Remanence Carriers Research Articles

High‐Latitude Paleointensities During the Cretaceous Normal Superchron From the Okhotsk–Chukotka Volcanic Belt

AbstractWe conducted an absolute paleointensity survey on 74 lava flows from the Okhotsk–Chukotka Volcanic Belt (NE Russia), emplaced 90–83 Ma toward the end of the Cretaceous Normal Superchron (CNS, 121–84 Ma). Relying on preliminary results, we restricted our analysis to eight lava flows (140 Thellier–Coe experiments), two of which also yielded successful Wilson determinations. A detailed analysis of the magneto‐mineralogy—based on X‐ray structural analysis, reflected‐light microscopy, and thermomagnetic curves—indicates that the determinations from solely two lava flows can be fully trusted, with remanence carriers (a) dominated by low‐titanium titanomagnetite, (b) showing unambiguous traces of high‐temperature oxidation, and (c) yielding partial thermoremanent magnetization (pTRM) tails representative of pseudo‐single‐domain grains. Recalculated in terms of geomagnetic dipole strength, our two successful flow‐mean determinations yield virtual dipole moments of 4.76 ± 0.26 × 1022 Am2 (N = 7) and 9.07 ± 0.84 × 1022 Am2 (N = 8). Using an updated version of the paleointensity database for the Cretaceous epoch, we stress that determinations based on nonglassy whole rocks, submarine basaltic glasses, and single crystals are mutually inconsistent, suggesting a separate analysis of their distributions is more appropriate. Despite statistically indistinguishable estimates of dipole strength before and after the onset of the CNS—in accord with recent studies refuting the existence of a strict correlation between chron duration and dipole moment—we found that the distribution of dipole moments during the CNS is slightly bimodal with a leptokurtic dominant mode, thus more inclined to produce outliers and suggesting distinct geomagnetic field behavior during the CNS.

Hysteresis parameters and magnetic anisotropy of silicate-hosted magnetite exsolutions

SUMMARYAnisotropy of remanent magnetization and magnetic susceptibility are highly sensitive and important indicators of geological processes which are largely controlled by mineralogical parameters of the ferrimagnetic fraction in rocks. To provide new physical insight into the complex interaction between magnetization structure, shape, and crystallographic relations, we here analyse ‘slice-and-view’ focused-ion-beam (FIB) nano-tomography data with micromagnetic modelling and single crystal hysteresis measurements. The data sets consist of 68 magnetite inclusions in orthopyroxene (Mg60) and 234 magnetite inclusions in plagioclase (An63) were obtained on mineral separates from the Rustenburg Layered Suite of the Bushveld Intrusive Complex, South Africa. Electron backscatter diffraction was used to determine the orientation of the magnetite inclusions relative to the crystallographic directions of their silicate hosts. Hysteresis loops were calculated using the finite-element micromagnetics code MERRILL for each particle in 20 equidistributed field directions and compared with corresponding hysteresis loops measured using a vibrating sample magnetometer (VSM) on silicate mineral separates from the same samples. In plagioclase the ratio of remanent magnetization to saturation magnetization (Mrs/Ms) for both model and measurement agree within 1.0 per cent, whereas the coercivity (Hc) of the average modelled curve is 20 mT lower than the measured value of 60 mT indicating the presence of additional sources of high coercivity in the bulk sample. The VSM hysteresis measurements of the orthopyroxene were dominated by multidomain (MD) magnetite, whereas the FIB location was chosen to avoid MD particles and thus contains only particles with diameters <500 nm that are considered to be the most important carriers of palaeomagnetic remanence. To correct for this sampling bias, measured MD hysteresis loops from synthetic and natural magnetites were combined with the average hysteresis loop from the MERRILL models of the FIB region. The result shows that while the modelled small-particle fraction only explains 6 per cent of the best fit to the measured VSM hysteresis loop, it contributes 28 per cent of the remanent magnetization. The modelled direction of maximal Mrs/Ms in plagioclase is subparallel to [001]plag, whereas Hc does not show a strong orientation dependence. The easy axis of magnetic remanence is in the direction of the magnetite population normal to (150)plag and the maximum calculated susceptibility (χ*) is parallel to [010]plag. For orthopyroxene, the maximum Mrs/Ms, maximum χ* and the easy axis of remanence is strongly correlated to the elongation axes of magnetite in the [001]opx direction. The maximum Hc is oriented along [100]opx and parallel to the minimum χ*, which reflects larger vortex nucleation fields when the applied field direction approaches the short axis. The maximum Hc is therefore orthogonal to the maximum Mrs/Ms, controlled by axis-aligned metastable single-domain states at zero field. The results emphasize that the nature of anisotropy in natural magnetite does not just depend on the particle orientations, but on the presence of different stable and metastable domain states, and the mechanism of magnetic switching between them. Magnetic modelling of natural magnetic particles is therefore a vital method to extract and process anisotropic hysteresis parameters directly from the primary remanence carriers.

High-Resolution Petrographic Evidence Confirming Detrital and Biogenic Magnetites as Remanence Carriers for Zongpu Carbonates in the Gamba Area, South Tibet

Paleocene carbonates from the Gamba area of South Tibet provide the largest paleomagnetic dataset for constraining the paleogeography of the India-Asia collision in the early stage. Previous studies argued that the characteristic remanences (ChRMs) obtained from this unit were remagnetized via orogenic fluids. This study carries out a high-resolution petrographic study on the Paleocene carbonates from Gamba aiming to test the nature of the ChRMs. Electron microscopic observation on magnetic extracts identified a large amount of detrital magnetite that are multi- to single domain in sizes and nanoscale biogenic magnetite. Minor framboidal iron oxides were also identified, which were previously interpreted as authigenic magnetite that substitutes pyrite. However, our scanning and transmission electron microscopic (SEM/TEM) observations, along with optical microscope and Raman spectrum investigations further suggest that these magnetic minerals are pigmentary hematite and goethite that are incapable of carrying a stable primary magnetization. We therefore argue that the ChRMs of the limestones from the Zongpu Formation in the Gamba area are carried by detrital and biogenic magnetites rather than authigenic magnetite. The paleomagnetic data from the Gamba area are interpreted as primary origin and can thus be used for tectonic reconstructions. We emphasize that magnetic extraction, integrated with advanced mineralogic studies (e.g., electron backscatter diffraction and electron diffraction) are effective approaches for investigating the origin of magnetic carriers in carbonate rocks.

New Paleointensity Data From Aniakchak Volcano, Alaska, USA

AbstractThis study presents the first set of Holocene, high‐quality absolute paleointensity data from Alaska, USA. Existing paleointensity data for the Holocene are generally located at mid‐northern latitudes in North America, Europe, the Middle East, and eastern Asia. Relatively few data are from the Alaska region. IZZI‐modified paleointensity experiments were conducted on glassy volcanic materials from Aniakchak volcano, a mid‐ to high‐latitude composite volcano on the Alaska‐Aleutian arc. The CCRIT selection criteria were applied to the paleointensity results. A total of 30 specimens from six samples with estimated ages ranging from 1931 CE to 2,300 years before present passed all selection criteria. The sample‐mean paleointensities ranged from 49.5 to 68.0 microTesla (μT). The sample‐mean paleointensity results are comparable to modeled intensities, however all except for one sample‐mean paleointensity are lower than those predicted by geomagnetic field models. The paleointensity estimate for the historical 1931 CE eruption was about 15 μT greater than the expected field strength. This overestimate may result from unrecognized alteration or non‐ideal remanence carriers in this sample. Further evaluation of samples from the 1931 CE eruption using a Bayesian estimation method resulted in a paleointensity estimate that encompasses the historical field strength within uncertainty. These new paleointensity results are a valuable contribution to the mid‐ to high‐northern latitude paleomagnetic data set. Incorporation of these data into future geomagnetic field models will improve the predictions of geomagnetic field behavior in the Alaska region.

Improvements to the Shaw-Type Absolute Palaeointensity Method

Palaeointensity information enables us to define the strength of Earth’s magnetic field over geological time, providing a window into Earth’s deep interior. The difficulties in acquiring reliable measurements are substantial, particularly from older rocks. Two of the most significant causes of experimental failure are laboratory induced alteration of the magnetic remanence carriers and effects relating to multidomain magnetic carriers. One method that has been claimed to overcome both of these problems is the Shaw method. Here we detail and evaluate the method, comparing various selection criteria in a controlled experiment performed on a large, non-ideal dataset of mainly Precambrian rocks. Monte Carlo analyses are used to determine an optimal set of selection criteria; the end result is a new, improved experimental protocol that lends itself very well to the automated Rapid 2G magnetometer system enabling experiments to be carried out expeditiously and with greater accuracy.

Recording Fidelity of Relative Paleointensity Characteristics in the North Pacific Ocean

AbstractNorth Pacific Ocean sediments are important archives of geomagnetic field and paleoenvironmental evolutions, yet late Quaternary sedimentary sequences in the North Pacific Ocean are less explored because of generally low sedimentation rates and the challenge of dating sediments deposited below the calcite compensation depth. Core NP02 sediments from the North Pacific Ocean contain three visible tephra layers, which are identified as the To‐Of, Spfa‐1, and Kt‐3 tephra, respectively. An age model for core NP02 is established based on tephra correlation and one radiocarbon date, which gives a mean sedimentation rate of ∼11.6 cm/kyr. Magnetic analyses suggest the dominance of two remanence carriers; detrital vortex state and biogenic single domain magnetite. Variable depth offsets between the relative paleointensity (RPI) signals carried by the two remanence carriers adds a negligible age error (<0.5 kyr) to the core NP02 RPI record. Pronounced RPI amplitude variations are observed, and the Rockall and Laschamp excursions are identified in the core NP02 RPI record based on the age model. The fidelity of the core NP02 RPI record is further verified by comparison with other RPI stacks and records, and we demonstrate that the RPI variations can assist in chronology refinement.

Mineral Magnetic Characterization of High‐Latitude Sediments From Lake Levinson‐Lessing, Siberia

AbstractLevinson‐Lessing Lake in northern Central Siberia is a sedimentary archive characterized by continuous, widely constant sedimentation at high rates (0.7 m ka−1 for >32 ka). This study provides the first evidence of the suitability of the lake′s sediments for paleomagnetic analyses using the 46‐m‐long core Co1401. Although the lowermost 8 m are disturbed, the upper 38 m of Co1401 provide the preconditions for an exceptional, high‐resolution paleomagnetic record located within the tangent cylinder of the inner core. High‐resolution analyses of magnetic susceptibility, anhysteretic remanent magnetization, isothermal remanent magnetization, and hysteresis parameters show largely uniform mineral magnetic properties. First‐order reversal curves indicate magnetite particles in pseudo‐single domain state are the main remanence carrier, supplemented by single‐domain particles, originating likely from magnetotactic bacteria. Above 6.7 m, the bulk magnetic mineralogy is slightly harder than below and initial greigite formation occurs. However, the main remanence carriers are still of detrital origin.

New high-quality paleomagnetic data from the Borborema Province (NE Brazil): Refinement of the APW path of Gondwana in the Early Cambrian

The Neoproterozoic-Paleozoic transition (~541 Ma) was a turning point in Earth’s history resulting in great biological changes between the microbial Precambrian life and the Ediacaran biotic revolution with the occupation of the sedimentary substrate, the dawn of biomineralization and the appearance of the earliest multicellular organisms. In parallel, this period is marked by a large plate reorganization leading to the assembly of Gondwana and by major climatic changes (extreme glacial events). Due in part to a poor paleomagnetic database for the different cratons in the Ediacarian-Cambrian times, the global paleogeography at that time remains controversial. In this study we present a new high-quality paleomagnetic pole (R = 7) for the Monteiro dyke swarm in the Borborema Province (NE Brazil) located at 18.2°S and 344.9°E (A95 = 11.7° K = 9.3). They are fine-grained hornblende dolerite dated by U-Pb on zircon at ~538 Ma. Rock magnetic data indicate that magnetite and pyrrhotite are the main remanence carriers. Positive baked-contact tests support the primary remanence obtained for these dykes (19 sites). A positive reversal test (classified C) was also obtained from the 14 sites with negative inclination and the 5 sites with positive inclination, indicating that the paleosecular variation was eliminated. Our new key pole is not consistent with the classical apparent polar wander path of the Gondwana which consists of a long track from a southern polar position at ~590 Ma to an equatorial position at ~520 Ma, and suggests instead rapid and small oscillations of the APW, after the end of the large IITPW at ca. 560 Ma. These TPWs are supposedly caused by changes in the inertia tensor of the Earth due to internal mass redistribution, related to rapid changes in subduction velocity. Links of these rapid oscillations and the timing of the Cambrian radiation could be crucial to understand the early history of animal life

Single Particle Multipole Expansions From Micromagnetic Tomography.

Micromagnetic tomography aims at reconstructing large numbers of individual magnetizations of magnetic particles from combining high‐resolution magnetic scanning techniques with micro X‐ray computed tomography (microCT). Previous work demonstrated that dipole moments can be robustly inferred, and mathematical analysis showed that the potential field of each particle is uniquely determined. Here, we describe a mathematical procedure to recover higher orders of the magnetic potential of the individual magnetic particles in terms of their spherical harmonic expansions (SHE). We test this approach on data from scanning superconducting quantum interference device microscopy and microCT of a reference sample. For particles with high signal‐to‐noise ratio of the magnetic scan we demonstrate that SHE up to order n = 3 can be robustly recovered. This additional level of detail restricts the possible internal magnetization structures of the particles and provides valuable rock magnetic information with respect to their stability and reliability as paleomagnetic remanence carriers. Micromagnetic tomography therefore enables a new approach for detailed rock magnetic studies on large ensembles of individual particles.

Dating the Hemudu Neolithic rice cultivation site, East China, by paleomagnetic chronostratigraphy

Hemudu is a famous archaeological site with the earliest rice remains unearthed in East China and represents a classic example of how Neolithic people managed coastal farmland. However, appreciation of human adaptation to Holocene sea-level changes has been hampered by low-resolution chronology due to lack of datable materials in coastal sediments. Correlation of paleomagnetic directions and intensity on a regional scale provides independent relative dating of such sediments. We did high-resolution paleomagnetic chronology work on core HMD13 (27 m in length) from Hemudu Neolithic site and discussed relevant early Holocene paleoclimate change of Southern China. Magnetic minerals identified by scanning electron microscopy are magnetite, iron-bearing silicates, and iron sulfide (pyrite or greigite). Rock magnetic measurements indicate that the primary remanence carrier is single-domain magnetite. Stepwise alternating field (AF) demagnetization experiments at 1 cm intervals on U-channel samples show that paleomagnetic inclinations fluctuate around 60°, with five major peaks and four troughs. A relative paleointensity (RPI) was estimated using normalizing natural remanent magnetization intensity to anhysteretic remanent magnetization over 20–40 mT AF range, which has four major peaks. Variations of inclination and RPI in core HMD13 resemble the data from the East China Sea and allowed the development of a refined age-depth model. The new adjusted age-depth model minimized dating errors of 14C ages among different datable materials. From the new age model, inclination and RPI of HMD13 are comparable to paleosecular variation (PSV) stack from East Asia and predicted results from geomagnetic models. Four cold events in the early Holocene recorded by geochemical proxies imply that sedimentary sequence of core HMD13 was influenced by global paleoclimate variation, while its long-term trend points to local paleoenvironmental change. Increases in sedimentation rates and the marine-derived sediment fractions suggest a massive transgression in the early Holocene (9–7.5 ka). Subsequently, ancient people developed and built pile dwellings since ~7 ka and cultivated wild rice from ~6.3 ka. Our study demonstrates that regional stratigraphic correlation with well-dated PSV and RPI records is a practical approach to establishing reliable age-depth models. A high-resolution chronology on continuous sedimentary sequence has excellent potential to elucidate prehistoric human-environment co-evolution.

Hysteresis of Natural Magnetite Ensembles: Micromagnetics of Silicate‐Hosted Magnetite Inclusions Based on Focused‐Ion‐Beam Nanotomography

AbstractThree‐dimensional geometries of silicate‐hosted magnetic inclusions from the Harcus intrusion, South Australia have been determined using focused‐ion‐beam nanotomography (FIB‐nt). By developing an effective workflow, the geometries were reconstructed for magnetic particles in a plagioclase (162) and a pyroxene (282), respectively. For each inclusion, micromagnetic modeling using Micromagnetic Earth Related Rapid Interpreted Language Laboratory provided averaged hysteresis loops and backfield remanence curves of 20 equidistributed field directions together with average Ms, Mrs, Hc, and Hcr. The micromagnetic structures within each silicate are single‐domain (SD), single‐vortex (SV), multivortex (MV) and multidomain states. They have been analyzed using domain‐state diagnostic plots, such as the Day plot and the Néel plot. SD particles can be subdivided into groups with dominant uniaxial anisotropy (Mrs/Ms ∼0.5 and 10 < Hc < 100 mT) and mixed uniaxial/multiaxial anisotropy (Mrs/Ms ∼0.7 and 10 < Hc < 30 mT). Most SV particles lie on a trend with 0 < Mrs/Ms < 0.1 and 0 < Hc < 10 mT, while others display a broad range of intermediate Mrs/Ms and Hc values. SV and MV states do not plot on systematic grain‐size trends. Instead, the multicomponent mixture of domain states within each silicate spans the entire range of natural variability seen in bulk samples. This questions the interpretation of bulk average hysteresis parameters in terms of grain size alone. FIB‐nt combined with large‐scale micromagnetic simulations provides a more complete characterization of silicate‐hosted carriers of stable magnetic remanence. This approach will improve the understanding of single‐crystal paleomagnetism and enable primary paleomagnetic data to be extracted from ancient rocks.

New paleomagnetic pole and magnetostratigraphy of the Cauvery Basin sediments, southern India

Magnetostratigraphy or magnetic polarity stratigraphy (MPS) is constructed with paleomagnetic parameters for the Campanian–Maastrichtian (Upper Cretaceous) onshore sediment sequences of the Cauvery Basin, southern India. Twenty-nine sedimentary outcrops in the vicinity of Ariyalur district of Tamil Nadu, India were studied using AF (5–150 mT) and thermal demagnetization (100–700°C). The observed remanence carrier is attributed to hematite through rock magnetic experiments. The virtual geomagnetic pole (VGP) latitudes were computed using the acquired characteristic remanent magnetization (ChRM) directions. The mean ChRM produce Dm= 338, Im= –38, (α95=23.91°, k = 15.73, N=60). The mean VGP is estimated at 51.33°N, 292.71°E deriving a paleolatitude of 21.3°S. The constructed magnetic polarity stratigraphy (MPS) is correlated with the standard geomagnetic polarity time scale (GPTS). The composite MPS of these sequences comprises of 12 magnetozones (6 normal and 6 reversed events) that are corroborated with Chron C33n to Chron C30n of the GPTS. The derived paleolatitude position from the present study places Indian subcontinent at little shallow southern latitudes indicating moderately higher drift velocities during Upper Cretaceous.

New high precision full-vector archaeomagnetic data from a roman kiln in Mérida (Spain)

This study presents new high precision age and full-vector archaeomagnetic data from a kiln excavated in the Roman archaeological site of Mitreo's house (Mérida, Badajoz, Spain). The age of the kiln was obtained by the stratigraphic method and by the ceramological study of the italic and sigillata pottery found with a very precise age date of 55 ± 15 years AD. Rock-magnetic experiments pointed towards magnetite as the main carrier of remanence and highly reversible thermomagnetic curves suggested that the studied samples were suitable for archaeoeointensity determinations.Paleomagnetic experiments including thermal and stepwise alternating field demagnetization yielded the following mean direction for the kiln: declination D = 0.6°; inclination I = 54.0°; (k = 481; α95 = 2.5°). Archaeointensityexperiments with the Thellier – Coe protocol on 28 samples yielded successful determinations in 27 cases. Anisotropy factors between 0.90 and 1.04 were obtained from anisotropy of thermoremanent magnetization (ATRM) experiments. A mean anisotropy-corrected archaeointensity value F = 56.3 ± 5.5 μT was obtained.The geomagnetic model SHA.DIF.14 k was used for an archaeomagnetic dating yielding a chronological interval between 40 BCE and 150 CE. This low age resolution when compared with the pottery-based age data is related to the behavior of the geomagnetic field in the Iberian Peninsula during the Roman period, which does not allow to differentiate well between results corresponding to those centuries. However, it is also related to the fact that the Iberian archaeomagnetic dataset in the analysed time range is highly scattered. A high quality full-vector data with a very precise age have been obtained which contribute to improve the Iberian secular variation curve and geomagnetic databases.

Magnetoelastic properties and behaviour of 4C pyrrhotite, Fe7S8, through the Besnus transition

Pyrrhotite, Fe7S8, is a commonly occurring carrier of magnetic remanence and has a low temperature transition, the Besnus transition, involving a change in spin state. Variations of the thermodynamic, magnetic and elastic properties through this transition at ∼33 K in a natural sample of 4C pyrrhotite have been tested against a group theoretical model for coupling between order parameters relating to Fe/vacancy ordering (irrep U1(1/2,0,1/4)) and magnetic ordering (irreps m and m). Magnetoelastic coupling is weak but the pre-existing microstructure of ferroelastic and magnetic domains, that develop as a consequence of Fe/vacancy and ferrimagnetic ordering during slow cooling in nature (P63/mmc → C2′/c′), causes subtle changes in the low temperature transition (C2′/c′ → P). The Besnus transition involves a rotation of magnetic moments out of the a–c plane of the monoclinic structure, but it appears that the transition temperature might vary locally according to whether it is taking place within the pre-existing domain walls or in the domains that they separate. Evidence of metamagnetic transitions suggests that the magnetic field–temperature phase diagram will display some interesting diversity. Low temperature magnetic transitions in minerals of importance to the palaeomagnetism community have been used to identify the presence of magnetite and haematite in rocks and the Besnus transition is diagnostic of the existence of pyrrhotite, Fe7S8.

Palaeomagnetism of the Dundas–Fossey Trough, Tasmania: Oroclinal rotation and Late Cretaceous overprinting

The Dundas–Fossey Trough, a curved belt of Early Palaeozoic rocks in western and northern Tasmania, is hypothesised to have developed as an orocline driven by asthenospheric flow behind a rapidly retreating subduction zone on the East Gondwana margin. Rocks of the Wurawina Supergroup from the trough were sampled for a palaeomagnetic test of this hypothesis. Rock magnetic analysis identifies both magnetite and hematite remanence carriers. Hematite carries a normal-polarity overprint which was acquired at relatively low temperature. Thermal demagnetisation over the magnetite unblocking range reveals a linear trend that defines component A, which displays both normal and reversed polarity. Component A passes a modified version of the fold test, indicating that it is pre-deformational. The declination of component A correlates linearly with regional strike, thus passing the orocline test. A palaeomagnetic pole for the Cambrian Owen Group, after correction for oroclinal rotation, is displaced from the Gondwana polar wander path, suggesting that the western limb of the trough may have been rotated anticlockwise by about 40° prior to the development of the orocline, presumably during known Early to Middle Ordovician deformation. Adjustment of the palaeomagnetic declination data to account for this earlier phase of rotation improves the fit parameters of the orocline test. The palaeomagnetic results are consistent with the orocline model for the Dundas–Fossey Trough, and support the inference that the trough extends beneath later cover in southeastern Tasmania. Overprint component B yields a mean pole in broad agreement with other overprints previously observed both in Tasmania and the eastern seaboard of the Australian mainland, and like them appears to have been acquired during the Late Cretaceous normal polarity superchron. We speculate that magnetic overprinting in Tasmania is related to enhanced oxidation by meteoric water driven by regional uplift.

Downward remagnetization of a ∼74-m-thick zone in lake sediments from palaeo-Lake Idaho (NW United States)—Locating the Gauss/Matuyama geomagnetic boundary within a dual-polarity zone

SUMMARY Remagnetization is an important issue in palaeomagnetism. Here, we discuss an extraordinarily thick (∼74 m) dual-polarity transition zone between the Gauss and Matuyama Chrons. The studied succession is from a drill core through lacustrine sediments of palaeo-Lake Idaho (Snake River Plain, NW United States of America) that are intercalated with basalt units. We identified detrital Ti-rich titanomagnetite and magnetite in lamellar exsolutions as the main carriers of a primary remanence, likely derived from the basalts that erupted in the Snake River Plain. Stepwise thermal demagnetization revealed a single-component remanent magnetization with reversed and normal polarities above and below the transition zone, respectively. Based on rock-magnetic results, microscopic observations, and previously known events in the evolution of palaeo-Lake Idaho, the reversed-polarity component in the transition zone represents a secondary chemical remanent magnetization caused by magnetic mineral alteration or partial neo-formation of magnetite, in association with strong depletion of the primary detrital magnetic minerals that affected a wide depth range below the level where the remagnetization event occurred. This remagnetization event was most likely related to lake-level lowering and partial desiccation of palaeo-Lake Idaho. Understanding the nature and origin of the remagnetization allows to identify the polarity boundary in the unusual case of a secondary magnetization with reversed polarity produced downward in a sequence to an extraordinary large depth. Based on available age information, the observed reversal represents the Gauss/Matuyama boundary, which provides an important age constraint for palaeoclimatic interpretation of the succession.

Quaternary stratigraphic architecture and sedimentaryevolution from borehole GB014 in the westernXiong’an New Area

To scientifically utilize underground space and to explore the regional structural characteristics and processes of basin evolution of the North China Plain, we combine paleomagnetic and sedimentary analyses of sediments from borehole GB014, which extends 200 m deep, in the western Xiong’an New Area. Magnetostratigraphy and regional sedimentary characteristics were determined to establish a chronological framework. Sedimentary facies and sedimentary systems were reconstructed by considering the lithology, geophysical logs gamma ray ( GR ), and grain size, sediment color ( L *, a * and b *) and magnetic susceptibility measurements. To determine the remanence carriers and magnetic mineralogy of the sediments, rock magnetic measurements were performed on 8 representative samples from various depths. A total of 145 specimens were subjected to progressive thermal demagnetization up to a maximum temperature of 690 ° C, with intervals of 25−50 ° C below 585 ° C and 10−25 ° C above 585 ° C, using a Magnetic Measurements Thermal Demagnetizer (TD48) with a residual magnetic field less than 10 nT. Paleomagnetic measurements were made using a 2G Enterprises Model 760-R cryogenic magnetometer installed in a magnetically shielded space ( GR logs obtained at 20-cm intervals were used to analyze the sedimentary facies. For measurements of sediment color, 526 powder samples were air-dried and then disaggregated, passed through a 200-mesh sieve and measured using a Konica-Minolta SPAD503 spectrometer. The 526 powder samples were packed into 8-cm3 plastic boxes and used to obtain measurements of magnetic susceptibility ( χ ) using a Bartington Instruments MS2B sensor. Electronic scales with a resolution of 0.001 g were used to weigh the samples to enable the mass-specific susceptibility to be calculated. For grain-size measurements, 189 powder samples were pretreated with 10% H2O2 to remove organic matter and 10% HCl to remove carbonates. After standing for 24 h, the residues were dispersed with 10% (NaPO3)6 and ultrasonicated for 10 min. The grain size measurements were made using a Mastersizer-2000 laser analyzer (relative error The main findings are as follows: (1) Magnetite is the main carrier of the characteristic remanent magnetization in these sedimentary sequences, and the secondary carrier is hematite. (2) The borehole measurements recorded the Brunhes and Gauss normal chrons and the Matuyama reversed chron. The depths of the Matuyama/Brunhes and Gauss/Matuyama boundaries are 33.8 m and 135 m, respectively. (3) According to the chronological framework and sedimentary facies, five sedimentary units have been identified, from bottom to top: Unit V, with a depth of 200−146.6 m and sedimentary rate of 4.9 cm/ka, whose age is 3.90−2.81 Ma, is dominated by alluvial fan facies with coarse grain sediments. Unit IV, with a depth of 146.6−108.0 m and sedimentation rate of 2.76 cm/ka, whose age is 2.81−1.88 Ma, is dominated by flood plain facies with fine grain sediments. Unit III, with a depth of 108.0−57.6 m and sedimentation rate of 5.86 cm/ka, whose age is 1.88−1.02 Ma, is dominated by braided channel facies with coarse particle sediments. Unit II, with a depth of 57.6−35.8 m and sedimentation rate of 9.48 cm/ka, whose age is 1.02−0.79 Ma, is dominated by flood plain facies with fine grain sediments. Unit I, with a depth of 0−35.8 m and sedimentation rate of 4.53 cm/ka, whose age is 0.79−0 Ma, is dominated by flood plains interbedded with crevasse fan facies. At borehole GB014, evidence of two tectonic movements that occurred at 3.90−2.81 and 1.88−0.79 Ma have been preserved since the late Pliocene, and sediment provenance probably changed during 1.88−1.02 Ma. The piedmont area of Taihang Mountain hosts two widely deposited layers of coarse-grained sediments resulting from these two tectonic movements, and the Middle and Late Pleistocene sand layers are mainly related to the marine transgression in Bohai Bay and the enhancement of the East Asian monsoon system.

Identification of paleomagnetic remanence carriers in ca. 3.47 Ga dacite from the Duffer Formation, the Pilbara Craton

The ca. 3.47 Ga Duffer Formation has been considered to carry one of the oldest paleomagnetic records. Yet, the lack of rock magnetic data limits the interpretation of the nature of the remanence. We conducted a rock magnetic and paleomagnetic investigation on columnar dacite of the Duffer Formation. The main magnetic minerals are phenocrysts of titanomagnetite and magnetite, and secondary hematite in groundmass. Detailed thermal demagnetization revealed more complex natural remanence than previously estimated, consisting of four components with typical unblocking temperature of 200–350, 200–500, 590, and 690 °C. Combined with alternating field demagnetization and rock magnetic data, they are attributed to titanomagnetite, coarse-grained magnetite, fine-grained magnetite, and hematite, respectively. The comparison of unblocking temperature and coercivity suggests that the previously proposed secondary component is carried by fine-grained magnetite as well as hematite, while the putative primary component is carried by coarse-grained magnetite and titanomagnetite. Microscopic observations showed that coarse-grained magnetite and titanomagnetite are primary crystals, although this does not necessarily indicate they preserve primary remanence. The remanence directions of all components revealed higher scatter than the previous studies, suggesting the need for caution in interpretation. The low unblocking temperature of titanomagnetite suggests that if their remanence is truly primary, the rocks must have kept below ~ 250 °C for ~3.47 billion years.

Constraining the Intracontinental Tectonics of the SW Central Asian Orogenic Belt by the Early Permian Paleomagnetic Pole for the Turfan‐Hami Block

AbstractIn order to better understand the kinematics and geodynamics of the late Paleozoic to early Mesozoic transition from accretionary to intracontinental tectonics in the southwest Central Asian Orogenic Belt, we performed a paleomagnetic study on Lower Permian strata in the Turpan‐Hami Basin, NW China. Magnetite and hematite are shown to be the principal magnetic remanence carriers. A typical sedimentary fabric that has not been modified by postdepositional deformation is recognized via magnetic fabric study. Stable characteristic remanent magnetizations, all of reverse magnetic polarity, are revealed by step demagnetizations. Remanence age is determined to be of Early Permian affinity, based on a fold test, remanence behavior of minerals, and geochronologic data. With inclination shallowing corrections, the first Early Permian paleomagnetic pole for the Turpan‐Hami Block is acquired as λ = 75.7°N, φ = 276.3°E, A95 = 5.7°, and N = 10 sites. Comparisons of this new pole with published ones from neighboring cratonic blocks provide kinematic constraints on the tectonic transition and subsequent intracontinental tectonics of this region. The Turpan‐Hami and Yili blocks have kept their relative positions since the Early Permian. Significant latitudinal movement of 14.7° ± 7.2° occurred between the Turpan‐Hami and South Junggar blocks and could be mainly accommodated by late Paleozoic crustal shortening of at least ~530 km across an intra‐arc basin in the Bogda belt. The Turpan‐Hami Block has experienced large‐magnitude relative rotations of −41.1° ± 7.1° and 21.2° ± 9.4° with respect to Tarim and South Junggar since the Early Permian, respectively, corresponding to dominant intracontinental tectonics characterized by large‐magnitude strike‐slip displacements along megashear zones.

Multistep Parametric Inversion of Scanning Magnetic Microscopy Data for Modeling Magnetization of Multidomain Magnetite

AbstractDevelopment in instrumentation and technology now allows for mapping of magnetic anomalies, caused by spatial variations in magnetization in the source material, from the mineral to the crustal anomalies scale. High‐resolution magnetic mapping techniques allow for accurate investigation of the magnetization in natural rock samples and particularly of their remanence carriers, which can record geologically meaningful information. Multidomain magnetic grains are expected to retain a remanence that is susceptible to change by exposure to magnetic fields or by changes in temperature. Although this makes multidomain grains less reliable remanence carriers for paleomagnetic studies, their magnetization contributes to rocks bulk magnetization and to induced anomalies in the Earth crust. Here, we investigate the fine‐scale magnetization of a sample that exhibits a multidomain behavior. We used a scanning magnetic microscope, equipped with a room temperature magnetic tunnel junction sensor, to map the magnetic field over a petrographic thin section of the sample containing large magnetite grains (>100 μm) surrounded by serpentine and carbonate. We modeled the fine‐scale remanent magnetization of the magnetite by inverting the magnetic scans data acquired in near‐field‐free conditions. We applied a multistep inversion, a priori tested on a synthetic model, with a controlled range on the intensity of the magnetization. Modeling results on the study sample suggest homogenously magnetized regions within the magnetite grains with variable remanent magnetization intensities and directions coherent with the multidomain behavior inferred from bulk measurements.