Internal Cracks Research Articles

Impact of Optimal Silane Concentration on the Rheological Properties and 3D Printing Performance of Al2O3-Acrylate Composite Slurries

In this study, 3-trimethoxy-silylpropane-1-thiol (MPTMS) was used as a surface modifier for Al2O3 powder to systematically analyze the effects of MPTMS concentration on the rheological properties, photocuring characteristics, and 3D printing performance of photocurable composite slurries. MPTMS concentration significantly influenced the rheological behavior of the slurry. Slurries containing 2 wt.% and 5 wt.% MPTMS exhibited a wide linear viscoelastic range (LVR). However, at concentrations of 10 wt.% and 20 wt.%, the LVR range narrowed, which led to reduced dispersion stability. In dispersion stability tests, the slurry with 2 wt.% MPTMS showed the most stable dispersion, while the 5 wt.% MPTMS concentration exhibited the highest photocuring rate. In 3D printing experiments, the 5 wt.% MPTMS concentration resulted in the most stable printed structures, whereas printing failures occurred with the 2 wt.% concentration. At 10 wt.% and 20 wt.%, internal cracking was observed, leading to structural defects. In conclusion, MPTMS forms silane bonds on the Al2O3 surface, significantly impacting the stability, rheological properties, and printing quality of Al2O3-acrylate composite slurries. An MPTMS concentration of 5 wt.% was found to be optimal, contributing to the formation of stable and robust structures.

Performance Research and Engineering Application of Fiber-Reinforced Lightweight Aggregate Concrete

Low strength and low impact toughness are two of the main issues affecting the use of lightweight aggregate concrete in harsh cold environments. In this study, the strength of concrete was improved by adding high-strength fibers to bear tensile stress and organize crack propagation. Four sets of comparative experiments were designed with freeze–thaw cycles of 0, 50, 100, and 150 to study the mechanical properties of fiber-reinforced lightweight aggregate concrete under freeze–thaw conditions. A detailed study was conducted on the effects of freeze–thaw on the compressive strength, flexural strength, impact toughness, and microstructure of concrete with different fiber contents (3, 6, and 9 kg/m3). The results show that for ordinary lightweight aggregate concrete, under the freeze–thaw cycle, the internal pore water of the concrete froze and generated expansion stress, resulting in tensile cracks inside the concrete. The cracks gradually accumulated and expanded, ultimately leading to cracking and damage of concrete structures. After 150 cycles, the strength loss rate exceeded 25%. When adding a reasonable amount of fiber (6 kg/m3), the fiber took on the tensile stress and hindered the development of internal cracks, significantly enhancing the splitting tensile strength, flexural strength, and impact toughness of lightweight aggregate concrete. And the failure pattern of concrete was significantly improved. At the beginning of the freeze–thaw cycle, the internal tensile stress was less than the fiber tensile strength and the fiber–matrix bonding strength, and the strength reduction rate of the concrete was slow. Relying on the friction absorption capacity between the fiber and the matrix, the fiber used its own deformation to resist the tensile stress. In the late stage of the freeze–thaw cycle, due to the destruction of the fiber–matrix transition zone structure, the bond strength decreased, the crack resistance and toughening effect decreased, and the strength of the concrete decreased rapidly. Moreover, the reduction in impact toughness was greater than the compressive strength and flexural strength under static load.

State-of-the-Art Review of Microcapsule Self-Repairing Concrete: Principles, Applications, Test Methods, Prospects

Cement-based materials are widely used in construction worldwide, but they are vulnerable to environmental stressors and thermal fluctuations, leading to the formation of internal cracks that compromise structural integrity and durability. Traditional repair methods such as surface coatings, grouting, and groove filling are often costly and labor-intensive. In response, self-repairing technologies for cement-based materials have emerged as an innovative and promising solution, offering the potential to significantly extend the lifespan of structures and reduce maintenance costs. A particularly novel approach is the development of microcapsule-based self-repairing concrete. In this system, repair agents are encapsulated within microcapsules and combined with curing agents in the concrete matrix. When cracks form, the microcapsules rupture, releasing the repair agents to autonomously heal the damage. This self-repairing mechanism is characterized by its high efficiency, durability, environmental sustainability, and versatility, making it a promising alternative to traditional repair methods. Recent research has focused on the development of microcapsules with various core materials, such as TDI (toluene diisocyanate), IPDI (isophorone diisocyanate), or epoxy resin, as well as composite shell materials including paraffin wax, PE (polyethylene) wax, nano-SiO2, and nano-CaCO3. A novel advancement in this area involves the enhancement of microcapsules through the incorporation of magnetic nanomaterials into the shell, providing new possibilities for self-repairing systems that address cracks in cement-based materials.

Location Detection and Numerical Simulation of Guided Wave Defects in Steel Pipes

At present, researchers in the field of pipeline inspection focus on pipe wall defects while neglecting pipeline defects in special situations such as welds. This poses a threat to the safe operation of projects. In this paper, a multi-node fusion and modal projection algorithm of steel pipes based on guided wave technology is proposed. Through an ANSYS numerical simulation, research is conducted to achieve the identification, localization, and quantification of axial cracks on the surface of straight pipelines and internal cracks in circumferential welds. The propagation characteristics and vibration law of ultrasonic guided waves are theoretically solved by the semi-analytical finite element method in the pipeline. The model section is discretized in one-dimensional polar coordinates to obtain the dispersion curve of the steel pipe. The T(0,1) mode, which is modulated by the Hanning window, is selected to simulate the axial crack of the pipeline and the L(0,2) mode to simulate the crack in the weld, and the correctness of the dispersion curve is verified. The results show that the T(0,1) and L(0,2) modes are successfully excited, and they are sensitive to axial and circumferential cracks. The time–frequency diagram of wavelet transform and the time domain diagram of the crack signal of Hilbert transform are used to identify the echo signal. The first wave packet peak point and group velocity are used to locate the crack. The pure signal of the crack is extracted from the simulation data, and the variation law between the reflection coefficient and the circumferential and radial dimensions of the defect is calculated to evaluate the size of the defect. This provides a new and feasible method for steel pipe defect detection.

Component‐section transverse‐pressure effect on internal damage and failure mode of post‐installed rebar

AbstractA post‐installed rebar (PIR) is commonly used to establish structural connections between new components and existing structures, such as structural member extensions or concrete layer overlays in the construction/strengthening/retrofitting of buildings or bridges. In joint connections, the anchored PIR system always bears a non‐negligible compression in the component section, which is derived from the loads and self‐weight and has a confinement effect on the anchorage zone. However, excessive pressure can result in the fracture of the adhesive component, thereby leading to brittle failure in the PIR system. Owing to the important role of the adhesive component in the PIR system, this study is focused on the internal damage to the PIR system, and the effect of transverse pressure on the failure modes is investigated. This study comprises an experimental investigation of the failures of a PIR system under transverse pressure and a description of the internal damages based on the test results. Finally, an elastic analysis was established to explain the internal cracking and investigate the stress distribution in the PIR system. The tests on 34 pull‐out specimens showed two typical failures for the PIR system under transverse pressure (adhesive–rebar [A–R] interface failure and adhesive fracture failure). The A–R interface failure resulted from the shearing failure in the adhesive component, while the adhesive fracture failure resulted from the propagation of longitudinal and transverse cracks. The elastic analysis indicated that cracking in the concrete and adhesive component was dominated by circumferential stress, and the rebar rib direction and adhesive component thickness had a significant influence on the stress distribution. Based on this, some suggestions for anchorage design were made.

Biologically inspired adaptive crack network reconstruction based on slime mould algorithm.

The dynamic crack propagation trajectories play a crucial role in enhancing our understanding of spatial mechanisms involved in crack expansion. However, visualization of internal cracks under complex crack conditions has always been a challenge. Biological networks have been honed by many cycles of evolutionary selection pressure and are likely to yield reasonable solutions to such combinatorial optimization problems. This study applied the slime mould algorithm to improve the accuracy of internal crack localization in rocks and employed Minimum spanning tree and Gaussian mixture model to construct the crack propagation trajectories. By introducing the concept of bond length, the evolution characteristics of crack levels were effectively characterized. Research results showed that this approach effectively preserves essential crack localization information while mitigating the influence of interfering parameters, providing crack characterization results that exhibit high consistency with actual fracture patterns. The curves of cumulative bond length and relative bond length over time conform to the trend of a Growth/Sigmoidal curve. The strength of the bond was correlated with the temporal process of crack propagation. This result could be helpful for analyzing crack trajectories and predicting rock stability.

Insights of Physicochemical Structure Changes of Bituminous Coal with Acidification-assisted Controlled Electric Pulse through SEM, XRD and FTIR

Controlled electric pulse (CEP) cracking coal effectively enhances its permeability, but a high coal breakdown voltage (BV) can result in technical difficulties. To address this problem, the method of using HCl solution to improve the electrical conductivity of coal was proposed. The effects of HCl on coal BV were investigated, and the microstructural changes in coal were analyzed through scanning electron microscopy, X-ray diffraction, and Fourier-transform infrared spectroscopy. Compared with raw coal, the BV of acidified coal decreased significantly. The crushing degree of the coal samples was clearly enhanced with an increasing HCl concentration. Some internal coal minerals were acidified and dissolved, the aromatic layer spacing (d002) increased and the layer sheet stacking height (Lc) decreased, and the crystal structure was damaged. When acidified coal was broken down, numerous internal pores and cracks appeared, active coal groups were shed, the aliphatic hydrocarbons and oxygen-containing functional group contents increased, surface activity was reduced, and the hydroxyl content was reduced, which was conducive to rapid gas desorption. Acidification effectively reduces the BV of coal and improves the cracking and permeability enhancement effect of coal by CEP action.

Effect of cementitious capillary crystalline waterproof material on the mechanical behavior of concrete

Cementitious capillary crystalline waterproof material (CCCW) is a material that can react with substances inside the concrete, generating crystals that fill the pores and cracks in the concrete. This chemical reaction is expected to improve the mechanical properties of the concrete. This study investigated the effects of CCCW content and water-cement ratio (W/C) on the compressive behavior of cementitious capillary crystalline waterproof concrete (CCCWC). The results indicated that as the CCCW content increased from 0% to 1.5% for W/C of 0.4, the compressive and tensile strength values of concrete slightly decreased. This is because excessive CCCW generates too many crystals within the concrete, leading to internal matrix expansion and crack formations. However, in the cases of W/C of 0.45 and 0.5, the compressive and tensile strength values of the CCCWC increased wit increasing CCCW content from 0% to 0.5%, but declined with 1.5% CCCWC addition. The reaction between CCCW and concrete generates numerous crystals, which densify the concrete matrix and enhance its strength. Moreover, with increasing W/C, the CCCWC's compressive strength and tensile strength decreased due to the increased porosity of the concrete matrix and the reduced availability of the concrete constituents that react with CCCW. Furthermore, the appropriate choice of CCCW content and W/C can significantly enhance the slope and peak stress of the stress-strain curve. Based on this, a compressive constitutive model of CCCWC was established. The findings showed that the optimal CCCW content varied with W/C. For instance, for a W/C of 0.4, the maximun compressive strength of 54.82 MPa was achieved without any CCCW addition. In contrast, the addition of 0.5% CCCW to concrete produced with W/C of 0.45 and 0.5 resulted in the highest compressive strengths of 50.98 MPa and 44.90 MPa, respectively.

Improving the adsorption of cloud concrete stone porous aggregate to phase change materials by alkali modification

In this paper, the pore structure of cloud concrete stone (CCS) was optimized by alkaline hydrothermal treatment to improve its adsorption capacity for phase change materials (PCMs), thus enhancing the heat storage effect of phase change composite aggregates. The results showed that the adsorption rate of CCS modified by alkaline solution for 36 h was 21.49%, which increased by 30.64% relative to that without modification. The macroscopic and microscopic morphology showed that the 24-hour modified CCS appeared small cracks in the surface and the internal pores became more numerous. The 48-hour modified CCS appeared exfoliated on the surface and the internal pores and cracks increased. Hydrothermal treatment changes the pore structure of CCS, making it more conducive to the adsorption of PCM.

Numerical analysis of failure mechanics of concrete under true dynamic triaxial loading using a four-phase meso-model

In the present paper, the failure mechanics of concrete under true triaxial dynamic loading is investigated. A four-phase concrete meso-model is developed. The meso-model consists of aggregate, mortar, interfacial transition zone (ITZ) and macropores. A finite element (FE) model of a split Hopkinson pressure bar is also created to apply true triaxial dynamic loading. The development of cracks in concrete is presented for the uniaxial, biaxial and triaxial loading cases. The presence of local discontinuity is modelled, and its effect on the failure of concrete is extensively investigated and discussed. In the last, the effect of aggregate distribution is also analysed. It is found that the internal structure of concrete changes the stress distribution from true triaxial to compression or extension triaxial, which is the prime cause of internal cracking.

Damage accumulation in carbon steel under low-cycle loading at the crack initiation stage and strain ageing temperature

Based on the strain criterion for fatigue fracture and experimental studies, the damage accumulation kinetics from recoverable plastic strain (plastic strain in the tensile half-cycle), from the unilateral accumulation and elastic strain with the increasing number of loading cycles was studied. The influence of stress ageing on the redistribution of the levels of these components of damage, depending on the number of cycles before destruction, was studied. Depending on the load level, the limit states (formation of a surface macro-crack or buckling failure of strain stability due to the formation of an internal crack in the quasi-static fracture range) were established. Strain ageing reduces the range of quasi-static fracture. It is shown that the critical values of strains and stresses correspond to the limit states. The parameters determining the capacity of structural materials under static and cyclic loading under conditions of stress ageing are confirmed.

Evolution of Holes and Cracks in Pre-Carbonized Glassy Carbon.

Being a type of carbonaceous material, glassy carbon possesses thermomechanical properties akin to ceramics, offering both mechanical and chemical stability at high temperatures; therefore, it can be applied in electrochemistry and high-temperature manufacturing. However, the direct pyrolysis of a bulk precursor leads to internal pores and cracks, usually resulting in fracture. Our characterization results show that at temperatures below 400 °C, large pores do not form, and pre-carbonized glassy carbon (PGC) formed at 350 °C has a dense microstructure without cracks. It exhibits a high compressive strength of ~370 MPa and flexural strength of ~190 MPa, making it suitable for load-bearing applications. Additionally, the PGC-350 material shows small mass loss (~5%) and reasonably low thermal expansion (2.5 × 10-6/°C) when heated to 350 °C again. These properties suggest the potential of PGC for high-temperature applications. As a demonstration, PGC formed at 350 °C was employed to fabricate molds to press chalcogenide glass blanks, which exhibited favorable molding results for various surface morphologies.

Structural characteristics and evolution in the crack propagation process of NiCrAlY/YSZ gradient coatings through thermal shock at 900 °C

In this study, four different thicknesses of NiCrAlY/8YSZ gradient coatings were fabricated using atmospheric plasma spraying (APS) technology. The failure behavior and lifetime of coatings were subsequently compared and analyzed through thermal shock experiments. The results revealed a pronounced correlation between the initiation and propagation of internal cracks within the gradient coatings and the thickness of the gradient region at a thermal shock temperature of 900°C. Both horizontal and vertical cracks were observed to propagate and interconnect, with horizontal crack propagation being the primary cause of coating failure. Notably, samples featuring a gradient region thickness of 150μm exhibited superior thermal shock resistance, suggesting promising prospects for enhanced coating durability.

Crack evolution and fractal characteristics of fractured red sandstone based on acoustic emission parameters

Rock is a widely used engineering material, and accurate understanding of its internal microcrack evolution process during loading can provide a theoretical basis for preventing instability and failure in rock engineering. The rock pressure test system and acoustic emission equipment were used to carry out uniaxial loading and acoustic emission monitoring tests on fractured red sandstone. Based on the RA and AF values of acoustic emission and the fractal theory, the internal crack patterns and evolution rules of red sandstone with different crack angles were explored. The results show that the compressive strength of red sandstone varies with the crack Angle in the shape of “U”, and there is an obvious stress drop after the elastic stage of 30° and 45° crack red sandstone, which has a good correspondence with the acoustic emission ringing count rate. During the loading process, the damage mainly caused by tension cracks first appears inside the rock, and then the tension cracks increase steadily and the shear cracks gradually increase, indicating that the rock enters the stage of fracture instability development. With the development of shear cracks, the peak strength is finally reached and the instability failure occurs. During the loading process of 30° fracture red sandstone, the corresponding stress drop phenomenon of “shear crack group” appears. According to the D/S statistical analysis of different crack samples based on acoustic emission ringing count, the fractal dimension presents a decreasing-rising-decreasing trend with the increase of crack inclination, which corresponds to the change of the complexity of crack development in rock.

An anode‐supported tubular proton conductor fuel cell with an inner ceramic ammonia cracking component

AbstractA tubular proton‐conducting fuel cell, anode‐supported, was fabricated using dip‐coating and followed by the co‐sintering of anode and electrolyte at 1500°C. The electrolyte and anode thicknesses are respectively 6 and 500 µm. The outer diameter of the tubular cell is 5.8 mm, featuring an anode porosity of 23%. Ammonia‐fueled single cell with Ru‐catalyzed internal cracking reactor is operated at various temperatures from 400°C to 600°C. Calculation results indicate that double‐ring current collection is an efficient current‐collecting mode. At 600°C, the device exhibited a high open‐circuit voltage of 1.02 V and a peak power density of 216 mW cm−2, with a total active area of 2.28 cm2. Exhaust gas analysis reveals a 99.13% ammonia decomposition rate at 600°C.

Study on non-destructive visualization identification of concrete internal cracks based on SH array ultrasound

Ultrasonic nondestructive testing (NDT) technology was one of the most frequently used and fastest-developing NDT techniques in detection field. This method had high detection sensitivity, more accurate defect localization, and was harmless to the human body. With the development of ultrasonic testing technology, modern ultrasonic imaging technology generally had automatic data acquisition and processing functions, which allowed for intuitive and clear recognition of internal defects by the human eyes. The overall purpose of this study was to visualize the cracks in concrete by synthetic aperture focusing technique (SAFT) and full-waveform inversion (FWI) algorithms on the basis of ultrasonic nondestructive testing technology. At present, there have been studies on the use of ultrasonic instruments to detect the internal defects of concrete. However, the accuracy and authenticity of this method have not been compared in previous studies. Therefore, in this experiment, four concrete specimens with different buried depths, angles, shapes, and thicknesses of cracks were designed. Based on SH ultrasonic wave NDT technology, two types of operations were performed on the collected ultrasonic wave data: one was the application of SAFT method, and the other was the first application of FWI method for detecting internal cracks in concrete. The study found that both algorithms were most accurate in determining the burial depth of cracks, with error results not exceeding 10 %. They also showed good recognition effects for the angle, shape, and thickness of the buried cracks. This proved that both identification methods had the capability to recognize internal cracks. The Introview software bundled with the ultrasonic instrument could identify cracks using SAFT directly and quickly. When FWI was used with MATLAB computation, the results were more precise and intuitive. The overall purpose of this study was to detect cracks in concrete by SAFT and FWI algorithms on the basis of ultrasonic nondestructive testing technology. Combining the two crack identification techniques could be of great significance for ensuring the long-term safety and stability of concrete structures, providing strong support for structural maintenance and reinforcement.

Performance and mechanism of triethanolamine-triisopropanolamine corrosion inhibitor to deterioration of reinforced concrete under the coupling effect of freeze-thaw cycles and chloride attack

The purpose of this study is to propose an efficient and economical organic triethanolamine-triisopropanolamine corrosion inhibitor (OTTCI) to reduce the corrosion of steel in reinforced concrete. The influence of OTTCI on corrosion of steel in reinforced concrete under the coupling effect of freeze-thaw cycles and chloride attack (FTCs-CA) were characterized by electrochemical impedance spectroscopy (EIS), dynamic electrode potential (PDP), mechanical properties (mass loss rate (M), compressive strength (fn) and relative dynamic elastic modulus value (Pi)), capillary water absorption (CWA), bubble spacing coefficient (BSC) and scanning electron microscope (SEM). The inhibition mechanism of OTTCI was also analyzed and summarized. The results displayed that the dosage of OTTCI delayed the degradation of reinforced concrete under FTCs-CA. After 150 cycles, the M value of specimens with 1.0 % OTTCI reduced by 66.31 % compared to that of specimens without OTTCI, the Pi value increased by 51.9 %, and the polarization resistance and corrosion inhibition efficiency reached 2744.19 Ω cm2 and 92.88 %, respectively. In addition, OTTCI significantly reduced the CWA value and porosity. After 150 cycles, the CWA and porosity with 1.0 % OTTCI decreased by 60.1 % and 54.54 % respectively. The capillary water absorption coefficient increased linearly with the increase of FTCs-CA. SEM tests illustrated that OTTCI inhibited the development of internal cracks and macropores in concrete and promoted the formation of hydrated calcium silicate gels and calcite. The application of this study not only provides a new method to alleviate the deterioration of reinforced concrete, but also offers theoretical and technical support for further investigate on the deterioration characteristics of reinforced concrete in harsh environments.

Performance Investigation of Multi-Turn Pickup for Circular Fractal Flexible Planar Eddy Current Probe

ABSTRACT This paper aims to compare and analyze the performance differences between a single-coil and multi-coil pickup coil layout in a flexible circular fractal planar eddy current probe. Flexible planar eddy current probes offer flexibility and adaptability, making them widely used in the detection of complex structures. The circular fractal flexible planar eddy current probe is a new type of probe that has a lower miss rate in detecting cracks at specific angles compared to traditional circular and rectangular coil eddy current probes. However, the single-coil structure of the probe’s pickup coil has the drawback of being less sensitive to weak signals. This paper investigates the detection performance of the flexible circular fractal probe by varying the number of turns in the original pickup coil. Experimental comparisons were conducted by preparing and installing single-coil and multi-coil circular fractal planar eddy current probes. The performance differences between single-coil and multi-coil configurations were compared and analyzed under various excitation frequencies, liftoff distances, and internal crack depths. The results showed that, compared to the single-coil probe, the multi-coil probe exhibited significantly improved detection signal values and sensitivity.

Hard rock fragmentation by dynamic conical pick indentation under confining pressure

Mechanical mining and excavation in deep metal mines can be regarded as the process of crushing hard rock by conical pick indentation. In this study, a confining pressure loading device was designed and used to carry out dynamic conical pick indentation crushing tests under confining pressure conditions on three types of granite with varying strengths, using the Split Hopkinson Pressure Bar (SHPB). The objective was to quantitatively investigate the effect of confining pressure and rock strength on the indentation crushing characteristics of deep hard rocks. The results indicate that as the confining pressure increases from 5 MPa to 20 MPa, the dimensional parameters such as volume, diameter and depth of the impact groove decrease linearly, while parameters such as the specific energy, indentation force, indentation index and energy utilization rate progressively increase. The increase in the confining pressure inhibits the formation of internal cracks in the rock, enhancing its resistance to pick indentation, which in turn makes rock fragmentation more difficult. This creates unfavorable conditions for efficient rock breaking. Furthermore, rock strength plays a crucial role in the pick indentation process. The higher the rock strength, the greater its resistance to pick indentation, leading to increased energy consumption, accelerated wear of the conical picks, and reduced efficiency in rock breaking.

Experimental Study on Damage Constitutive Model of Rock under Thermo-Confining Pressure Coupling

Underground engineering frequently encounters the challenges of high temperatures and high confining pressures. The combined effects of temperature and confining pressure can significantly alter the mechanical properties of rock. Evaluating the impact of these factors on rock is a crucial aspect of engineering. This study investigates the mechanical properties of rocks under various temperature and stress conditions, focusing on the deformation and failure characteristics of four typical rock types: granite, red sandstone, gray sandstone, and shale under temperature-confining pressure coupling. The results indicate that high temperatures cause internal structural damage and crack propagation in rocks, leading to a reduction in compressive strength and elastic modulus. Conversely, high confining pressures can inhibit crack propagation and enhance rock deformation capacity. Additionally, significant differences were observed in the mechanical responses of different rocks; red sandstone and shale predominantly exhibited shear failure under the coupled effects of temperature and confining pressure, whereas granite and gray sandstone exhibited bulging failure. Based on the experimental results, an elastic modulus fitting model considering the temperature-confining pressure coupling effect was proposed, and the parameters of the Drucker–Prager criterion were modified. A constitutive model was constructed to accurately reflect the stress–strain state of rocks under the coupled effects of temperature and confining pressure. The constitutive model results show good agreement with the experimental findings.