Optical Gratings Research Articles

Nanofabrication and profile tailoring of high index Ta2O5 optical gratings for LiDAR using C4F8/SF6 plasma mixtures

Optical elements, such as dielectric meta-surfaces, photonic crystals, nanophotonic waveguide circuits, and diffractive grating couplers are all based on high refractive index materials. In this respect, a highly versatile material is tantalum pentoxide, which features a refractive index above 2 and low loss over a broad range of wavelengths from ultraviolet to near-infrared. However, the engineering of e.g. optical relief gratings requires tight control of the relief profiles to tailor the diffraction efficiency for the specified diffraction angles and polarizations. The current work presents a fabrication process offering high etch rate and uniformity across a 150 mm wafer, providing a tailored profile by means of gas flow control of etch- and passivation species during the inductively coupled plasma etching of tantalum pentoxide. The fabricated structures show good agreement between simulated and measured diffraction efficiency. Our findings enable highly efficient Ta2O5 platforms featuring over 85% diffraction efficiency for both transverse electric (TE) and transverse magnetic (TM) polarizations at a center wavelength of 808 nm, which is relevant for medium-range light detection and ranging (LiDAR) systems. It is observed that to achieve polarization-independent, high diffraction efficiency solutions it is necessary to tune the sidewall angle of the obtained structures, potentially boosting the efficiency of Ta2O5-based solutions. The findings constitute a scalable and flexible method for processing and designing meta- and diffractive optics for various trending applications requiring high diffraction efficiency such as LiDAR and augmented/virtual reality (AR/VR) modules.

Spatiotemporal observation of surface plasmon polariton mediated ultrafast demagnetization

Surface plasmons offer a promising avenue in the pursuit of swift and localized manipulation of magnetism for advanced magnetic storage and information processing technology. However, observing and understanding spatiotemporal interactions between surface plasmons and spins remains challenging, hindering optimal optical control of magnetism. Here, we demonstrate the spatiotemporal observation of patterned ultrafast demagnetization dynamics in permalloy mediated by propagating surface plasmon polaritons with sub-picosecond time- and sub-μm spatial- scales by employing Lorentz ultrafast electron microscopy combined with excitation through transient optical gratings. We discover correlated spatial distributions of demagnetization amplitude and surface plasmon polariton intensity, the latter characterized by photo-induced near-field electron microscopy. Furthermore, by comparing the results with patterned ultrafast demagnetization dynamics without surface plasmon polariton interaction, we show that the demagnetization is not only enhanced but also exhibits a spatiotemporal modulation near a spatial discontinuity (plasmonic hot spot). Our findings shed light on the intricate interplay between surface plasmons and spins, offer insights into the optimized control of optical excitation of magnetic materials and push the boundaries of ultrafast manipulation of magnetism.

Optical fibre long-period grating sensors modified with antifouling bio-functional nano-brushes.

Recent advances in optical sensing technologies underpin the development of high-performance, surface-sensitive analytical tools capable of reliable and precise detection of molecular targets in complex biological media in non-laboratory settings. Optical fibre sensors guide light to and from a region of interest, enabling sensitive measurements of localized environments. This positions optical fibre sensors as a highly promising technology for a wide range of biochemical and healthcare applications. However, their performance in real-world biological media is often limited by the absence of robust post-modification strategies that provide both high biorecognition and antifouling capabilities. In this study, we present the proof-of-concept antifouling and biorecognition performance of a polymer brush nano-coating synthesized at the sensing region of optical fibre long-period grating (LPG) sensors. Using a newly developed antifouling terpolymer brush (ATB) composed of carboxybetaine methacrylamide, sulfobetaine methacrylamide, and N-(2-hydroxypropyl)methacrylamide, we achieve state-of-the-art antifouling properties. The successful on-fibre ATB synthesis is confirmed through scanning electron microscopy (SEM), fluorescence microscopy, and label-free bio-detection experiments based on antibody-functionalized ATB-coated LPG optical fibres. Despite the challenges in handling optical fibres during polymerization, the resulting nano-coating retains its remarkable antifouling properties upon exposure to blood plasma and enables biorecognition element functionalization. These capabilities are demonstrated through the detection of IgG in buffer and diluted blood plasma using anti-IgG-functionalized ATB-coated sensing regions of LPG fibres in both label-based (fluorescence) and label-free real-time detection experiments. The results show the potential of ATB-coated LPG fibres for use in analytical biosensing applications.

Quantum weak measurement enhanced distributed acoustic sensing.

An enhanced distributed acoustic sensing (DAS) is proposed based on an extended Mach-Zehnder interferometer utilizing quantum weak measurement. The acoustic signals are encoded as the relative phase of the polarized light in several channels by fibers between optical fiber Bragg gratings (FBGs). With appropriate preselection and postselection, the acoustic signal can be extracted by performing the Fourier transform on the contrast ratio of the detected light intensity. Theoretical analysis shows that the scheme can achieve a spatial resolution of 1 m, and the system noise can be decreased by three orders of magnitude compared to classical distributed acoustic sensing. Moreover, this scheme might have potential application in long-distance acoustic source localization.

Detection of matrix cracks in composite laminates using embedded fiber-optic distributed strain sensing

We used an optical frequency-domain reflectometry fiber Bragg grating (FBG) distributed strain measurement system to detect matrix cracks in carbon fiber-reinforced plastics. Load/unload tests were performed on cross-ply laminates under ambient-, high-, and low-temperature conditions using embedded 100 mm gauge FBG sensors. We measured the strain distributed along the gauge and examined the crack initiation using optical microscopy and soft X-ray inspection. A peak appeared in the distributed strain corresponding to the occurrence of cracks. The strain distribution during crack initiation was calculated in each temperature range via finite element analysis and compared with the measurement results. We determined that the number and location of cracks can be determined by extracting the peaks from the distributed strain. However, the peaks in the distributed strain do not correspond to the occurrence of cracks that are close to each other, warranting a measurement method with a higher strain resolution.

Real-time optical fibre near-infrared chromatic dispersion analyser using collocated optical fibre gratings.

We present what we believe to be a novel optical fibre device for real-time measurements of near-infrared chromatic dispersion of a liquid medium from 1100 nm to 1700 nm. This inline optical fibre chromatic dispersion analyser is based upon collocated fibre long-period gratings written adjacently in the core by femtosecond laser inscription yielding 8 attenuation bands associated with different cladding modes, yielding 8 independent measurements. This fibre device is tested on a series of chemical compounds associated with wines. The results for each compound yielded distinctive chromatic responses. A machine learning pipeline was developed that successfully clustered and classified spectral responses of the different chemicals to illustrate the distinctive responses. The limits of detection for these fibre devices ranged from 1×10-3 to 6×10-5 mol/L for the compounds associated with wines, demonstrating the potential usefulness of an optical fibre chromatic dispersion analyser is capable of monitoring in real-time effective chromatic dispersion that is not offered by any current technology.

Methods of active friction control in the presence of lubricant compositions with mesogenic additives

Purpose of research. The aim of the study is to systematize the latest literature data related to the modulation of the friction coefficient by external fields when using lubricant compositions with liquid crystal mesogens and polymer composites.Methods. The article considers the methods of tribological tests using various schemes of friction pairs (cylinder-disk, pin-on-disk). Some commonly used methods of applying coatings to the elements of friction pairs are considered: ion beam-assisted deposition, chemical and physical thermal spraying, molecular layer deposition, photopolymerization, etc. Of the discussed methods of characterizing tribosystems, the following are indicated: dielectric spectroscopy, Raman scattering, polarization optical microscopy, nuclear-physical methods (positron annihilation spectroscopy and Xray diffraction).Results. The article systematizes modern trends in the development of modulated modes of operation of tribological circuits with lubricant compositions containing liquid crystals and polymer composites. The following approaches are used to implement active control of the friction coefficient: 1) modulation of friction by an electric field, 2) modulation of friction by a temperature field, and 3) modulation of friction on optical gratings under light irradiation. These approaches take into account the changed characteristics of the lubricant associated with the use of mesogenic additives, modes of exposure to electromagnetic and thermal fields, electrical characteristics, geometry of the surface of friction pairs, and provide the values of tribological characteristics (friction coefficient and wear) that are achieved as a result of friction modulation.Conclusion. A positive effect of mesogenic additives of liquid crystals and polymers on tribological characteristics with active control of the friction coefficient has been established: a decrease in the friction coefficient is observed, which helps to reduce material wear.

Polycrystalline methylammonium-lead bromide perovskite films for photonic metasurfaces

Polycrystalline films of organo-inorganic perovskite semiconductors are promising as a foundation for creating functional optical metasurfaces. The requirements for film structural perfection, thickness uniformity, and defect-free characteristics are much more stringent compared to perovskite films for photovoltaics. This work presents the results of searching for optimal conditions for one-step synthesis of lead methylammonium bromide films using centrifugation, and describes the successful fabrication of subwavelength optical gratings from these films through focused ion beam processing. The measured spectra of light transmission through the gratings demonstrated their excellent optical quality and confirmed the possibility of creating semiconductor photon metasurfaces with submicrometer periodicity and high-Q dielectric resonances.

Optical Fiber Bragg Grating as a Strain Sensor

Abstract: The sensor technology industry has come to recognize and value the optical fibre sensor (OFS). It is frequently used to detect changes in the environment and to respond to outputs from other systems, such as those in industrial, monitoring, and chemical analysis applications. While a brief segment of optical fiber with a particular wavelength is reflected with light in a device known as a Fibre Bragg Grating, a Bragg reflector begins to grow and transmit all other wavelengths. Through software modeling, the current study focuses on the changing traits and behaviors of temperature and strain sensors that are used with fiber bragg gratings (FBG). The main objective of this work is to study the properties and behavior of strain sensors utilized in conjunction with fiber bragg gratings. A strain sensor can be used to determine the strain in an object whose resistance changes when force is applied

Optical Fiber Bragg Grating As A Temperature Sensor

The optical fibre sensor (OFS) has become quite well-known and prominent in the sensor technology industry. It is often used to react to outputs from other systems, like those in industrial, monitoring, and chemical analysis applications, and to detect changes in the environment. A Fibre Bragg Grating (FBG) is a device that allows light to be reflected from a short section of optical fiber at a specific wavelength, while the Bragg reflector expands and transmits all other wavelengths. The current effort focuses on the evolving characteristics and behaviors of strain and temperature sensors operating on fiber bragg gratings through computer modeling. The temperature sensor is employed to detect and quantify any variations in temperature on the Fiber Bragg Grating that could result in accidents or fires. This will show how the Fibre Bragg Grating may be used to showcase temperature sensors.

A simple method to prepare and characterize optical fork-shaped diffraction gratings for generation of orbital angular momentum beams

A simple method to prepare and characterize optical fork-shaped diffraction gratings for generation of orbital angular momentum beams

Sensor Systems for Measuring Force and Temperature with Fiber-Optic Bragg Gratings Embedded in Composite Materials

Currently, there is a lot of interest in smart sensors and integrated composite materials in various industries such as construction, aviation, automobile, medical, information technology, communication, and manufacturing. Here, a new conceptual design for a force and temperature sensor system is developed using fiber-optic Bragg grating sensors embedded within composite materials, and a mathematical model is proposed that allows one to estimate strain and temperature based on signals obtained from the optical Bragg gratings. This is important for understanding the behaviors of sensors under different conditions and for creating effective monitoring systems. Describing the strain gradient distribution, especially considering different materials with different Young’s modulus values, provides insight into how different materials respond to applied forces and temperature changes. The shape of the strain gradient distribution was obtained, which is a quadratic function with a maximum value of 1500 µ, with a maximum value at the center of the lattice and a symmetrically decreasing strain value with distance from the central part of the fiber Bragg grating. With the axial strain at the installation site of the Bragg grating sensor under applied force values ranging from 10 to 11 N, the change in strain was linear. As a result of theoretical research, it was found that the developed system with fiber-optic sensors based on Bragg gratings embedded in composite materials is resistant to external influences and temperature changes.

Refractive Index Determination and Air-Void Characterization of BNNT Assembly Using Optical Fiber Bragg Grating Sensors

Refractive Index Determination and Air-Void Characterization of BNNT Assembly Using Optical Fiber Bragg Grating Sensors

Talbot phenomenon in binary optical gratings under Gaussian illumination

Binary optical gratings are used in applications such as optical metrology. Due to the fact, that self-imaging phenomenon depends on the grating fill factor, in present work the effect of fill factor on Talbot image formation has been analyzed when the grating is illuminated with a Gaussian beam. A model based on Fresnel regime is used to determine the intensity distribution in the near field. Self-images are obtained under different initial beam conditions and it is found several regimes of the effect of Gaussian beam intensity distribution on the self-images are found: (I) decreasing intensity of grating slit at the beam border when Gaussian waist radius is 10 times greater than grating period, (II) transforming binary-like self-image to the cosine-like one in case when Gaussian waist radius ranges from 2 to 5 grating periods, and (III) disappearing regular grating structure when Gaussian waist radius is less than grating period. Additionally it is analyzed transform from Fresnel to Fraunhofer regime in case of Gaussian beam and effect of wavefront curvature radius value on the distance where different regimes appear.

One-step light-induced hierarchical surface wrinkles on photodegradable polymer films

Photodegradable polymers have become an emerging class of stimulus-sensitive materials for advanced applications, in which using the photolysis characteristic for patterning surface is a key but still a notable challenge. Herein, we report a simple, facile, green and high-efficiency strategy to induce and further tune surface wrinkling only relying on one-step ultraviolet (UV) irradiation of a photodegradable polymer-based film/substrate composite system. Interestingly, a series of intriguing wrinkling states from no wrinkling to surface wrinkling and final no wrinkling with UV exposure take place on the photodegradable polymer film. This wrinkling behavior is intimately related to the competition between the stress accumulation from the heating effect of UV lamp itself and the stress release from the UV-induced molecular chain breakage. Meanwhile, the dependence of photodegradable polymer film modulus and photodegradation-induced stress release on the exposure time has been characterized by taking advantage of surface wrinkling metrology, which is not easily accessible to other systems and methods. This one-step light irradiation strategy has enabled the fabrication of diverse hierarchical surface wrinkling on photodegradable polymer film by simply controlling the UV exposure time. As demonstrated, these hierarchical surface wrinkles with tunable features have been applied for optical information display/storage and optical gratings. Notably, this simple flexible light control strategy not only provides new insights into the photo-induced change in mechanical properties and stress release of photodegradable polymers in molecular level, but also paves new avenues for advanced wrinkle-based applications by incorporating desirable functional materials into the photodegradable polymer-based systems.

Portable Hadamard-Transform Raman Spectrometer: A Powerful Analytical Tool for Point-of-Care Testing.

A portable Hadamard-transform Raman spectrometer with excellent performance was fabricated consisting of a 785 nm laser, an optical filter, an optical system, a control system, and a signal processing system. As the core of the spectrometer, the optical system was composed of a slit, collimator, optical grating, reflector, digital micromirror devices (DMD), lens system, and InGaAs photodetector. Compared with a conventional dispersive Raman spectrometer, the proposed Raman spectrometer adopted the DMD and corresponding controlling device (DLPC350 control chip) to collect the Raman spectrum. Thus, in our design, the gratings are fixed, while the full Raman spectrum was collected by the deflection of the micromirror. This design can greatly improve the vibration resistance ability of the spectrometer since the gratings are not rotating during the spectrum collecting. More importantly, Hadamard-transform was used as signal processing technology, which has the ability of faster calculation, the merits of high energy input, single detector multichannel simultaneous detection (imaging) ability, and high signal-to-noise ratio (SNR). Hence, the Hadamard-transform portable Raman spectrometer has the potential to be applied in the field of point-of-care testing (POCT).

Streak artefact removal in x-ray dark-field computed tomography using a convolutional neural network.

Computed tomography (CT) relies on the attenuation of x-rays, and is, hence, of limited use for weakly attenuating organs of the body, such as the lung. X-ray dark-field (DF) imaging is a recently developed technology that utilizes x-ray optical gratings to enable small-angle scattering as an alternative contrast mechanism. The DF signal provides structural information about the micromorphology of an object, complementary to the conventional attenuation signal. A first human-scale x-ray DF CT has been developed by our group. Despite specialized processing algorithms, reconstructed images remain affected by streaking artifacts, which often hinder image interpretation. In recent years, convolutional neural networks have gained popularity in the field of CT reconstruction, amongst others for streak artefactremoval. Reducing streak artifacts is essential for the optimization of image quality in DF CT, and artefact free images are a prerequisite for potential future clinical application. The purpose of this paper is to demonstrate the feasibility of CNN post-processing for artefact reduction in x-ray DF CT and how multi-rotation scans can serve as a pathway for trainingdata. We employed a supervised deep-learning approach using a three-dimensional dual-frame UNet in order to remove streak artifacts. Required training data were obtained from the experimental x-ray DF CT prototype at our institute. Two different operating modes were used to generate input and corresponding ground truth data sets. Clinically relevant scans at dose-compatible radiation levels were used as input data, and extended scans with substantially fewer artifacts were used as ground truth data. The latter is neither dose-, nor time-compatible and, therefore, unfeasible for clinical imaging ofpatients. The trained CNN was able to greatly reduce streak artifacts in DF CT images. The network was tested against images with entirely different, previously unseen image characteristics. In all cases, CNN processing substantially increased the image quality, which was quantitatively confirmed by increased image quality metrics. Fine details are preserved during processing, despite the output images appearing smoother than the ground truthimages. Our results showcase the potential of a neural network to reduce streak artifacts in x-ray DF CT. The image quality is successfully enhanced in dose-compatible x-ray DF CT, which plays an essential role for the adoption of x-ray DF CT into modern clinicalradiology.

A piston and tilt wavefront sensor dedicated to the cophasing of segmented optics in low light level conditions

We present a new interferometer to measure piston, tip and tilt of segmented mirrors, using the combination of an optical grating and a microlens array. Since this interferometer is able to collect all the incident light and to operate with a large spectra bandwidth, it is particularly suitable to operate in low light level conditions, for example for the co-phasing of segmented primary mirrors like James Webb Space Telescope. We tested our new device on a 37-segment deformable mirror and obtained an accuracy better than λ/100. The measurement is self-referenced and errors can be estimated on the measurement itself thanks to closure relationships.

Fabrication of Quasi-Sinusoidal Surface Relief Optical Transmission Gratings in Pyrex and IOG Glasses by Implantation with Oxygen and Nitrogen Ion Microbeams of the 5-6 MeV Energy Range.

A method for the fabrication of high diffraction efficiency optical transmission gratings with quasi-sinusoidal profile in glasses by microbeams of medium-mass ions of 5-6 MeV energy was devised and demonstrated. Gratings with a 30 μm grating constant have been manufactured and characterized by interference microscopy and microprofilometry. The obtained surface profiles of the gratings were found to be quasi-sinusoidal with up to 265 nm amplitude. Measured highest first-order diffraction efficiencies were around 26% in both Pyrex and IOG glasses. Such gratings could serve as coupling elements in integrated optics and photonic integrated circuits.

Long-range dipole-dipole exchange-induced atomic grating.

We propose a theoretical scheme for dipole exchange-induced grating (DEIG) based on a hybrid coherent atomic system. The system consists of an ultra-cold rubidium (87Rb) atomic ensemble and movable Rydberg spin atoms. The optical response of the grating appears as a superposition of three- and four-level configurations, which is similar to the cooperative optical nonlinearity caused by the dipole blockade effect. The far-field diffraction properties of the cooperative optical nonlinear grating are tuned by the probe field (intensity and photon statistics). However, our Rydberg atomic grating uniquely responds to the spatial positions of spin atoms, which offers a novel approach to dynamically control electromagnetically induced gratings (EIG).