Properties Of Heat Affected Zone Research Articles

Microstructure, mechanical properties and deformation behavior of laser additively repaired 5083 and 6061 Al alloys utilizing AlMgScZr powders

Laser additive repair (LAR), as an efficient repair method, lacks specialized repair materials for Al alloys. In this work, the high-strength AlMgScZr powder was employed to address the scarcity of specialized materials and the issue of inadequate performance in LAR of 5083-H112/6061-T6 Al alloy. The microstructure, mechanical properties and deformation behavior of repaired specimens were studied. The repair zone (RZ) had high strength and high density, and the porosity was as low as 0.12 %. There was good compatibility between the repair material and the base metal (BM), and good metallurgical bonding was achieved at the fusion line. The microstructure and strengthening phase (T-phase) in the heat affected zone (HAZ) of the 5083 repaired parts exhibited negligible changes, there was no deterioration in mechanical properties. The yield strength was 162 MPa, tensile strength was 291 MPa, and elongation was 16.2 %, reaching 94 %, 104 %, and 70 % of the BM, respectively. The mechanical properties are superior in the current research on LAR of Al alloys. The LAR technique showcases its versatility in repairing aging non-strengthening Al alloys. The transition of β′′→β′ (or with B′/U1/U2)→β of the nano-reinforced phase resulted in deteriorative mechanical properties of HAZ in the 6061 repair part, consequently, the tensile strength of 6061 repair part was only 63.8 % of the strength of BM. After solution aging treatment, the β′′ phase in HAZ re-precipitated, effectively restoring the strength of 6061 repaired parts. The tensile strength of the repaired parts was increased to 95.2 % of the strength of BM. The present study elucidates the evolution of microstructure and mechanical properties during LAR process of Al alloys, offering valuable insights for future applications of this technology on Al alloys.

Deep learning coupled Bayesian inference method for measuring the elastoplastic properties of SS400 steel welds by nanoindentation experiment

Nanoindentation experiment has shown broad application prospects due to its ability to measure the mechanical properties of various materials at multiple scales. In this paper, a deep learning coupled Bayesian inverse approach is proposed for measuring the elastoplastic parameters of SS400 steel welds by nanoindentation experiment. The nanoindentation experiments were performed on the SS400 steel welds, including base metal (BM), weld zone (WZ), and heat affected zone (HAZ), and the experiment load–displacement (P-h) curves were obtained. The hyper-parameters tunable artificial neural network (ANN) was established to correlate elastoplastic parameters with indentation P-h curves. Based on Bayesian inference theory, the posterior density function for estimating the unknown material parameters was established. Transitional Markov chain Monte Carlo was used for sampling from the posterior density function, and the elastoplastic properties in different regions of SS400 steel welds were identified. The advantage of the established measuring method is that the hyper-parameters optimized ANN model can provide the very accurate forward relationship between material properties and indentation P-h curves. Besides, the inverse Bayesian framework can quantify the potential uncertainty of the identified elastoplastic parameters. The measured elastoplastic properties of the base metal of SS400 steel show good agreement with tensile experiment data, of which the maximum measuring error is less than 12%. The measured elastoplastic properties in WZ and HAZ are also proved to be effective. The uncertainty of the identified elastoplastic parameters of SS400 steel welds can be quantified by posterior marginal distribution, using Mean and Variance values. The results proved that the proposed inverse measuring method is reliable and effective.

Influence of microalloying on precipitation behavior and notch impact toughness of welded high-strength structural steels

Microalloying elements such as Nb and Ti are essential to increase the strength of quenched and tempered high-strength low alloy (HSLA) structural steels with nominal yield strength ≥ 690 MPa and their welded joints. Standards such as EN 10025–6 only specify limits or ranges for chemical composition, which leads to variations in specific compositions between steel manufacturers. These standards do not address the mechanical properties of the material, and even small variations in alloy content can significantly affect these properties. This makes it difficult to predict the weldability and integrity of welded joints, with potential problems such as softening or excessive hardening of the heat-affected zone (HAZ). To understand these metallurgical effects, previous studies have investigated different microalloying routes with varying Ti and Nb contents using test alloys. The high-strength quenched and tempered fine-grained structural steel S690QL is the basic grade regarding chemical composition and heat treatment. To evaluate weldability, three-layer welds were made using high-performance MAG welding. HAZ formation was investigated, and critical microstructural areas were identified, focusing on phase transformations during cooling and metallurgical precipitation behavior. Isothermal thermodynamic calculations for different precipitations were also carried out. Mechanical properties, especially Charpy notch impact toughness, were evaluated to understand the influence of different microalloys on the microstructure of the HAZ and mechanical properties.

Local shear fracture properties in heat-affected zone of resistance spot-welded advanced high-strength steel

In the process of resistance spot welding of advanced high-strength steel (AHSS), the development of heat-affected zones (HAZs) considerably modifies the mechanical properties of the weld region. However, the limited reporting in the study of shear behavior in the HAZ hinders the accurate prediction of joint fracture and failure behavior. This study focused on the shear fracture behavior of resistance spot-welded AHSS. Given the limited extent of the HAZ, a miniature shear test was designed and shear fracture tests were conducted on JSC590, JSC980, and JSC1180. These tests facilitated the acquisition and compilation of data regarding the shear mechanical properties of diverse steel grades and their respective HAZs. A hardness-based empirical model for the strength coefficient and the strain-hardening exponent in Hollomon's law was introduced, and this model was subsequently integrated into finite element method calculations. The accuracy of the model was validated by shear strength reproductions, exhibiting errors within the range of 5.4%–13.5% and the averaged error was less than 10%. Further analyses confirmed that stress triaxiality at critical positions varied from 0 to 0.33, indicative of shear-dominant stress conditions. Moreover, the evolution of stress states revealed a notable association between the fracture surfaces across different stress states and steel grades. These findings fill the gap regarding the shear behavior of localized HAZs and expand the understanding of their mechanical behavior under various stress states. It will contribute to accurate fracture prediction by stress triaxiality based fracture criteria, such as Modified Mohr-Coulomb (MMC) model, applied to AHSS.

Mechanical behavior of dissimilar AL6XN-IN718 welded joint obtained by cold metal transfer

Cold metal transfer (CMT) welding process was used to join the AL6XN super-austenitic stainless steel to a nickel-based super alloy IN718. Microhardness, tensile and low cycle fatigue tests were carried out to determine the mechanical properties of the welded joint. The heat used to perform the weld decreases the microhardness in the heat affected zone (HAZ) of the IN718 material. A decrement of about 50% with respect to the base material (∼410 HV0.2) was observed, which is attributed to the microstructural transformation produced by the weld thermal cycles, inducing the partial dissolution of the γ'′ phase in the nickel matrix. In contrast, the HAZ on the AL6XN side, the microhardness tends to be similar with respect to the base material (∼203 HV0.2). In terms of the fracture energy, determined from the stress-strain plot, the welded joint decreases about 60–65% with respect to the base materials. This tendency was also observed in the case of the Charpy impact test behavior. From the low cycle fatigue test, it was observed that AL6XN material and AL6XN-IN718, performed better than the IN718 alloy, i.e. more tolerance to the strain cyclic, increasing the number of cycles to failure. A 3-D transient thermal conduction finite element model was developed to correlate the thermal history with the microstructural transformation on the HAZ and mechanical properties. The weld thermal cycles are in good agreement with the experimental measurements obtained by K-type thermocouples.

The Effects of Post Weld Heat Treatment on Microstructure and Mechanical Properties of API X70 Linepipe using Submerged Arc Welding

API X70 steel requires high strength and toughness for safety in extreme environments like high pressure and low temperature. Submerged Arc Welding (SAW ) is effective for manufacturing thick steel pipes. However, the welding heat input during SAW alters the microstructure and mechanical properties of the heat affected zone (HAZ). Therefore, investigating the correlation between microstructure and mechanical properties in welded X70 pipes is important to address potential degradation of HAZ and weld metal (WM). In this study, post weld heat treatment (PWHT) was performed to improve mechanical properties of HAZ and WM and to reduce residual stress caused by the welding process. We performed PWHT at 640°C for 15 hours and followed by air cooling. After heat treatment, we observed the microstructure through OM and SEM analysis, and investigated the mechanical properties through tensile test, hardness test, and Charpy impact test.

Embrittlement Fracture Behavior and Mechanical Properties in Heat-Affected Zone of Welded Maraging Steel.

In welded maraging steels, mechanical properties, particularly ductility and toughness, are often compromised in the heat-affected zone (HAZ). This study focuses on 300-grade maraging steel bars, solution annealed at 1123 K for 1.5 h (5.4 ks) and welded using gas tungsten arc welding, followed by a post-weld heat treatment at 753 K for 13.33 h (48 ks). In situ observations during three-point bending tests on HAZ samples featuring coarsened prior austenite grain sizes were conducted to examine damage behavior and the crack path near the crack tip. The main crack initiated at the peak applied load during the bending test and, upon further loading, exhibited significant deflection and extension accompanied by numerous microcracks and localized crack branching. Distinctive damage features, such as transgranular cracking across block regions, intense intergranular cracking along packet boundaries with a pronounced shear component, and crowding of microcracks ahead of the crack tip, were observed in the HAZ sample during the in situ test. The interaction between the main crack tip and microcracks and its influence on the local crack propagation driving force was discussed using fracture mechanics. Experimental results, including tensile fracture surface observations and in situ images, along with analysis of the stress anti-shielding effect by microcracks, suggest that the HAZ sample exhibits embrittlement fracture behavior with lower ductility and toughness compared to the base metal sample.

Effect of intrinsic thermal cycles on the microstructure and mechanical properties of heat affect zones in laser cladding coatings on full-scale rails

Laser cladding (LC) wear-resistant alloy on the surface of pearlite rails has been proven to be able to improve their wear resistance significantly. However, the rapid cooling rate in LC will result in the formation of martensite structures with high hardness but low toughness in heat affected zone (HAZ), making the rails' service safety endangered. In this paper, a novel method was proposed to eliminate the un-tempered martensite in U71Mn rail based on the in-situ gradient tempering (IGT) effect induced by the intrinsic thermal cycles in multilayer LC. The influence mechanisms of interlayer and inter-track thermal cycles on the evolutions of microstructure and mechanical properties of HAZs were studied systematically. The results illustrate that the martensite in HAZs can be gradually tempered within the optimal IGT temperature range, and the tempering processing mechanisms are as follows: firstly, the ε-carbides precipitate from HAZs and then dissolve to form granular cementites. Then, the cementites form colonies of lathlike particles with similar orientations. Finally, a composite structure consisting of fine-tempered sorbite and granular cementites forms, in which the lamellar spacing of sorbite is <1/5 of that of the original pearlite, and the proportion of the high angle grain boundaries has increased by 2.2 times. During the tempering process, the microhardness of HAZs gradually decreases, accompanied by the increase of the bending properties therein. The ultimate bending strength and fracture strain of the specimens with fully tempered HAZs are enhanced to be about 1.6 and 5.5 times as much as those of the specimens with fully quenched HAZs, even much better than the substrate.

Reducing the taper and the heat-affected zone of CFRP plate by Micro fluid assisted laser induced plasma micro-drilling

Carbon Fiber Reinforced Plastics (CFRP) with superior mechanical properties are widely used in aerospace, automotive, and medical fields. The characteristics of CFRP with anisotropy and inhomogeneous result in poor machining performances by conventional drilling techniques. Laser drilling is a non-contact high precision machining technique without tool wear but leads to a large heat-affected zone (HAZ) and taper. Although underwater laser drilling could reduce thermal damage on CFRP surface, bubbles produced in the machining process severely affect the machining stability and surface quality. In this study, a micro fluid-assisted laser-induced plasma drilling (MFA-LIPMD) method was proposed to relieve the negative effect of bubbles as well as reduce the taper and HAZ. A comprehensive analysis of hole surface quality, HAZ, taper, and mechanical properties was conducted, and MFA-LIPMD performed more advantages over laser in the air (LIA) and laser-induced plasma drilling (LIPMD). It was found that the taper of micro-holes was reduced by 42.8%–51.78%, and the thermal damage rate of micro holes processed by the MFA-LIPMD process was reduced by 65.3%–68.1% compared with the LIPMD process, and the maximum tensile load of samples was increased by about 7.68%. Therefore, MFA-LIPMD has great potential for machining high-quality micro holes of CFRP plates.

The effect of heat input in multi-pass GMAW of S960QL UHSS based on weaving and stringer bead procedure on microstructure and mechanical properties of HAZ

Quenched and tempered S960QL (yield strength ≥ 960 MPa) ultra-high strength steel (UHSS) thick plates were joined by multi-pass robotic gas metal arc welding (GMAW) using weaving and stringer bead techniques. The effects of microstructural changes in heat-affected zone (HAZ) of the joint on toughness and hardness were examined. Weaving and stringer bead techniques applied for the multi-pass welding procedure altered average peak temperatures and exposure time to those temperatures. Mechanical properties of HAZs were evaluated by utilizing notch impact and hardness tests, and these results were correlated with microstructural characterizations using optical (OM) and scanning electron microscopes (SEM). Prior austenite grain (PAG) coarsening occurred because of increased exposure time to peak temperature in coarse-grained HAZ (CGHAZ) of the W-5 (weaving pass) joint. CGHAZs at the face pass, which have not been subjected to a second thermal cycle, have the highest hardness in both joints. Hardness of SCHAZ and CGHAZ of S-12 joint was 7% and 1% higher compared with W-5 joint, respectively. Weld metal hardness of W-5 joint was 15% lower than that of S-12 joint. Both joints not only fulfilled the requirements of minimum 50 J per EN ISO 10025-6 at −20 °C but exceeded this limit by 50% (W-5) and 200% (S-12). Lateral expansions for impact toughness specimens were around 17.5% for S-12 joint, whereas it was 4% for W-5 joint. Since HAZ in the S-12 (stringer bead) joint is narrow compared with the one in the W-5 joint, impact toughness values were higher with the S-12 joint due to the locations of the notches of the impact specimens.

ELECTROCHEMICAL ARC DRILLING OF NICKEL–TITANIUM SHAPE MEMORY ALLOY USING MOLYBDENUM ELECTRODE: INVESTIGATION, MODELING AND OPTIMIZATION

In the present scenario, electrochemical arc machining (ECAM) (hybrid of electric discharge erosion and electrochemical dissolution) is an evolving procedure for difficulty in machining the materials due to constraints of existing processes. This research aims to investigate the machinability of Ni[Formula: see text]Ti alloy through electrochemical arc drilling using molybdenum electrode. Electrolyte concentration (ethanol with ethylene glycol and sodium chloride), supply voltage, and tool rotation are considered as the variable factors to evaluate the ECAM performance characteristics in drilling blind hole operation concerning overcut (OC), tool wear rate (TWR) and materials removal rate (MRR). Consequently, response surface methodology is implemented for predictive modeling of various performance characteristics. Finally, multi-objective optimization through desirability function approach (DFA) has produced a set of optimal parameters to improve the productivity along with the accuracy, which is the prime requirement for the industrial applicability of the ECAM process. Results demonstrated that supply voltage is the influential key factor for improvement of machining rate. Scanning electron microscope (SEM) photographs revealed the development of heat affected zone (HAZ), white layer, melted droplet, craters, re-solidified material, ridge-rich surface and voids as well as cavities around the end-boundary surfaces of a blind hole. Composition analysis through energy dispersive spectroscopy (EDS) indicated the oxygen content on the machined surface because electrolyte breakdown causes oxidation to take place at elevated temperatures across the machining zone. Moreover, carbide precipitation like TiC was found in the melting zone of the drilled hole, as revealed by X-ray diffraction (XRD) analyses, which has the affinity to reduce the SMA properties in HAZ.

Using Functionally Graduated Materials Concept to Predict the Damage of Heat-Treated Elbows Under Bending and Pressure Loading

Abstract Elbows in pressurized tubular structures are increasingly stressed by loadings with radial and tangential stresses. These stresses are completely different from those of straight tubular structures. Through the finite element method and using the ABAQUS computer code, the damage of a tubular structure in X60 of an elbow attached by straight parts stressed in internal pressure and in the moment of bending in closing is analyzed in this work. As a proposal for reinforcement, this structure is previously heat-treated and partially at the level of the elbow. The formulation of the heat-treated X60 material is based on the concept of functional graded materials (FGM), where the graduation by volume fraction between the metal in its base and that previously heat-affected named heat affected zone (HAZ) is under a power function of a parameter named volume fraction index (n). The graded properties of HAZ in the base metal along the thickness of the tubular structure are introduced by a row of finite elements using a proposed meshing technique. The elastic–plastic behavior of the HAZ-base metal mixture under the Voce model follows the equivalent stress flow theory of Von Mises. The technique of extended finite element technique (XFEM) in the damage and the mesh proposed in the graduation, were used to evaluate the various parameters, such as: the internal pressure and the heat treatment (surface and index n). The latter condition the response of the structure and the level of its damage.

Preliminary assessment of the possibility to use large-diameter pipes of Х52 steel for transportation of pure gaseous hydrogen under pressure

To assess resistance to hydrogen embrittlement caused by the presence of hydrogen in the transported product, and, accordingly, suitability of pipes for hydrogen transport, the base metal of large-diameter pipes of X52 strength class manufactured by JSC “ChelPipe” (part of the PJSC “TMK” group of companies) was studied. The work included the study of pure gaseous hydrogen effect under pressure up to 10 MPa on change in mechanical characteristics of the base metal of large-diameter pipes (LDP) during preliminary hydrogen charging for various time periods in a stationary autoclave under pressure, and during simultaneous loading with a slow strain rate (SSRT) under expected operating conditions. Results of the X52 LDP metal study show that there is no significant impact on the effect of gaseous hydrogen under pressure for up to 144 hours on mechanical characteristics of the base metal determined by static uniaxial tension (decrease in ductile characteristics does not exceed 9 %). During SSRT at a rate of not more than 1·10–6 s–1 in pure gaseous hydrogen environment under a pressure of 10 MPa, the change in strength and ductile characteristics does not exceed 13 % in comparison with reference tests in nitrogen environment under the same pressure. The results obtained allow us to consider that the base metal of low-alloy pipe steel with ferrite-perlite microstructure of X52 strength class is sufficiently resistant to hydrogen embrittlement. Final confirmation of the possibility to use LDP made from steel under study will be the results of further qualification tests, including the study of the weld metal and heat-affected zone properties.

Shared mechanism between flow drill screw and friction stir welding and its impact on failure prediction of steel-aluminum joints

Severe plastic deformation and heat generation during the flow drill screw (FDS) process led to profound changes in the microstructures and mechanical properties of the heat-affected zone (HAZ). Microhardness measurements, electron backscattered diffraction (EBSD), and forming process simulation results showed that the HAZ was located within 1.0 mm from the thread tip. According to the simulated results of the joint forming process, the HAZ was divided into four subzones. The challenge in the numerical simulation of FDS joints lied in how to accurately acquire the mechanical properties of HAZ with limited size. In the present study, large-sized equivalent specimens were prepared with the friction stir welding (FSW) process. Based on the mechanical testing results of the equivalent specimens, a three-dimensional numerical model was established. Simulation results revealed that considering the material softening of HAZ was crucial for accurately predicting the mechanical behaviour of the joints under the tensile loading condition. The prediction accuracy of the peak force and failure displacement was improved by 7.0% as compared with that obtained using the numerical model without considering the material softening of HAZ. Under shear and mixed loading conditions, the error difference of predicted peak force and failure displacement with the two models was less than 3.0%. The deformation and failure characteristics of the joints could be accurately predicted by both the models.

Precipitation mechanism of nanoscale Cu-rich particles in restrained welding conditions and its effect on the mechanical properties of HAZs

The effect of welding constraint on nanoscale Cu-rich precipitation in welding heat affected zones (HAZs) of Cu-bearing steel was studied in this work. Due to the constraint tensile stress of 150 MPa, α-Fe transformation start temperature (Ts) of CGHAZ and FGHAZ increased by 55 °C and 42 °C, respectively. The volume fraction and average size of 9R-structural Cu-rich particles in FGHAZ increased from 0.3 % to 0.8 % and from 5 nm to 8 nm, respectively. Three-dimensional phase field simulation shows that the increment of Ts promoted the precipitation of Cu-rich particles in α-Fe matrix. However, the Ts of restrained CGHAZ was too low to favor the precipitation of Cu-rich particles. The tensile strength of FGHAZ increased from 970 MPa to 1032 MPa due to the nanoscale Cu-rich precipitation strengthening.

Creep life estimation of a service‐exposed P91 cross‐weld joint based on a primary‐secondary creep deformation model

AbstractCreep deformation and rupture behavior of welded joints from service‐exposed P91 steel were investigated by creep tests and microstructure examination. A series of miniature tensile creep tests were conducted at 569°C under applied stresses ranging from 182.5 to 286 MPa for the heat‐affected zone (HAZ), base metal, and weld metal. Creep deformation behavior was modeled using the experimentally measured creep strain data as the primary creep‐secondary creep (PC‐SC) model and fitting closely with the measured creep curves of each metal. Power‐law type creep equations were employed to describe the primary and secondary creep behavior. The creep rupture life of the cross‐weld specimen was predicted using the PC‐SC model with HAZ properties. An accurate prediction was possible if the stress in estimation was increased to 1.14 times of the actual applied stress. The creep test results with the cross‐weld specimens were used for verification. Applying the Monkman–Grant relationship and the creep damage tolerance factors to the cross‐weld joint life prediction are also discussed.

Characterization of Crack Tip Mechanical Field of Inhomogeneous Materials in Welded Joints by USDFLD Subroutine

The unevenly distributed mechanical properties of welded joints are one of the important factors, which affect welded joints’ safety seriously. The user-defined field (USDFLD) subroutine in ABAQUS finite element software can introduce variable-dependent material properties. This method can define inhomogeneous materials whose mechanical parameters depend on spatial coordinates and can be used to characterize the uneven mechanical properties of heat-affected zone and fusion zone. By establishing the static crack finite element model of welded joint with continuous change in yield strength, the sudden change in mechanical field in the numerical simulation process of sandwich structure model is eliminated. Compared with the existing numerical simulation methods of local mechanical heterogeneity of welded joints, this method provides a method to realize the structural integrity evaluation of welded joints.

Critical assessment 42: acicular ferrite formation and its influence on weld metal and heat-affected zone properties of steels

Toughness and fatigue resistance of welds and associated heat-affected zones (HAZs) in high-strength steels are important design parameters in structural applications. Acicular ferrite microstructures, which can be achieved through control of weld process and nucleant (inclusions or precipitates) characteristics, are often regarded as key to enhancing weld metal and HAZ properties of welded steels. This paper addresses the transformation characteristics of acicular ferrite related to alloying and weld processing as well as the specific role of acicular ferrite in weld performance, along with future research needs to identify weld processes suitable to specific alloying strategies.

Effect of alloy element on microstructure and properties of heat-affected zone

In the present study, the influences of general composition (GC steel), magnesium deoxidation treatment (MT steel) and magnesium deoxidation treatment with high vanadium (MVT steel) content on the inclusions, microstructure and low-temperature toughness of the welding heat affected zone of EH36 steel were studied. The thermal cycle process of the heat-affected zone (HAZ) was simulated by a thermal simulator, and then microstructure and impact properties were tested and analyzed. Obtained results show that Magnesium deoxidation treatment and magnesium deoxidation treatment with higher vanadium content decrease the number and average size of inclusions. Compared with GC steel, the austenite grain size of MT and MVT steel reduces at high temperatures so that the nucleation temperature of acicular ferrite in HAZ microstructure increases. Compared with GC steel, the low-temperature impact toughness of HAZ by MT steel and MVT steel increases.

Effect of Repeated Weld Repairs on Microstructure and Mechanical Properties of Heat-Affected Zone in CA6NM Stainless Steel

The low-carbon martensitic stainless steel CA6NM is widely used in the impellers of hydroelectric and nuclear power units due to its advantages of high hardness, corrosion fatigue strength, and good fracture toughness. In order to analyze the number of repair welding times on the properties of heat-affected zone (HAZ, the most unstable area of welded joint property) in CA6NM, the microstructure and mechanical properties of HAZ with once-repaired welds (1R) and twice-repaired welds (2R) were tested. Through data analysis, the following conclusions are drawn for welded joints: (1) the grain size of HAZ with a different number of repair welding processes is smaller than that of the base material; (2) the density of texture concentration is reduced and the directionality is not obvious; (3) the density of twins and dislocations are increased; (4) the hardness and impact energy of HAZ of the 1R and 2R specimens are higher than that of the base material.