through the electrodes’ geometry) were deposited onto YIG-GGG-YIG trilayers with different YIG film thicknesses and doping levels and served for excitation of multimode HBAR at gigahertz frequencies. ADSWs were detected by measuring the shifts of resonant HBAR modes in a tangential external magnetic field when the conditions for magnetoelastic resonance (MER) were satisfied. It was shown that the design of the transducer with a continuous bottom electrode provides all acoustical excitation of spin waves (pure ADSWs), suppressing the additional inductive magnetic dynamics excitation due to the electrodes’ geometry. The theoretical study of the HBAR spectrum in a magnetic field showed that the resonance harmonics in the MER region can either almost continuously transfer from one to another, or decay and form an evident magnetoelastic gap. In this case, the shift of resonant frequencies can achieve several intermodal distances. The results obtained are important for applications of HBAR-based devices in spintronics and magnonics.

Modeling frequency shifts of collective bubble resonances with the boundary element method.

Increasing the number of closely packed air bubbles immersed in water changes the frequency of the Minnaert resonance. The collective interactions between bubbles in a small ensemble are primarily in the same phase, causing them to radiate a spherically symmetric field that peaks at a frequency lower than the Minnaert resonance for a single bubble. In contrast, large periodic arrays include bubbles that are further apart than half of the wavelength such that collective resonances have bubbles oscillating in opposite phases, ultimately creating a fundamental resonance at a frequency higher than the single-bubble Minnaert resonance. This work investigates the transition in resonance behavior using a modal analysis of a mass-spring system and a boundary element method. The computational complexity of the full-wave solver is significantly reduced to a linear dependence on the number of bubbles in a rectangular array. The simulated acoustic fields confirm the initial downshift in resonance frequency and the strong influence of collective resonances when the array has hundreds of bubbles covering more than half of the wavelength. These results are essential in understanding the low-frequency resonance characteristics of bubble ensembles, which have important applications in diverse fields such as underwater acoustics, quantum physics, and metamaterial design.

Printed Wireless Battery-Free Sensor Tag for Health Monitoring of Polymer Composites

This paper presents a fully printed wireless sensor tag for structural health monitoring of smart lightweight construction parts. The sensor concept aims for sustainability and was developed in line with the European Green Deal, fabricated by inkjet printing on uncoated paper substrate, working without the use of a battery or a chip. Measurement results show a wireless operation over a distance of 3mm, a sensitivity of 4.16 kHz resonant frequency shift per % relative humidity for the humidity sensor, 165 kHz per 1 % strain for the strain sensor and a temperature coefficient of resistance of 1.61*10 <sup xmlns:mml="http://www.w3.org/1998/Math/MathML" xmlns:xlink="http://www.w3.org/1999/xlink">-3</sup> K <sup xmlns:mml="http://www.w3.org/1998/Math/MathML" xmlns:xlink="http://www.w3.org/1999/xlink">-1</sup> for the temperature sensor. In case of all three sensors, the measurement data shows a linear response and is in good agreement with literature and reference data.

Testing universality of Feynman-Tan relation in interacting Bose gases using high-order Bragg spectra

The Feynman-Tan relation, obtained by combining the Feynman energy relation with the Tan’s two-body contact, can explain the excitation spectra of strongly interacting 39K Bose-Einstein condensate (BEC). Since the shift of excitation resonance in the Feynman-Tan relation is inversely proportional to atomic mass, the test of whether this relation is universal for other atomic systems is significant for describing the effect of interaction in strongly correlated Bose gases. Here we measure the high-momentum excitation spectra of 133Cs BEC with widely tunable interactions by using the second- and third-order Bragg spectra. We observe the backbending of frequency shift of excitation resonance with increasing interaction, and even the shift changes its sign under the strong interactions in the high-order Bragg spectra. Our finding shows good agreement with the prediction based on the Feynman-Tan relation. Our results provide significant insights for understanding the profound properties of strongly interacting Bose gases.

Decoupling free chloride and water ingress in concrete by a dielectric resonant sensor

The origin of rebars corrosion in concrete infrastructures is frequently associated with the ingress of chloride ions present in water. This is particularly the case of infrastructures located in marine environments or exposed to deicing salts. The present study aims at developing a radio-frequency dielectric sensor dedicated to free chloride ingress monitoring in a well-defined volume of the material. A resonant method operating in a wide frequency range is selected to separate the effects associated with the variation of the real part of the dielectric permittivity and tangent loss. As it will be shown, the method provides useful information on the presence of free chloride in concrete and can be used for the monitoring of chloride diffusion. For this purpose, considering the variation of the transmission parameter S12 value presents clearly some advantages with respect to the frequency shifts of resonances. This allows to decouple water and chloride content.

Measurement of Complex Permittivity for Rapid Detection of Liquid Concentration Using a Reusable Octagon-Shaped Resonator Sensor

Substrate-integrated waveguides (SIWs) are widely used in microwave systems owing to their low cost and ease of integration. In this study, an SIW-based resonator that reacts to the complex permittivity variation of solutions with dimensions of 79.2 mm × 59.8 mm is introduced. This octagon-shaped sensor can be installed on a preliminary monitoring system to test water quality by observing the parameter variations caused by external factors. The resonant structure was used to test different concentrations of ethanol-water and acetone-water mixtures for verification. The resonant frequency and quality factor (Q-factor) were found to vary with the relative complex permittivity of the liquid in the S-band, and the electric field distribution varied when liquid droplets were placed in the center of the substrate. The designed sensor operates at 2.45 GHz in the air, and the observed minimum resonant frequency shift with liquid was 15 MHz. The measurement error was approximately 3.1%, and the results reveal a relationship between the resonant frequency and temperature as well. Considering the observed sources of error, the measured relative permittivity is consistent with the actual values. The proposed sensor is economically convenient and suitable for various test environments.

A novel wireless oxygen gas sensor based on silver film loaded on a patch antenna

In this work, a patch antenna loaded with sensitive silver film was employed for the detection of oxygen gas at high concentrations. SEM micrographs demonstrate that the morphology of the Ag film presents an elevated degree of porosity, confirming that the film is suitable for adsorbing O2 gas molecules on its surface. Numerical simulation performed was validated, and the values of the far-field parameters showed that the investigated device works efficiently as an antenna. During the tests carried out, it was observed that the device responds sensitively to the presence of oxygen gas demonstrating shifts of the antenna resonant frequency to higher values as a function of the O2 concentration. The antenna sensitivity was calculated, presenting a value of 0.14 MHz/O2% for the frequency at 5.968 GHz, 0.23 MHz/O2% for frequency at 8.246 GHz, and 0.15 MHz/O2% for the frequency at 10.039 GHz. Results obtained indicate that the patch antenna tested could be used as a sensor of oxygen gas in environments with elevated concentrations of this gas, such as oxygen concentrators and other medical equipment. Because the device analyzed is an antenna, it would be possible transmitting the sensing information to another device which would make it a potential candidate for application in healthcare monitoring.

Self-organized limit cycles in red-detuned atom-cavity systems

Recent experimental advances in the field of cold-atom cavity QED provide a powerful tool for exploring nonequilibrium correlated quantum phenomena beyond conventional condensed-matter scenarios. We present the dynamical phase diagram of a driven Bose-Einstein condensate coupled with the light field of a cavity, with a transverse driving field red-detuned from atomic resonance. We identify regions in parameter space showing dynamical instabilities in the form of limit cycles, which evolve into chaotic behavior in the strong driving limit. Such limit cycles originate from the interplay between cavity dissipation and atom-induced resonance frequency shift, which modifies the phase of cavity mode and gives excessive negative feedback on the atomic density modulation, leading to instabilities of the superradiant scattering. We find interesting merging of the limit cycles related by a ${Z}_{2}$ symmetry, and identify a limit cycle formed by purely atomic excitations. The effects of quantum fluctuations and atomic interactions are also investigated.

Improving Specific Absorption Rate Efficiency and Coil Robustness of Self-Decoupled Transmit/Receive Coils by Elevating Feed and Mode Conductors.

Self-decoupling technology was recently proposed for radio frequency (RF) coil array designs. Here, we propose a novel geometry to reduce the peak local specific absorption rate (SAR) and improve the robustness of the self-decoupled coil. We first demonstrate that B1 is determined by the arm conductors, while the maximum E-field and local SAR are determined by the feed conductor in a self-decoupled coil. Then, we investigate how the B1, E-field, local SAR, SAR efficiency, and coil robustness change with respect to different lift-off distances for feed and mode conductors. Next, the simulation of self-decoupled coils with optimal lift-off distances on a realistic human body is performed. Finally, self-decoupled coils with optimal lift-off distances are fabricated and tested on the workbench and MRI experiments. The peak 10 g-averaged SAR of the self-decoupled coil on the human body can be reduced by 34% by elevating the feed conductor. Less coil mismatching and less resonant frequency shift with respect to loadings were observed by elevating the mode conductor. Both the simulation and experimental results show that the coils with elevated conductors can preserve the high interelement isolation, B1+ efficiency, and SNR of the original self-decoupled coils.

Mechano/acousto-electric coupling between ReS2 and surface acoustic wave

Two-dimensional (2D) materials are promising candidates for developing next generation electronic/optoelectronic devices with programmable multi functions, due to their widely tunable properties by various physical stimuli. Mechanical strain is one of the most promising means to effectively modulate the physical properties of 2D materials. Nevertheless, few studies reported micro/nano scale controllable strain application platforms, limiting the development of novel mechano-electrical/optoelectrical devices based on 2D materials. This work proposes surface acoustic wave (SAW) device as a controllable strain modulation platform for 2D materials with sub-micro scale resolution. The platform uses the piezoelectric material (LiNbO3) as the substrate, which is deposited with interdigitated transducers (IDT) to generate SAW on the surface. The propagation of SAW causes surface deformation, which is then transferred to the 2D materials on the substrate. The period of the surface deformation/strain is related with that of SAW, which is determined by the period of IDT with nano meter scale. It is demonstrated that the photo luminescence spectrum of a 2D ReS2 flake on this platform gradually shifts with the SAW excitation power, which reaches a shift of 3 nm as the SAW excitation power achieves 26 dBm, corresponding to a band gap increase of 5 meV. Meanwhile, the platform is also capable to provide acousto-electric coupling between SAW and 2D materials, which is demonstrated by the shift of the SAW resonant frequency due to the re-distribution of photo-generated carriers in ReS2 upon light illumination.

Evaluation of a Developed MRI-Guided Focused Ultrasound System in 7 T Small Animal MRI and Proof-of-Concept in a Prostate Cancer Xenograft Model to Improve Radiation Therapy.

Focused ultrasound (FUS) can be used to physiologically change or destroy tissue in a non-invasive way. A few commercial systems have clinical approval for the thermal ablation of solid tumors for the treatment of neurological diseases and palliative pain management of bone metastases. However, the thermal effects of FUS are known to lead to various biological effects, such as inhibition of repair of DNA damage, reduction in tumor hypoxia, and induction of apoptosis. Here, we studied radiosensitization as a combination therapy of FUS and RT in a xenograft mouse model using newly developed MRI-compatible FUS equipment. Xenograft tumor-bearing mice were produced by subcutaneous injection of the human prostate cancer cell line PC-3. Animals were treated with FUS in 7 T MRI at 4.8 W/cm2 to reach ~45 °C and held for 30 min. The temperature was controlled via fiber optics and proton resonance frequency shift (PRF) MR thermometry in parallel. In the combination group, animals were treated with FUS followed by X-ray at a single dose of 10 Gy. The effects of FUS and RT were assessed via hematoxylin-eosin (H&E) staining. Tumor proliferation was detected by the immunohistochemistry of Ki67 and apoptosis was measured by a TUNEL assay. At 40 days follow-up, the impact of RT on cancer cells was significantly improved by FUS as demonstrated by a reduction in cell nucleoli from 189 to 237 compared to RT alone. Inhibition of tumor growth by 4.6 times was observed in vivo in the FUS + RT group (85.3%) in contrast to the tumor volume of 393% in the untreated control. Our results demonstrated the feasibility of combined MRI-guided FUS and RT for the treatment of prostate cancer in a xenograft mouse model and may provide a chance for less invasive cancer therapy through radiosensitization.

Battery-Free, Artificial Neural Network-Assisted Microwave Resonator Array for Ice Detection

Ice detection has developed into an integral part of aerospace and wind turbine sectors with the aim of preventing hazards and component breakdown. This article presents an ice detection system consisting of a battery-free, chip-less wirelessly interrogated resonator array, and an artificial neural network for enhanced detection robustness. The designed array of split-ring resonators (SRRs), operating at 3.05 GHz, was a narrowband frequency-selective structure with a ground plane reflector which shielded resonance from the effect of installation material. For an incident wave on the array’s surface, the reflection coefficient changed with the electrical properties of the ice and water, consequently affecting the <inline-formula xmlns:mml="http://www.w3.org/1998/Math/MathML" xmlns:xlink="http://www.w3.org/1999/xlink"> <tex-math notation="LaTeX">$S_{11}$ </tex-math></inline-formula> parameter of an interrogator antenna. The array had a surface area of <inline-formula xmlns:mml="http://www.w3.org/1998/Math/MathML" xmlns:xlink="http://www.w3.org/1999/xlink"> <tex-math notation="LaTeX">$13\times6.5$ </tex-math></inline-formula> cm2 and a substrate thickness of 0.79 mm and was wirelessly interrogated from a distance of 33 cm by a standard gain horn antenna. A custom LabView program was utilized for time-based data acquisition of the antenna’s reflection coefficient [ <inline-formula xmlns:mml="http://www.w3.org/1998/Math/MathML" xmlns:xlink="http://www.w3.org/1999/xlink"> <tex-math notation="LaTeX">$S_{11}$ </tex-math></inline-formula> (dB)], with results demonstrating a resonant frequency shift of 150 MHz when 30 <inline-formula xmlns:mml="http://www.w3.org/1998/Math/MathML" xmlns:xlink="http://www.w3.org/1999/xlink"> <tex-math notation="LaTeX">$\mu \text{L}$ </tex-math></inline-formula> ( <inline-formula xmlns:mml="http://www.w3.org/1998/Math/MathML" xmlns:xlink="http://www.w3.org/1999/xlink"> <tex-math notation="LaTeX">$\sim$ </tex-math></inline-formula> ) of ice was formed on the main split of SRRs. The artificial neural network then classified the reflection coefficients of the interrogator antenna to enhance ice/water differentiation. The neural network improved the classification of the <inline-formula xmlns:mml="http://www.w3.org/1998/Math/MathML" xmlns:xlink="http://www.w3.org/1999/xlink"> <tex-math notation="LaTeX">$S_{11}$ </tex-math></inline-formula> (dB) raw data to 94.67% while achieving an accuracy of 93.33% for a noisy simulated data set. The proposed battery-free artificial neural network-assisted ice sensor can be implemented in various sizes (depending on the footprint requirements of installation) with applications in aerospace and wind turbine industry.

Magnetic Resonance Frequency Shifts of Alkali Atoms in a K–Li Mixture

Magnetic Resonance Frequency Shifts of Alkali Atoms in a K–Li Mixture

Room Temperature 2-Fold Morphology Porous Silicon Impedance Matching Pesticide Sensor

In this work, an investigation was conducted to study the effect of electrodes’ configuration of the double morphology macPSi on the performance of electrically matched impedance pesticides sensors. The purpose was to develop an efficient electrical sensor for the quantitative detection process of (Chlorpyrifos) pesticide in organic solvents. The effect of electrodes configuration of the front, front-back, and back coplanar electrodes on macPSi as based substrate was tested to select an optimum sensor metallization pathway. The based efficient macPSi layer was fabricated using elevated laser irradiation power density at different periods. Morphological, optical, and electrical properties of the sensors were investigated using field emission scanning electron microscope (FE-SEM), X-ray diffraction (XRD), photoluminescence (PL) spectroscopy, and R-L-C measurement. The sensing method depended on measuring the resonance frequency shift as the organic solvent was exposed to the sensor’s surface. The sensor’s performance at various configurations and concentrations ppm was inspected at room temperature. The current findings revealed extremely low instabilities (less than 0.017 %), higher sensitivity, and a detection limit of 0.004ppm for top coplanar electrode configuration. The fabricated sensor is simple and low-cost for excellent quantitative pesticide detection.

Analysis on electric impedance-controlled active ultrasonic horn in radial vibration

As a key component of high-powered ultrasonic vibration systems, ultrasonic horns play an important role in various practical application scenarios. Recent advances in longitudinal ultrasonic horns have enabled them to magnify the Langevin transducer's mechanical vibration and efficiently transmit the mechanical vibration to the mechanical load. However, limited research has been devoted to active radial ultrasonic horns in radial vibration. Here we propose an electric impedance-controlled active radial ultrasonic horn (ARUH) capable of tuning both resonance frequency and displacement magnification in radial vibration. The resulting device consists of a radially polarized piezoelectric ring connected with adjustable electric impedance and two metal rings with variable sections. The underlying mechanism is that the change of the converted mechanical impedance of the piezoelectric material by the external electric impedance connected to the piezoelectric material modulates the resonance frequency and displacement magnification of the ARUH. It can be found that the resonant frequency shifts to higher frequencies as the resistance increases and the resonant frequency shifts to lower frequencies as the inductance and capacitance increase, while the displacement magnification has the opposite trend to the resonance frequency. For example, the resonance frequency of the constant-section radial horn is 41130.2 Hz. When the inductance increases from −0.007 to 0.007H, the resonance frequency shifts from 41171.3 to 34606.2 Hz and the displacement magnification moves from 1.189 to 3.5. The experiments are conducted to verify the effectiveness of the resulting device, which is in good agreement with the simulated results and theoretical predictions. Our design with functionality and flexibility opens up possibilities for the design of ARUHs and may find important application prospects in diverse fields such as cold-drawn steel tubes and ultrasonic plastic welding.

Vibroacoustic Characteristics of a Specific Patterned Polymer with Graphene for an Electrostatic Speaker.

Graphene/polymer actuators were developed using bilayer graphene and various polymer substrates for use as transparent, flexible, and robust electrostatic speaker units. Additionally, a resonant frequency shift was induced using a polymer substrate on which various micropatterns were transferred to boost bass. The total sound pressure level (SPL) in the graphene/polymer actuator was measured by a sweep, and the frequency of the spectrum was confirmed to be one-third that of the octave band frequency. The change in the vibroacoustic characteristic with changes in Young's modulus and density was studied for the polymers of the same size and thickness. Particularly, the possibility of boosting bass was confirmed by inducing a resonant frequency shift and increasing the total SPL by adding micropatterns on a polymer substrate under the same conditions. The resonance frequency of 523 Hz and the SPL of 54 dBA in flat polymer film became 296 Hz and 69 dBA in a specific pattern, which produced a sound of >15 dB based on the same flat polymer. We expect that the design and information provided herein can provide the key parameters required to change the resonant frequency in small-size devices for the application of graphene/polymer thin-film actuators.