Physical Methods Research Articles

Anti-corrosive properties of vermiculite-enhanced waterborne epoxy resins with two-dimensional exfoliation

Abstract Although waterborne epoxy resin coatings are widely used in the field of anti-corrosion, micropores and micro defects in their coatings are the key factors restricting their further development. The exfoliated vermiculite was stripped by a physical one-step stripping method, with good water dispersion and dense lamellar structure. As the nano-filler, it can effectively fill the micro defects in the coating, make the coating structure more compact, and effectively prevent the intrusion of corrosive media. When exfoliated vermiculite was added at 1%, two orders of magnitude increased the electrochemical impedance modulus to 2.276×106 Ω cm2 and the corrosion current was correspondingly reduced to 1.186×10−8 A cm−2, showing excellent corrosion resistance. Adding 1% exfoliated vermiculite creates a “labyrinth effect” in the coating that extends the penetration path of the corrosion particles, thus effectively preventing corrosion of the underlying metal substrate. This enables the coating to better cope with harsh corrosive environments and provides a viable idea for coating protection.

Research on electron beam irradiation in the multiscale structure of starch and its related applications: A review.

Electron beam irradiation (EBI), as a typical "green" emerging technology, can effectively alter the functional properties of starch by influencing its microstructure. This alteration enables starch to meet the current demands of consumers and the market for "health food." This paper reviews studies on modifying various starches using EBI and describes the changes in microstructure, physicochemical properties, and functional properties induced by this method. Additionally, the effects of EBI on starch-containing food products are discussed, along with issues to be addressed and research gaps in the synergistic treatment of modified starch. It is noted that the source, irradiation dose, and irradiation time all influence the effectiveness of starch modification. Given the characteristics of EBI technology, integrating physical, chemical, and biological modification methods can optimize the modification process and enhance efficiency. This technology can potentially diversify modified starch varieties and expand their applications. Furthermore, there remains significant research potential in producing modified starch using EBI technology and applying it to the food industry.

Research and design of low-noise cooling fan for fuel cell vehicle

Abstract The main noise source of fuel cell vehicles comes from the cooling vehicle, which has the characteristics of high voltage and large air volume. However, the large air volume makes the fan noise level significantly increase, reaching about 70dB. Even if the car adopts a variety of physical noise reduction methods, the noise level inside the car is still high, seriously affecting the passenger ride experience. In recent years, related research combined with bionic technology to improve the fan blade by designing a new shape structure, so that it has similar characteristics to some organisms to achieve the purpose of noise reduction. In this paper, ANSYS-CFX software is used to simulate the fan efficiency and noise level under different blade numbers, predict its performance, and optimize its structure.

Silkworm cocoon bionic design in wound dressings: A novel hydrogel with self-healing and antimicrobial properties

Hydrogels with rapid wound-healing capabilities and antimicrobial effects are gaining significant interest in related fields. Nonetheless, developing a multifunctional hydrogel wound dressing with injectable self-assembling, self-healing, antimicrobial properties, and efficient skin wound-healing capabilities remained a formidable challenge. In this experiment, we drew inspiration from silkworm cocoons' natural formation and protective mechanisms, employing a novel physical cross-linking method to create an injectable and self-healing quaternary hydrogel successfully. The hydrogel is based on a matrix of silk fibroin/silk sericin (SF/SS), with 1,2-dimyristoyl-sn-glycero-3-phosphate sodium salt (DMPG) serving as a physical cross-linking agent to form the hydrogel network structure, and the incorporation of silver nanoparticles (AgNPs) further enhances its antimicrobial capabilities. Our biomimetic hydrogel, which replicated the chemical properties of silkworm cocoons, demonstrated excellent hydrophilicity with a water contact angle that ranged from 37 to 52°. Its tensile and compressive resistance was approximately four times greater than that of a pure SF hydrogel, and its swelling performance was about three times higher than that of a pure SF hydrogel. Furthermore, the hydrogel exhibited an impressive bacterial inhibition rate of over 98 % in bacterial growth and inhibition experiments, which provided a solid foundation for accelerating wound healing. Likewise, experiments with mice and histological analyses revealed that on day 7, the expression of TNF-α and IL-1β in the wound tissues treated with the SF/SS/AgNPs hydrogel was significantly reduced by >25 % compared to the blank control group. This reduction indicates that the hydrogel could decrease the production of inflammatory cytokines, potentially aiding in the acceleration of wound healing and mitigation of inflammation-related adverse reactions. By day 14, the wounds were healed mainly, with the wound area reduced by 17 % compared to that of the blank group. This demonstrates the significant potential of this cocoon-mimetic hydrogel in accelerating wound healing and providing wound protection.

Temporal Dynamics and Physical Priori Multimodal Network for Rehabilitation Physical Training Evaluation.

Sensor-based rehabilitation physical training assessment methods have attracted significant attention in refined evaluation scenarios. A refined rehabilitation evaluation method combines the expertise of clinicians with advanced sensor-based technology to capture and analyze subtle movement variations often unobserved by traditional subjective methods. Current approaches center on either body postures or muscle strength, which lack more sophisticated analysis features of muscle activation and coordination, thereby hindering analysis efficacy in deep rehabilitation feature exploration. To address this issue, we present a multimodal network algorithm that integrates surface electromyography (sEMG) and stress distribution signals. The algorithm considers the physical knowledge a priori to interpret the current rehabilitation stage and efficiently handles temporal dynamics arising from diverse user profiles in an online setting. Besides, we verified the performance of this model using a learned-nonuse phenomenon assessment task in 24 subjects, achieving an accuracy of 94.7%. Our results surpass those of conventional feature-based, distance-based, and ensemble baseline models, highlighting the advantages of incorporating multimodal information rather than relying solely on unimodal data. Moreover, the proposed model presents a network design solution for rehabilitation physical training that requires deep bioinformatic features and can potentially assist real-time and home-based physical training work.

The Effect of Cigarettes Smoke on the Color and Properties of a Silicone for Maxillofacial Prostheses.

Although deterioration of silicone maxillofacial prostheses is severely accentuated in smoking patients, the phenomenon has not been systematically studied. To address a gap in the literature concerning the stability of maxillofacial prostheses during service, in this contribution, the effect of cigarette smoke on the aspect and physical properties of M511 silicone elastomer was evaluated. The aspect, surface, and overall properties of the silicone material, pigmented or not, were followed by AFM, color measurements, FTIR, water contact angle measurements, TGA-DTG and DSC, hardness and compression stress-strain measurements. The types of the contaminants adsorbed were assessed by XRF, ESI-MS, MALDI-MS, and NMR spectral analyses. Important modifications in color, contact angle, surface roughness, local mechanical properties, and thermal properties were found in the silicone material for maxillofacial prostheses after exposure to cigarettes smoke. The presence of lead, nicotine, and several other organic compounds adsorbed into the silicone material was emphasized. Slight decrease in hardness and increase in Young's modulus was found. The combined data show important impact of cigarette smoke on the silicone physical properties and could indicate chemical transformations by secondary cross-linking. To our knowledge, this is the first study making use of complementary physical methods to assess the effect of cigarette smoke on the aspect and integrity of silicone materials for maxillofacial prostheses.

Microfluidic Device with an Oxygen Gradient Generator for Investigating Effects of Specific Hypoxia Conditions on Responses of Tumor Cells.

The oxygen level in the tumor microenvironment (TME) plays a critical role in regulating cell fates such as proliferation, migration, apoptosis, and so forth. To better elucidate how hypoxia affects tumor cell behaviors, a series of microfluidic strategies have been utilized to generate an oxygen gradient covering both hypoxia and normoxia conditions. However, in most studies, some chemicals are introduced into microfluidic chips, causing the potential of their poor biocompatibility. The common oxygen gradient with linear variation does not allow the effects of specific oxygen concentrations on tumor cells to be analyzed accurately. In this paper, based on the physical method of gas diffusion, a microfluidic device integrated with an oxygen gradient generator is proposed for investigating effects of different hypoxia levels on responses of tumor cells. This device consists of three layers, i.e., upper layer, thin film layer, and bottom layer. The upper layer is used for introducing the initial gas and generating an oxygen gradient in the form of gas. The bottom layer is used for introducing cells and culture medium. The thin film layer separates the former two layers, allowing the gas to diffuse from the top to the bottom through it. The oxygen gradient in the bottom layer is finally generated in the form of dissolved oxygen. The device is fabricated using microfabrication technology. The effects of structural and working parameters of the device on the oxygen gradient are evaluated by finite element simulation. The oxygen gradient in cell culture channels is characterized by using oxygen-sensitive fluorescence materials. The proliferation and morphology of HeLa cells under specific oxygen levels are compared after culturing for 48 h. The oxygen gradient with a ladder-like distribution demonstrates that this microfluidic device can provide a prospective experimental platform for in vitro cell studies and revelation of the mechanism of tumor metastasis associated with a specific hypoxic microenvironment.

Recent advancement in microplastic removal process from wastewater - A critical review

Microplastics, small sized plastic particles having size <5 mm are formed through primary process including production of beauty products, microbeads and microfibres as well as secondary process including mechanical weathering, friction, aberration and fragmentation of large plastics. The major sources of microplastics are land-based and ocean-based sources. Microplastic pollution is a serious concern due to the persistent, low biodegradability and bio-accumulative behaviour. Microplastics can bioaccumulate in the food chain and can cause ecological and human health risk. Hence, it is important to remove from the aquatic ecosystems. Microplastics are removed from aquatic systems and wastewater through a series of processes such as physical, chemical and biological treatments. In the present articles, >250 articles are reviewed to collect the information regarding the various physical, chemical and biological methods for the removal of microplastics. Also, the probable control strategies to combat with plastic pollution were assessed. It was concluded that recent water treatment methods are efficient in removing microplastic pollution. The efficiencies to remove microplastic from the water ranged between 74 %-99.2 %, 65 %-99.20 % and 77 %-100 % for physical, chemical and biological treatment methods, respectively. Among the three treatment methods, physical methods especially the filtration of water from biochar is the most efficient way (efficiency up to 100 %) to remove microplastics. It was also concluded that creating public awareness, promoting reusing, recycling and reducing, and application of bioplastics can control the production of microplastics from plastic wastes. This review will be useful to add current knowledge regarding the abatement of microplastic pollution, and finding novel solution to control microplastics. This review will also help the policymakers to implement most effective and cost-efficient method to remove microplastics, and to find out new methods to reduce, reuse and recycle plastic wastes.

A review of physical heat dissipation methods for 3D integrated technology

Three-dimensional integrated circuits have higher integration than two-dimensional integrated circuits, and can obtain higher performance and lower power consumption in a certain space. In order to fulfill higher efficiency, thermal management becomes particularly important in 3D integration technology. However, the traditional heat dissipation method cannot satisfy the heat dissipation needs of three-dimensional integrated circuits, which require better heat dissipation methods to be developed. This paper introduces the realization of three-dimensional integrated circuit using silicon via (TSV) technology, which allows the chip to be vertically stacked to transmit information. This paper summarizes the research methods and findings of three-dimensional integrated circuit heat dissipation in recent years, including thermal through silicon via (TTSV) and microchannel cooling. It also emphasizes the advantages and disadvantages of both mehods, and the challenges faced in current research via an overview. The future research trend for both heat dissipation methods mainly consists of combining special algorithms to achieve thermal-electrical codesign and thermal management of three-dimensional integrated circuits.

Physical constraint flow field reconstruction method for immersion scan-step flow

The lithography immersion flow field is highly sensitive to minor variations due to the precision demands of lithography. The scanning flow induces pressure fluctuations on the lens surface, subsequently impacting the quality of exposure. Previous measurement methods have encountered sparse distribution measurements on the lens surface due to limitations in sensor size and flow field dimensions. In this manuscript, the authors propose a modal fusion flow field reconstruction method, effectively integrating sensor-based experimental methods and equation-based computational methods. This method achieves high-resolution measurements of stress distribution and velocity distribution. Initially, a simulation of the flow field under operational conditions is conducted to acquire a dataset, followed by decomposing the dataset into modes to establish a modal library. Throughout the measurement process, the modal library is dynamically restructured based on sensor signal using a sparse representation method to forecast the flow field, and subsequently, the flow field is corrected in accordance with the Navier-Stokes equation.

Room temperature storage of myrtle (Eugenia gracillima Kiaersk.) tropical juice: Effects of physical and chemical preservation methods

Tropical fruit juices produced from native fruits have been widely marketed by small agribusinesses in the Brazilian semiarid region, necessitating a deeper understanding of the impact of preservation methods on quality parameters. This study aimed to prepare myrtle (Eugenia gracillima Kiaersk.) tropical juice and investigate the effects of physical preservation (90 °C for 60 s) and chemical preservation (potassium sorbate and sodium benzoate) methods. Tropical juice formulations were evaluated after preparation and every 15 days during 60 days of storage in high-density polyethylene bottles at room temperature (25 ± 2 °C). Microbiological parameters, optical microscopy, physicochemical and bioactive parameters, antioxidant capacity, and color parameters were determined. Heat-treated tropical juice showed low counts of all microbiological parameters, but optical microscopy revealed the presence of filamentous fungi after 60 days of storage. Combined use of potassium sorbate and sodium benzoate effectively prevented the development of total yeasts and molds up to 28 days of storage. Bioactive compounds in myrtle pulp contribute to storage stability, mainly total phenolics, estimated at 855.86 mg gallic acid equivalents 100 g−1. The results suggest that it is possible to harness the economic and agroindustrial potential of E. gracillima Kiaersk. fruits for the production of tropical juices, but it is recommended that other technologies be explored, such as aseptic processing or the combined use of physical and chemical methods.

Biogenic Zinc Oxide Nanoparticles as a Promising Antibacterial Agent: Synthesis and Characterization.

Nanotechnology has gained popularity in recent years due to its wide-ranging applications within the scientific community. The three main methods for synthesizing nanoparticles are physical, chemical, and biological. However, the adverse effects associated with physical and chemical methods have led to a growing interest in biological methods. Interestingly, green synthesis using plants has gained prominence in developing new treatments for bacterial infections. Zinc oxide nanoparticles (ZnO NPs) produced using environmentally friendly methods are more biocompatible and have potential applications as antibacterial agents in the biomedical field. As a result, this review discusses the green synthesis of ZnO NPs, factors influencing optimal synthesis, characterization techniques, and the antibacterial activity of some plant-mediated ZnO NPs. It also provides a comprehensive and analytical exploration of ZnO NP biosynthesis, the role of phytochemical compounds as reducing and stabilizing agents, the mechanism of action of their antibacterial properties and further highlights the challenges and prospects in this innovative research area.

디지털 콘텐츠 유통을 위한 OTT 비즈니스 모델 연구

The way cultural content is being distributed is rapidly changing in the digital age. This study focuses on the business model of Netflix, a dominant player in the global market for digital content distribution. The aim is to identify strategies and insights that can be useful for domestic OTT (Over-The-Top) companies seeking to distribute Korean content worldwide. Netflix is a global OTT company that provides a diverse range of content to consumers, including original productions. The STOF (Service, Technology, Organization, Finance) model is used to analyze Netflix's business model, which is suitable for Internet-based businesses. The study highlights the shift from traditional and physical methods of producing and distributing content, such as movies using the existing film method, to completely digital methods in the field of cultural content. The study is valuable for global and domestic OTT operators and policymakers, scholars, entertainment and media companies, and the general public who enjoy cultural content.

PPLICATION OF KINEMATIC APPROACHES IN GEOMETRIC PROBLEMS

This work is devoted to the use of kinematic methods in the process of solving geometric problems. The first part of the work is devoted to solving geometric problems by considering the movements of some image points. The minimum knowledge required to apply the kinematic method in elementary geometry is briefly outlined. Then a solution to a generalized version of a well-known geometric problem is presented. The importance of studying elements of operator calculus from an interdisciplinary perspective is also presented. The next part of the article examines problems selected according to the principle of gradual complication, from high school to bachelor’s degree. In these problems, the radius of curvature at various points is determined by kinematic way. Using the result of solving a kinematic problem about a body thrown in a horizontal direction, the expression for the radius of curvature of a parabola is determined. One physical method for determining the radius of curvature of a cycloid is presented. The problem of motion, which generates the equations of an ellipse and a hyperbola, is considered, and a kinematic version of determining the radii of curvature at the points of intersection of these curves and axes of symmetry is presented. The main methodological novelty of the work lies in the development, generalization and systematic presentation of kinematic problems that bring geometric results. Some methodological guidelines and arguments are also given to substantiate the importance of the discussed kinematic approaches to solving geometric problems.

Dislocation proliferation at the growth crystal/seed interface of physical vapor transport-grown 4H-SiC crystals

4H-SiC single crystal with [000 1¯ ] direction 4° off axis was prepared by physical vapor transfer method. To enlarge the observed interface area between the seed crystal and the nascent crystal, the wafers were processed at an Angle of approximately 2° in the (000 1¯ ) plane. The longitudinal optical phonon-plasmon coupled (LOPC) mode was measured by a laser Raman spectrometer, and the location of the growth interface was determined by evaluating the free carrier concentration at the seed-crystal interface. The defect structure at the seed-crystal/newly grown crystal interface and in nearby regions was examined by high-resolution x-ray diffractometry. The change in stress at the interface was characterized by a stress tester; the results showed that a greater stress at the interface correlated to more proliferated dislocations. The dislocation morphologies in the interfacial regions of different seed grains etched by molten KOH were observed via microscopy.

Green Synthesis of Iron Nanoparticles Using Spinacia oleracea and Their Role in Antioxidant Defence

The green synthesis of iron oxide nanoparticles (Fe2O3) using Spinacia oleracea leaf extract is explored in this study. Iron oxide nanoparticles are noted for their unique properties, such as enhanced chemical reactivity due to their high specific surface area to volume ratios. Unlike traditional physical and chemical methods, green synthesis presents an environmental friendly alternative, leveraging biological processes for nanoparticle production. This method is particularly significant due to its potential applications in various fields, including medicine, where iron nanoparticles demonstrate antibacterial activity. However, limited research exists on their antioxidant properties. In this research, Spinacia oleracea leaf extract is utilized to synthesize iron oxide nanoparticles, followed by characterization using UV-Visible spectroscopy, FTIR, XRD, and SEM techniques. The results underscore the necessity for further investigation into the impact of nanoparticles on biological processes and the long-term effects of high nanoparticle concentrations on ecological stability. Additionally, this study includes an evaluation of antioxidant properties of the nanoparticles to address gaps in current research. Key Words Green synthesis, iron oxide, ecological stability, antioxidant, biological, nanoparticles.

In-Plane Cyclic Behaviour Comparison of Adobe Wall Retrofitted by Mortar Enhanced by Physical and Chemical Methods

ABSTRACT A mortar overlay on damaged adobe masonry is employed for its load carrying capacity improvement and low skill requirement. Nevertheless, delamination between the adobe wall and mortar has been commonly observed due to bonding failure. Physical enhancement (groove, shear dowel, and wire mesh) and chemical enhancement (a novel biological and traditional Chinese binder, sticky rice pulp, SRP) are carried out to enhance the bonding between mortar and adobe. The high-moisture adsorption mortar is also utilized to alleviate water accumulation resulting from the application of mortar on earthen buildings. Four adobe walls with different retrofitting methods are subjected to in-plane lateral cyclic loading tests to analyse the failure mode, hysteretic load-displacement response, skeleton curve, ductility behaviour, energy dissipation and stiffness degradation. It indicates that the retrofitting effectiveness of adobe walls coated only with mortars is limited, as their peak load increases are comparatively modest compared to other retrofit wall systems. However, employing additional bonding enhancement methods significantly enhances the peak load capacity. Specifically, a combination of physical and chemical enhancements results in a remarkable 114% increase on the positive side and an astonishing 500.1% increase on the negative side.

Multidimensional images and aberrations in STEM

Abstract Recent advances in scanning transmission electron microscopy (STEM) have led to increased development of multi-dimensional STEM imaging modalities and novel image reconstruction methods. This interest arises because the main electron lens in a modern transmission electron microscope usually has a diffraction-space information limit that is significantly better than the real-space resolution of the same lens. This state-of-affairs is sometimes shared by other scattering methods in modern physics and contributes to a broader excitement surrounding multidimensional techniques that scan a probe while recording diffraction-space images, such as ptychography and scanning nano-beam diffraction. However, the contrasting resolution in the two spaces raises the question as to what is limiting their effective performance. Here, we examine this paradox by considering the effects of aberrations in both image and diffraction planes, and likewise separate the contributions of pre- and post-sample aberrations. This consideration provides insight into aberration-measurement techniques and might also indicate improvements for super-resolution techniques.

Enhanced oil recovery in tight reservoirs by ultrasonic-assisted CO2 flooding: Experimental study and molecular dynamics simulation

CO2-enhanced oil recovery (CO2-EOR) has attracted great attention due to its dual effects of geological carbon storage and economic benefits, but the clay swelling, asphaltene deposition and gas channeling induced by CO2 still restrict its field application. The employment of chemical agents for the purpose of improving CO2-EOR performance is often limited by the heterogeneity of reservoirs and the potential for formation damage. Physical methods, such as ultrasonic-assisted CO2 flooding, appear to offer a promising alternative for CO2-EOR and geological sequestration. This study has conducted oil displacement experiments to investigate the EOR potential of ultrasonic-assisted CO2 flooding in tight reservoirs and clarify the effects of different ultrasound parameters. The ultrasonic waves with 20 kHz of acoustic frequency, 30 W/cm2 of sound intensity, 30 min of sonication time and moderate intermittent working mode can yield violent cavitation effects and avoid undesirable energy dissipation. Nearly a quarter of the saturated crude oil can be recovered from the tight core through ultrasonic-assisted CO2 flooding. It can be attributed to the composition alterations of crude oil and property changes of core matrix. Coupling with ultrasonic waves, CO2 would extract and vaporize crude oil more easily, which promotes oil swelling, lowers oil density and viscosity, decreases oil–gas interfacial tension and thus improves oil recovery. Besides, the ultrasound can help to mitigate the impact of CO2 adsorption-induced clay swelling on pore sizes through fluctuating pressure. And the strong hydrodynamic shear forces generated by mechanical vibration of ultrasound may also help to connect individual small pores and extend micro-fractures. These synergistic effects result in the transformation of micropores into mesopores and macropores. Furthermore, the wettability alteration of core samples implies that the ultrasonic-assisted CO2 flooding can induce the detachment of oil films from the rock surface. Finally, the results of molecular dynamics simulations indicate that the improvement in pressure inside the core sample resulting from ultrasonic cavitation facilitates the mixing of CO2 and oil, thereby weakening gas channeling and improving the displacement efficiency.

Disease burden and symptom management in type 2 diabetic patients: A phenomenological study.

This study was conducted to address the experiences of diabetic patients from a psychosocial perspective, examine the burden of disease, and determine their practices for symptom management. In this study, a phenomenological research design, a qualitative research design, was used. The study included 20 diabetic patients. Individual and face-to-face interviews were performed, and Colaizzi's phenomenological analysis method was used to analyze the data. As a result of the data analysis, four categories (challenges with care and treatment, coping with the disease, effects, and healthy life behaviors) and eleven main themes (knowledge, application, symptoms, support resources, spiritual coping methods, physical coping methods, physical effects, spiritual effects, social effects, physical practices, and psychological practices) emerged. It was concluded that the disease burden of diabetic patients is intense and that the participants of the study were not effective in coping with the disease through symptom management and found spirituality important in coping.