Reliable Test Method Research Articles

Transient Short Circuit-Based Degradation of Lithium and Sodium Anode-Free Batteries

The demand for an extended range of electric vehicles has created a renaissance of interest in replacing the common lithium-ion with a higher energy-density metal anode (e.g., Li or Na). However, alkali metal cells suffer from capacity fading and potential safety issues. The uneven metal electrodeposition often results in dendrite formation and potentially hazardous situations such as cell short-circuiting and thermal runaway.Though lithium plating has been studied widely, a better understanding of the short-circuiting mechanisms and metal battery failure is required. Moreover, a considerable performance gap exists between symmetric metal cells and realistic metal batteries."Soft shorts" are small localised electrical connections between two electrodes that allow the co-existence of direct electron transfer and interfacial reaction. Although soft shorts were identified as a major safety issue in the early nineties, their detection and prevention were not widely studied. Therefore, a fundamental understanding of passivated metals' plating and a reliable testing method for soft short circuits is critical for realising metal batteries, such as Li-Air, Li-S, and anode-free batteries.Here we compared short circuit formation mechanisms and degradation in symmetric cells and anode-free lithium and sodium batteries using coupled galvanostatic impedance spectroscopy (GEIS) and in-situ nuclear magnetic resonance spectroscopy (NMR) for the first time.The coupling of in-situ NMR and EIS allows the observation of metal batteries' electrochemical and chemical dynamics and degradation in real time without affecting the cells' operation.We demonstrated that lithium and sodium short circuit formation mechanisms fundamentally differ and strongly depend on electrolyte composition and SEI stability. This new understanding of the metal plating mechanism is crucial to develop the next generation of rechargeable batteries with high energy density, prolonged cycling life and improved sustainability.

Acute Toxicity Assays with Adult Coral Fragments: A Method for Standardization.

Coral reefs are globally declining due to various anthropogenic stressors. Amongst those, chemical pollutants, such as pesticides from agricultural runoff, sewage or an overabundance of personal care products in coastal waters due to intense tourism, may be considered as a local stressor for reef-building corals. The extent to which such chemicals exhibit toxic effects towards corals at environmentally relevant concentrations is currently controversially discussed and existing studies are often based on varying and sometimes deficient test methods. To address this uncertainty, we adapted available methods into a reliable and comprehensive acute coral toxicity test method for the reef-building coral Montipora digitata. The toxicities of the four substances benzophenone-3 (BP-3), Diuron (DCMU), copper (Cu2+ as CuCl2, positive control) and dimethylformamide (DMF, solvent) were assessed in a 96 h semi-static test design. Endpoints such as maximum quantum yield, bleaching, tissue loss and mortality were evaluated with respect to their suitability for regulatory purposes. Overall, the endpoints bleaching and mortality yielded sensitive and robust results for the four tested substances. As the test method follows the principles of internationally standardized testing methods (ISO, OECD), it can be considered suitable for further validation and standardization. Once validated, a standardized test method will help to obtain reproducible toxicity results useful for marine hazard and risk assessment and regulatory decision making.

Development of a Large-Scale Pathogen Screening Test for the Biosafety Evaluation of Canine Mesenchymal Stem Cells

BackgroundThe action of mesenchymal stem cells (MSCs) is the subject of intense research in the field of regenerative medicine, including their potential use in companion animals, such as dogs. To ensure the safety of canine MSC batches for their application in regenerative medicine, a quality control test must be conducted in accordance with Good Manufacturing Practices (GMP). Based on guidance provided by the European Medicines Agency, this study aimed to develop and validate a highly sensitive and robust, nucleic acid-based test panel for the detection of various canine pathogens. Analytical sensitivity, specificity, amplification efficiency, and linearity were evaluated to ensure robust assessment. Additionally, viable spike-in controls were used to control for optimal nucleic acid extraction. The conventional PCR-based and real-time PCR-based pathogen assays were evaluated in a real-life setting, by direct testing MSC batches.ResultsThe established nucleic acid-based assays displayed remarkable sensitivity, detecting 100–1 copies/reaction of template DNA. They also exhibited high specificity and efficiency. Moreover, highly effective nucleic acid isolation was confirmed by the sensitive detection of spike-in controls. The detection capacity of our optimized and validated methods was determined by direct pathogen testing of nine MSC batches that displayed unusual phenotypes, such as reduced cell division or other deviating characteristics. Among these MCS batches of uncertain purity, only one tested negative for all pathogens. The direct testing of these samples yielded positive results for important canine pathogens, including tick-borne disease-associated species and viral members of the canine infectious respiratory disease complex (CIRDC). Notably, samples positive for the etiological agents responsible for enteritis (CPV), leptospirosis (Leptospira interrogans), and neosporosis (Neospora caninum) were also identified. Furthermore, we conducted biosafety evaluation of 12 MSC batches intended for therapeutic application. Eleven MSC batches were found to be free of extraneous agents, and only one tested positive for a specific pathogen, namely, canine parvovirus.ConclusionIn this study, we established and validated reliable, highly sensitive, and accurate nucleic acid-based testing methods for a broad spectrum of canine pathogens.

Linking Farmers’ Bargaining Power in Trade to their Plans for Future Economic Activities

Abstract This paper aims to examine the relationship between the bargaining power of farmers in trade and their plans for future economic activity. While there is existing evidence shedding light on the factors influencing trading power and its consequences, there remains a compelling exigency for scientific substantiation clarifying the aforementioned nexus. A questionnaire was designed and utilized to collect primary data from farmers in Albania (with a sample size of 640). Factor analysis, reliability test and non-parametric statistical methods were used. Evidence was found in support of the aforesaid relationships. Hence, farmers who have plans for investments reflect a higher bargaining power in trading, as opposed to those without such plans. Moreover, interest in increasing farm activity is significantly associated with improved bargaining power in trade. This study enriches the literature, especially in the agribusiness field, by offering additional insights from a transition and developing country.

Successful Treatment-Free Remission in Low- and Middle-Income Countries

Introduction Discontinuation of tyrosine kinase inhibitors (TKIs) is feasible in a subset of chronic myeloid leukemia (CML) patients who have maintained a deep molecular response (MR) for ≥2 years. Numerous TKI discontinuation trials from high-income settings show that ~50% of patients relapse after discontinuing TKIs and need to restart treatment. However, most patients with CML worldwide are from low- and middle-income countries LMIC where TKI access and molecular testing make routine care and attempts of treatment-free remission (TFR) problematic. The successful implementation of TFR in LMICs would benefit both CML patients as well as the health economics of each country. This analysis describes the experience of attempting TKI discontinuation in the LMIC setting. Methods The Max Foundation's TFR Support Program provides financial and wrap-around support for patients attempting TFR in LMICs. The program operates in countries where The Max Foundation has existing partner institutions and physicians, imatinib and second line TKIs are available, and there is ≥1 reliable method of quantitative RT-PCR testing for BCR::ABL1. Eligible patients were >18 years old, diagnosed with chronic phase CML and treated with imatinib for ≥10 years with no history of resistance, and had a BCR-ABL level MR 4.5 or better (≤0.0032%) for ≥12 months (m) as demonstrated by 2 RT-PCR tests. Patients who consented were enrolled in the program and monitored by their treating physician. Upon starting TFR, patients' BCR::ABL1 levels were tested monthly for the first 6 m, then every 3 m for the following 6 m, then every 6 m. Patients who relapsed (BCR::ABL1 loss of MR 3 or >0.1%) after beginning TFR restarted imatinib and were tested approximately every 1-3 m until they achieved MR 3. We conducted a retrospective analysis on the outcomes of patients enrolled in The Max Foundation's TFR Support Program to better understand TFR outcomes in an LMIC setting. Results The molecular results pre- and post-TKI discontinuation are shown in Figure 1. In total, 39 patients from sites in 5 countries (Armenia, Honduras, India, Kenya, and Paraguay) were followed by 8 program physicians. The mean age of the patients was 51 years (range, 22-77), with 22 females and 17 males. Patients had been on imatinib for an average of 15 years (range, 10-20). At time of discontinuation, all but 1 patient was on 400 mg/day of imatinib (1 treated at 300 mg/day). Thirty-two patients had undetectable BCR::ABL1 for both pre-discontinuation tests, 6 had one test with a value of <0.01%, and 1 had both tests detectable at <0.01%. Of the 39 patients, 32 remain actively followed, with 14 patients completing >12 m of follow-up. Nine patients had a molecular relapse (23%) with a BCR::ABL1 >0.1% IS after a median of 2 m of discontinuation (range, 1-18 m). Of these, 2 patients have not had repeat testing to confirm molecular relapse, and 1 patient became undetectable on follow-up 1 m later. None of these 3 patients have restarted TKI therapy. Seven of 39 patients (18%) have restarted TKI treatment. Of these 7 patients, 3 were restarted on TKI, but have not had a follow-up BCR::ABL1 evaluation. Of the remaining 4 patients who restarted TKI, 2 had no detectable BCR::ABL1 at the 9 m and 12 m follow-up, and 2 remain with evidence of BCR::ABL1 at 12 m and 17 m follow-up. Conclusions The data suggest that under conditions that allow frequent follow-up examination and testing, patients attempting TFR in LMIC have similar outcomes to those patients described in controlled clinical trials from academic settings in high-income countries. Additional confirmation of these findings will likely impact both the health of CML patients and the health economics in these LMICs. Figure 1. BCR:ABL1 and outcomes following TKI discontinuation.

Biodegradation of plastics in the pelagic environment of the coastal zone – Proposed test method under controlled laboratory conditions

The increasing quantities of plastic litter accumulated in the oceans, including microplastics, represent a serious environmental threat. Despite the recent legislative actions, the plastic littering problem will not disappear in a short time. It may, however be ameliorated by replacing conventional non-degradable plastics with bio-based materials biodegradable in marine environment (targeting the non-recycled or mismanaged plastic waste). Although priority is set to prevention of plastic litter by means of the circular economy principles, biodegradability is a means of controlling unintentional plastic pollution. In this effort, the development of reliable test methods that would be used along with standard specifications for determining the biodegradability of novel polymeric materials or plastics in marine environments, is a necessary complementary component of the whole strategy to control the marine plastic litter and micro-, nano-plastics threat. The present work focuses on identifying gaps and improving available laboratory test methods for measuring the aerobic biodegradation of plastics in the seawater column within the coastal zone (pelagic environment). The research work followed a methodology that is based on recommendations of ASTM D6691:2017 concerning biodegradation of plastics in the seawater and the similar ISO 23977-1:2020. Three different implementation schemes of the test method were applied using different experimental setups and measuring techniques for monitoring the evolved CO2. The effect of critical parameters affecting nutrient adequacy (concentration in inoculum) and oxygen adequacy (bioreactor size, sample size, frequency of aeration) on the biodegradation of four tested materials was explored, and optimal values are proposed. The results allowed for the refinement of the proposed test method to improve reliability and reproducibility.

Thin and Ultra-thin Sidewall Protected P-WLCSP

Diversity in packaging for a strong supply chain requires higher performance and lower cost processes for new manufacturers. Six-side protected, aka “6S or fully protected”, CSP is an emerging and rapidly growing market. Fully protected CSP (without substrates or lead-frames) was first implemented with processes such as M-series and eWLB. These processes require costly and complex die reconstitution, expensive tapes, molding, and other operations most common to FO to obtain 6-side die protection. These steps can be eliminated in a wafer level process to provide high-performance low-cost P-WLCSP to enable new CSP manufacturing capability, Fan-In and Chiplets. American Semiconductor’s Semiconductor-on-Polymer (SoP) 300mm SoP-TM, a P-WLCSP process, is an advanced packaging process optimized for protected CSP, fan-in, and chiplets. Protected FI process innovations can improve performance in power devices, RF switches, photonic IC (PIC), die stacking, and thin board applications. This paper builds on the SoP-TM process development provided at the IMAPS Symposium earlier this year with the addition of first silicon data for electrical test chips. SoP-TM test chip features include 10um silicon thickness, metal interconnect and micro-bumps, smooth silicon sidewalls and 6-side polyimide encasement. Reliability data and testing is a key area of investigation for thin-device technology. Ultra-thin device reliability test methods under consideration for new NIST standards will be presented. Mechanical, high temperature and high humidity reliability for SoP-TM test chips, Chip-on-Flex (COF) and Flip Chip using the new test methods will be presented.

Measurement of engine performance and maps-based emission prediction of agricultural tractors under actual operating conditions

This paper develops a comprehensive data collection system (CDCS) based on radio frequency identification (RFID) technology, on-board diagnostic system (OBD), and portable emission measurement system (PEMS) to study the performance of tractors in the real world. The actual operating modes, fuel consumption and emission levels of the tractor engine were studied and the braking thermal efficiency (BTE) under actual operating conditions was reported for the first time, with a maximum value close to 45%. The engine maps were developed and used to predict tractor emissions and fuel consumption, and the results showed that it can accurately predict tractor fuel consumption and carbon dioxide (CO2) emissions, with mean absolute percentage error (MAPE) and coefficient of determination (R2) values reaching over 90%. This article provides a reliable testing and prediction method for the actual performance of tractor engines, and suggests that real performance indicators should be given better attention.

Leader's influence on the climate in the team

This article analyses the influence of the leader on the team climate in different fields of activity. The article aims to determine the degree of influence of the leader's personality on forming the socio-psychological climate in teams from various fields of activity. The study was conducted with specialists from the IT sphere, pedagogical sphere, medicine, and law enforcement. Valid and reliable test methods were used to obtain reliable data. The prevalence of average indicators of leadership influence in the studied samples has been empirically proven. The tendencies of distribution of the components of the leader's personality depending on the sphere of professional activity were determined. Тhe study results suggest that leadership skills and organisational skills are the most important factors influencing team climate in teams of medical professionals and law enforcement, while communication skills and emotional intelligence are more important in teams of teachers and IT specialists. The research hypothesis has been confirmed. Prospects for further scientific research include studying the impact of different leadership styles on the organisational climate of the team, as well as expanding the research sample by involving representatives of a broader range of specialities.

Best Practices to Quantify and Identify Particulate Matter on the Interior Surfaces of Single-Use Systems.

The manufacturing of a wide range of biopharmaceuticals, from antibodies and vaccines to cell-based therapies, increasingly takes place in single-use processing equipment. Manufactured in clean rooms and sealed and sterilized, single-use systems (SUSs) are ready-to-use and easily scalable. Controls in the "clean-build" manufacturing of SUSs reduce the probability of occurrence of particulate matter in SUSs. However, the size, complexity, and limited transparency of SUSs clearly limit the detectability of particulate matter on the interior (fluid-contacting) surfaces of a SUS during a visual inspection, as demonstrated in a recent study. In applications downstream of final filters or in aseptic processing, particulate matter on the surfaces of a SUS could detach and contaminate the final drug product. A realistic assessment of this risk requires reliable test methods that quantify and identify particulate matter present on the interior surfaces of SUSs. Clearly problematic is the common certification of the cleanliness of a SUS via a force-fit adaptation of the pharmacopeial standard USP <788> entitled "Particulate Matter in Injections". USP <788> does not describe a procedure for extraction of particulate matter from the interior surfaces of SUSs. In addition, application of Method 1 Light Obscuration significantly limits the probability of detection for particles in the visible size range (≥ 100 µm). In this article, we describe best practices for extracting, counting, sizing, and chemically identifying particulate matter on the interior surfaces of SUSs. Highly effective procedures for the extraction of particulate matter result from application of the qualification methodology described in a recently published ASTM standard. Filtration of the liquid extract concentrates particulate matter onto the surface of a membrane filter, allowing rapid particle counting and sizing using automated membrane microscopy, along with detailed chemical identification using infrared microscopy and/or automated confocal Raman microscopy.

Development and Validation of a Simple, Fast, and Accessible HPLC-UV Method for Cannabinoids Determination in Cannabis sativa L. Extracts and Medicinal Oils.

Cannabis sativa L. is a well-recognized medicinal plant. Cannabis regulations in Argentina are insufficient to solve the problem of patient access to full-spectrum cannabis-based products. So, the market of artisanal products with unknown quality and dosage of cannabinoids is increasing, and so is the local demand and need for analyzing these products. However, much of the latest validated methodologies for cannabinoid quantification include expensive instrumentation that is not always available in laboratories of health institutions in Argentina. The aim of this work was to develop and validate a simple and rapid HPLC-UV method for the identification and quantification of principal cannabinoids in cannabis resins, inflorescences, and medicinal oils using standard HPLC equipment. The cannabinoids selected for validation were cannabidiol acid (CBDA), cannabigerol (CBG), cannabidiol (CBD), cannabinol (CBN), delta-9-tetrahydrocannabinol (Δ9-THC), cannabichromene (CBC), and tetrahydrocannabinol acid (THCA). A method for the simultaneous identification and quantification of these 7 main cannabinoids was developed and then validated. Some data parameters were comparable to other reports with more sophisticated analytical instruments for the analysis of cannabis. The assessed limits of detection and the limits of quantitation ranged from 0.9 to 3.66 μg/mL and 2.78 to 11.09 μg/mL, respectively. The concentration-response relationship of the method indicated a linear relationship between the concentration and peak area with R2 values of > 0.99 for all 7 cannabinoids. The relative standard deviation (RSD%) varied from 2.34 to 4.82 for intraday repeatability and from 1.16 to 3.15 for interday repeatability. The percentage of recovery values was between 94 to 115% (resins) and 80 to 103% (inflorescence extract). The cannabis industry is growing rapidly, and there is a need for reliable testing methods to ensure the safety and efficacy of cannabis products. In addition, current methods for cannabinoid analysis are often time-consuming and expensive, while the HPLC-UV method herein reported is a simple, rapid, accurate, and cost-effective alternative for the analysis of cannabinoids in cannabis resins, inflorescences, and medicinal oils. This method will be proposed to be included in the Cannabis sativa L. monograph of the Argentine Pharmacopoeia.

Evaluating Cemented Paste Backfill’s Strength Development at Early Age Using the Laboratory Vane Shear Test

Abstract The Unconfined Compressive Strength (UCS) test is the most widely used method in the underground mining industry to assess strength development during binder hydration. However, testing errors are common for weak materials (UCS less than 100 kPa, i.e., cemented paste backfill at early curing stage), and reliable test methods must be established for designs relying on early age strengths, particularly for continuous pours. Therefore, the standard geotechnical laboratory vane shear test is investigated as an alternative. A newly designed “cast-in-place” mold is used to avoid specimen damage arising from vane insertion. Parametric tests with vane rotation speeds of 30 to 120 degrees per minute show strength insensitivity to these shear rates. Vane shear strengths correlate linearly with UCS over the strength ranges used; however, the trend does not follow the usual assumption for clays in the undrained state, because the material does not shear at a constant volume as clays do. The influence of suppressed dilation is investigated using direct shear tests, but these results do not fully explain the discrepancy, suggesting other mechanisms also have an important influence. Therefore, vane shear tests can provide a useful complement to UCS tests not only at the laboratory scale but in the in situ condition for early strength characterization. It should be noted that the correlation to UCS must be considered empirical, and separate calibrations are required for each backfill material.

Development of the test method for wind turbine blade subcomponent under combined bending and torsion loads

The conventional full-scale wind turbine blade testing method is unable to study the detailed structural response of blades' key subcomponents under complex loads. Therefore, developing an efficient and reliable blade subcomponent testing method is of great significance for investigating the structural characteristics of blades. This paper develops an innovative blade subcomponent test method framework, which is capable of studying the structural response under combined bending and torsion load conditions. A high-fidelity finite element model corresponding to the framework that considers nonlinear factors is established. This study further investigated the influence of boundary conditions on the results. The results showed that the test method proposed in this paper is reasonable, and the experiment based on this method is successfully conducted. The contact nonlinearity and size effects will affect the accuracy of the test results, which can be avoided by adjusting the size of the clamp.

Universal test bench for repeatable multiparametric cochlear implant insertion tests

Abstract Introduction: In cochlear implant surgery, the insertion of the electrode array (EA) into the cochlea is critical as its implementation can influence the preservation of residual hearing. Insertion tests are the primary method for basic research on parameters influencing the insertion and help to further improve the design of EAs and surgical techniques. With automated insertion devices close to clinical application, a consensus on optimal insertion parameters is needed, which requires reliable testing methods. Moreover, the limited availability of EAs needs to be considered. We propose a test setup that provides high repeatability and flexibility for various research questions. Methods: Design requirements for multiple types of experiments such as variability of insertion speed or trajectory as well as cochlear geometry guided the computer aided design of the test bench. Moreover, repeated insertions with the same EA were supposed to be possible. To evaluate its functionality, insertion tests into a 3D printed cochlea model were performed and recorded. Results: The central components of the test bench are a linear actuator driving the EA and a goniometer changing the orientation of the target - a cochlea model or a specimen. A force sensor can be mounted below the target to measure forces in its frame of reference. The experimental results show high reproducibility of insertion forces for recurring trajectories with a single EA. Conclusion: The test bench enables reproducible insertion tests with a high number of repetitions and reduced EA usage. This allows a more detailed investigation of broadly discussed influences on the insertion such as the insertion speed or trajectory as well as cochlear geometry and can thereby drive future EA development.

In Vitro Experimental Study on Hemodynamics of Transcatheter Aortic Valve Replacement

The patient-specific aortic silicone model was established based on CTA data. The digital particle image velocimetry (DPIV) test method in the modified ViVitro pulsatile flow system was used to investigate the aortic hemodynamic performance and flow field characteristics before and after transcatheter aortic valve replacement (TAVR). The results showed that the hemodynamic parameters were consistent with the clinical data, which verified the accuracy of the model. From the comparative study of preoperative and postoperative effective orifice area (0.33 cm2 and 1.78 cm2), mean pressure difference (58 mmHg and 9 mmHg), percentage of regurgitation (52% and 8%), peak flow velocity (4.60 m/s and 1.81 m/s) and flow field distribution (eccentric jet and uniform jet), the immediate efficacy after TAVR is good. From the perspective of viscous shear stress and Reynolds shear stress, the risk of hemolysis and thrombotic problems was low in preoperative and postoperative patient-specific models. This study provides a set of reliable DPIV testing methods for aortic flow field, and provides biomechanical basis for the immediate and long-term effectiveness of TAVR from the perspective of hemodynamics and flow field characteristics. It has important application value in clinical diagnosis, surgical treatment and long-term evaluation.

A non-destructive test method for assessment of cement-sand mortar quality on blockwalls finishes: A short-cut method for achieving acceptance criteria

Monitoring quality of cement-sand mortars used for plastering/rendering masonry surfaces has not been given utmost attention thereby adversely encouraging damp rising and other defects in walls. An attempt is made in this paper to propose a methodology for monitoring the quality of mortars using non-destructive testing method. It enables categorization of the quality of mortar mixes for making decision on acceptance criteria for short-term and long-term strengths of the composite mixture. Firstly, a factorial experimental design using the Central Composite Design (CCD) was used, to design the mix and compressive strengths at 28-day was obtained within the design domain considered. Secondly, a hardness test using the Mohs’ hardness scale was used on both the laboratory specimens and field tests on plastered walls of some selected housing estates. The method clearly exhibited defect patterns on the blockwall finishes which are closely related to the quality of the mix which also varied based on heights above ground level. The Mohs’ hardness test has proven to be a reliable non-destructive test method which can be used to reveal quality and categorization of cement mortar mix used on blockwall finishes. Consequently, the upper bound mix with ratio 1:4 cement to sand mortar remains a reliable mixture proportion based on the scale of hardness and strength performance both in the short-term and long-term values measured. This method would enable a reward system measurement/assessment on contractors and consultants on various building projects.

Research on the Reliability Test and Life Assessment Methods of Relays Used in Circuit Breaker Operating Mechanism

As one of the key components of the circuit breaker operating mechanism, the relay can experience performance degradation due to harsh environmental factors, such as salt spray, during operation, which can ultimately affect the normal operation of the circuit breaker and threaten the safe and stable operation of the power system. To effectively evaluate the condition of the relay operating in salt spray environments over the long term, this study conducted accelerated aging experiments on a certain model of auxiliary switch under salt spray conditions using an existing test platform. The relay’s pull-in voltage, release voltage, pull-in time, and release time were analyzed as characteristic parameters affected by salt spray. The results showed that the intrusion of salt spray caused a decline in the coil performance of the relay, which required higher voltage to provide the electromagnetic force needed for operation, leading to an increase in operating voltage. On the other hand, coil degradation also caused a decrease in the electromagnetic force generated by the step voltage, resulting in a slower operating time. Subsequently, a Genetic Algorithm_Back Propagation Neural Network GA_BP) algorithm model suitable for identifying the relay status in this study was established. After optimization by a Genetic Algorithm Neural Network (GA), the recognition accuracy increased from 78.6% to 91.8%, which showed significant improvement. By clarifying the changes in the characteristic parameters of the relay in a salt spray environment and relying on experimental data, this study established a relevant state recognition model. The research results have important engineering application value for understanding the relay operating status of the circuit breaker operating mechanism in salt spray environments, conducting circuit breaker operating mechanism relay life prediction, and preventing circuit breaker operating mechanism failures.

Pengaruh Kepercayaan dan Harga terhadap Keputusan Pembelian dan Loyalitas Pelanggan pada pembelian Merchandise K-Pop melalui Group Order

Korean pop music or K-Pop is one of the Korean Wave products that millennials are interested in. During the pandemic era, K-Pop fans in Indonesia skyrocketed, leading to increased sales of K-Pop albums and other K-Pop merchandise. This study aims to determine the effect of trust and price on purchasing decisions and customer loyalty in purchasing merchandise K-Pop through Group Order. The research method used is descriptive quantitative. The population in this study are K-Pop fans who are members of the Group Order Jametal, while the samples obtained were 85 people. The sampling technique using the technique non probability sampling by method purposive sampling. Collecting data in this study used a questionnaire created through the Google form. Data was processed using IBM SPSS 25 software with validity and reliability test methods, classic assumption test, multiple linear regression test and hypothesis test (t test). The results of the study show that trust and price have a positive and significant effect on purchasing decisions. And trust and price have a positive and significant effect on customer loyalty.

A comprehensive assessment method for the health status of bronzes unearthed at archaeological sites

As one of the common physical materials in Chinese archaeological excavations, ancient bronzes are an essential basis for studying the development of Chinese bronze culture, which is of great significance for exploring the development law of ancient human civilization and reconstructing ancient human society. As China’s infrastructure advances, the number of bronzes unearthed by archaeological excavations continues to increase. However, environmental damage to artefacts is very complex, whether the buried environment of the artefacts or the above-ground environment when the artefacts are unearthed, leading to different health problems for the excavated bronzes. A scientific assessment of these bronzes needs to be carried out prior to extraction to inform staff how they should be extracted, moved, and transported and how they should be restored afterwards. In response to the above problems, this paper takes excavated bronzes from archaeological sites as the research object and, by analysing and studying the relevant industry standards and the disease characteristics of bronzes, establishes a three-tier indicator framework for assessing the health of bronzes in a layer-by-layer refinement and proposes quantitative indicators with typical correlations. Through extensive research and testing, we screened out efficient, non-destructive, convenient and reliable assessment and testing methods and assessment models that combine subjective and objective aspects suitable for archaeological sites. On this basis, the paper achieves a scientific and practical assessment of the health status of bronzes excavated from archaeological sites. After repeated experiments, a set of comprehensive methods for quickly and conveniently assessing the health status of excavated bronzes was proposed for the first time and successfully applied to the archaeological excavation site of Sanxingdui site in Guanghan City, Sichuan Province, China.

On the Chloride Distribution in Concrete and Mortar Samples after an RCM Test.

It is of essential need to face the challenges of CO2 reduction in industrial cement and concrete production reliable test methods in order to evaluate the performance of concretes, especially with regard to the service life of our infrastructure. The rapid chloride migration test (RCM test) is a standard method to assess the resistance against chloride ingress of concrete. However, during our study, certain critical questions arose with regard to the chloride distribution. The sharp chloride ingress front based on the model assumptions contradicted the shallow gradient of the experimental data. For this reason, investigations on chloride distribution in concrete and mortar samples after RCM tests were performed. The focus was on the factors influencing the extraction, e.g., time after RCM test and the location on sample. Furthermore, differences between concrete and mortar samples were investigated. The investigations showed that no sharp gradient on concrete samples was found due to the extremely uneven chloride front. In contrast, the theoretical profile shape was instead demonstrated on mortar specimens. The prerequisite for this result is that the drill powder must be taken directly after the completion of the RCM test from very uniform penetration areas. Thus, the model assumptions on the chloride distribution via the RCM test could be confirmed.