The Giribaile archaeological site is one of the most important Iberian enclaves of the Alto Guadalquivir (Southern Spain). However, to date, only minimal excavation work has been performed at the site. Evaluation requires a preliminary, non-destructive general analysis to determine high-interest areas. This stage required a geophysical survey. Specifically, a 100m2 grid was selected, where an initial campaign of nine electrical resistivity imaging (ERI) profiles was performed, where each profile was 111m in length; these profiles were previously located using a detailed topographical survey. A total of 112 electrodes were used for each profile, spaced at 1m apart with a Wenner-Schlumberger configuration. Secondly, 201 GPR profiles were created using a 500MHz antenna. The 100m long profiles were spaced 0.5m apart and parallel to one another.The present research analyses the efficiency of each of these geophysical tools in supporting archaeological research. Using these methodologies, the position, morphology, and depth of different buried structures can be determined. 3D interpretation of the geophysical survey in 100×100m grid allowed to differentiate structures square and rectangular, interesting buildings in a semicircle (interpreted as ovens) plus delineate different streets. From the geophysical survey follows the Carthaginian presence inside this ancient Iberian enclave.