The global demand for aggregates has escalated, leading to a decline in the availability of quality natural aggregates. In response, the cold bond pelletization (CBP) process emerged in the early 2000s as a novel approach to artificial aggregate production, utilizing dry powdered fly ash. This method involves agglomerating fly ash particles at room temperature in an inclined rotating pan to form pellets. However, the abstract lacks clarity in elucidating the significance of this approach. Our study investigates the mechanical properties of aggregates produced through the CBP method via experimental laboratory methods, focusing on variations in the ratio of fly ash to alkaline activator (FA/AA) and the molarity of Sodium Hydroxide (NaOH). Notably, we found that an effective molarity of 15 resulted in the lowest Aggregate Impact Value (AIV) percentage, indicating improved mechanical properties. Furthermore, we observed fluctuations in AIV values across different FA/AA ratios and NaOH molarities, suggesting nuanced effects on aggregate quality. Our findings underscore the importance of optimizing parameters in the CBP process for enhanced aggregate performance.