Interim Materials Research Articles

Comparative Evaluation of Surface Roughness and Color Stability of Polyetheretherketone with Conventional Interim Prosthetic Materials: An In Vitro Study.

The aim of this in vitro study was to compare the surface roughness and color stability of polyetheretherketone (PEEK) with those of conventional interim prosthetic materials like polymethylmethacrylate, bis-acrylic composite, and rubberized diurethane dimethacrylate, following immersion in solutions of varying pH value. A total of 320 circular discs with 10 mm diameter and 2 mm height were divided based on the fabrication (n = 80)-group A: polymethylmethacrylate; group B: bis-acrylic composite; group R: rubberized diurethane; and group P: hot-pressed PEEK-and were subjected to baseline measurement of roughness (n = 40) and color (n = 40) using 3D profilometer and UV-Vis spectrophotometer, respectively. Later, 10 samples from each group were immersed in distilled water, black coffee, green tea, and Pepsi, respectively, for 120 days, and measurements of roughness and color were repeated. The differences in roughness (ΔRa) and color change(ΔE) were calculated and statistically analyzed with a significance level of p-value < 0.05. Irrespective of the immersion solution, the highest mean difference in the roughness values was shown by rubberized diurethane specimens: ΔRa = 3.574880 (0.0048350) in carbonated beverages, and lowest difference was shown by bis-acrylic composite: ΔRa = 0.29004 (0.0017473) in distilled water. The greatest color stability was exhibited by PEEK. The type of interim material and immersion solution had a statistically significant effect on change in color and roughness values. The immersion in solutions of varying pH had a significant effect on surface roughness and color stability of all the tested materials. The Ra value of all specimens after immersion was still within the clinically acceptable range. Polyetheretherketone was the most color stable material in all solutions, except in green tea. This study will provide guidance to dentists and patients regarding the selection of interim material for long-term use, depending on the effect of beverage consumption on its color stability and roughness. How to cite this article: Saraswathy A, Latha N, Ayyadanveettil P, et al. Comparative Evaluation of Surface Roughness and Color Stability of Polyetheretherketone with Conventional Interim Prosthetic Materials: An In Vitro Study. J Contemp Dent Pract 2024;25(10):930-935.

Investigation of the Effects of Thermal Cycling and Surface Treatments on Interim Resin Materials Produced with Additive Manufacturing

This study aimed to compare the impact of thermal cycling on the flexural strength (σfs) of 3-dimensional (3D) printer resins and polymethyl methacrylate (PMMA). It also aimed to evaluate different surface treatment protocols and surface sealant applications on the surface roughness (Ra) and surface hardness (VHN) of the resins used. Rectangular (25�2�2 mm) and disc (Ø10�2-mm) specimens were fabricated from auto-polymerized PMMA, and 3D-printed resins were tested for mechanical properties (ISO 10477) using thermal cycling (n=10). Disc specimens were separated into three groups (n=10) based on the surface treatments: conventional sanding (C), disk polishing (P), and surface sealant coating (O). Ra and VHN values were statistically analyzed with the Kolmogorov Smirnov, Shapiro Wilk, Independent Samples t-test, Mann-Whitney test, one-way ANOVA test and Kruskal Wallis test (α =.05). A significant main effect was found on the flexural strength analysis for each of the two factors: thermal cycling procedure (p[0.001) and materials (p 0.001). A significant main effect was found on the surface roughness and hardness analysis for each of the two factors: surface treatment protocols (p[0.001) and materials (p[0.001). Based on the results; interim materials produced with 3D-printed resins have better mechanical properties than conventionally polymerized materials. Coated materials had lower surface roughness values than polished ones, and adding a surface sealant agent increased their hardness significantly.

Effect of toothbrushing on surface roughness and gloss of CAD-CAM versus conventional interim materials with different surface treatments

Characterizing interim restorations promotes esthetics. However, studies on the effects of characterization materials on the surface roughness and gloss of interim materials after toothbrushing are lacking. The purpose of this in vitro study was to evaluate the surface roughness and gloss of 5 different interim materials with different surface treatments after 1 year of simulated toothbrushing. Cuboid specimens (10×12×2 mm) were fabricated from each interim material: autopolymerized polymethyl methacrylate (UNIFAST Trad), autopolymerized bis-acryl composite resin (Protemp 4), light-activated composite resin (REVOTEK LC), milled polymethyl methacrylate block (DD provi P HI), and 3-dimensionally printed methacrylate oligomer (Nextdent C&B MFH). Each material was divided into 3 groups based on surface treatment (n=10): polishing, application of Lite Art and Resin Glaze, and application of OPTIGLAZE color. The specimens were subjected to 5000 and 10 000 cycles of toothbrushing. The surface roughness and gloss were measured and separately analyzed by using 3-way repeated measures ANOVA (α=.05). Significant interactions of the surface roughness and gloss among interim materials, surface treatments, and toothbrushing durations were found (P<.001). After 5000 and 10 000 cycles, each polished material showed no significant difference in surface roughness compared with baseline: Protemp 4 (P>.999), REVOTEK LC (P>.999, P=.922), and Nextdent C&B MFH (P>.999), except for UNIFAST Trad and DD provi P HI (P<.001). Coating with Lite Art and Resin Glaze, as well as OPTIGLAZE color, significantly reduced surface roughness after both 5000 and 10 000 cycles for all materials (application of Lite Art and Resin Glaze with UNIFAST TRAD (P<.001), Protemp 4 (P<.001), REVOTEK LC (P<.001), DD provi P HI (P<.001), and Nextdent C&B MFH (P<.001, P=.002), and application of OPTIGLAZE color with UNIFAST TRAD (P<.001), Protemp 4 (P<.001), REVOTEK LC (P<.001, P=.002), DD provi P HI (P<.001), and Nextdent C&B MFH (P<.001, P=.008)). Specimens with these treatments also exhibited significantly better gloss compared with the polished specimens (P<.001). After 5000 to 10 000 cycles of toothbrushing, Protemp 4, REVOTEK LC, and Nextdent C&B MFH, interim materials containing fillers, exhibited smoother surfaces compared with UNIFAST Trad and DD provi P HI, interim materials without fillers. Coating of all materials reduced surface roughness and increased gloss. After 5000 to 10 000 cycles of toothbrushing, the surface roughness of each material remained stable; while the gloss decreased slightly, it remained within clinically acceptable levels.

Effect of Hydrogen Peroxide-Based Bleaching Agents on the Color Dimensions and Surface Roughness of Different Milled Restorative Dental Materials.

To compare the color dimensions, color discrepancies (ΔE00), and surface roughness of milled materials before and after application of a bleaching agent. A total of 10 extracted molars were obtained. Each tooth was cut in transverse sections to create disks (3-mm thick, 10-mm diameter; control group). Disk specimens of eight materials (n &#61; 10 per group) were fabricated: polymethyl methacrylate (PMMA) interim material (PMMA-Telio group), two resin nanoceramics (RNC-Ultimate group and RNC-Cerasmart group), two hybrid ceramics (HC-Shofu group and HC-Enamic group), lithium disilicate (LD-Emax group), zirconia-reinforced glass ceramic (ZGC-Suprinity group), and zirconia (Zr-InCeram group). Color measurements were obtained using a spectrophotometer before and after applying 35% hydrogen peroxide-based bleaching agent. Pre- and postbleaching surface roughness (Sa) analyses were completed using a profilometer. Significant L*, a*, b*, and ΔE00 value differences were found (P < .05). Color discrepancies (ΔE00) ranged from 0.30 ± 0.14 to 4.82 ± 0.10. The highest color discrepancies were measured on the PMMA-Telio group, while the lowest color discrepancies were computed for ZGC-Suprinity, RNCUltimate, and RNC-Cerasmart. Significant surface roughness differences were found (P < .05). The largest increase of surface roughness values between the pre- and postbleaching measurements was obtained in the PMMA-Telio group with a mean ΔSa value of 4.73 ± 3.02, while the largest decrease of surface roughness values between the pre- and postbleaching measurements was obtained in the Zr-InCeram group with a mean ΔSa value of -1.58 ± 0.10. The milled materials showed significant pre- and postbleaching color and surface roughness discrepancies.

Effect of milling procedures in CAD-CAM systems on the color changes of CAD-CAM polymethyl methacrylate resin material as interim material

PurposeThis study aimed to investigate the effects of new and used burs on CAD-CAM PMMA resin color changes following thermocycling.Materials and methodsTwenty disk-shaped specimens (10 × 2 mm) were made using a single brand of CAD-CAM polymethyl methacrylate resin (Polident) for the color test. Group N consisted of half of the specimens that were machined using the new tungsten carbide bur set, and Group U consisted of the specimens that were milled using the used bur set (500 machining time). A color test was performed on the specimens both before and after thermocycling. For the statistical analysis, the Kruskal-Wallis and Dunn Pairwise Comparison tests were employed.ResultsThe ∆E* value of specimens (2.057) milled with the used bur was higher than those of specimens milled with the new bur (0.340), but this value is within clinically acceptable limits. After thermocycling, specimens milled with the utilized burs had the greatest L* (93.850) and b* (5.000) values. After thermocycling, statistically significant differences were discovered between Group N and Group U as well as between specimens milled with the utilized bur before and after thermocycling.ConclusionThermocycling process have an effect on the mean ∆E values of specimens milled with the used carbide bur, but these ∆E* values were not statistically significant.Clinical significanceThe color and clinical performance of CAD-CAM restorations may be affected by variations in CAD-CAM milling bur properties, particularly those related to their frequent use.

Maximum Fracture Load of Interim Crowns Fabricated by Additive and Subtractive Techniques.

To evaluate fracture load values of five types of interim CAD/CAM crowns with and without thermocycling. A complete coverage crown was designed on a mandibular first molar with a uniform 1.5-mm axial and occlusal reduction, and the STL file was exported to manufacture 100 crowns using five materials (20 crowns per material): ZCAD Temp Esthetic (SM-ZCAD; Harvest Dental); Telio CAD (SM-TCAD); P pro Crown and Bridge (AM-PPRO); E-Dent 400 C&B MHF (AM-EDENT); and DENTCA Crown & Bridge (AM-DENTCA). Each group was then divided into two subgroups: before and after thermocycling (10 cornws per subgroup). The STL file of the mandibular first molar die was used to manufacture 100 resin dies. Each die was assigned to one interim crown. Interim crowns were then luted to their assigned die using a temporary luting agent. The fracture strength of crowns was then assessed using a universal testing machine at a crosshead speed of 2 mm/minute. Two-way ANOVA followed by Tukey multiple comparations post-hoc tests were used to assess the effect of material choice and thermocycling process on the fracture strength of interim crowns (α = .05). Material choice and the thermocycling process exerted a significant (P < .001) impact on the fracture strength of interim crowns. However, the interaction between these two factors did not yield a statistically significant effect (P = .176). Within the limitations of this study, the type of interim materials and thermocycling process have a significant impact on the fracture strength of interim crowns.

Current narratives of regional historical demography

Among the main tasks at the turn of the 20th-21st centuries, the most significant ones were to increase the life expectancy and quality of life of the population, improve their health, reduce mortality, and restore the population by increasing the birth rate, which is firmly intertwined with the factors of the socio-economic vector of social development. The demographic situation in the Orenburg Region, which developed in the nineties of the 20th century, was characterized by negative processes caused by a simultaneous reduction in the birth rate and an increase in mortality, characteristic of Russia as a whole. Considering that retrospectiveness in demography is relevant, the transformation of previous interim materials in order to implement the dynamics of processes in the examination, the “experience of historical demography”, including regional experience, should be clearly studied.

Comparison of fracture strength, surface hardness, and color stain of conventionally fabricated, 3D printed, and CAD-CAM milled interim prosthodontic materials after thermocycling.

The purpose of this in vitro study was to investigate the fracture resistance, surface hardness, and color stain of 3D printed, CAD-CAM milled, and conventional interim materials. A total of 80 specimens were fabricated from auto polymerizing polymethyl methacrylate (PMMA), bis-acryl composite resin, CAD-CAM polymethyl methacrylate resin (milled), and 3D printed composite resin (printed) (n = 20). Forty of them were crown-shaped, on which fracture strength test was performed (n = 10). The others were disc-shaped specimens (10 mm × 2 mm) and divided into two groups for surface hardness and color stainability tests before and after thermal cycling in coffee solution (n = 10). Color parameters were measured with a spectrophotometer before and after each storage period, and color differences (CIEDE2000 [DE00]) were calculated. The distribution of variables was measured with the Kolmogorov Smirnov test, and one-way analysis of variance (ANOVA), Tukey HSD, Kruskal-Wallis, Mann-Whitney U tests were used in the analysis of quantitative independent data. Paired sample t-test was used in the analysis of dependent quantitative data (P < .05). The highest crown fracture resistance values were determined for the 3D printed composite resin (P < .05), and the lowest were observed in the bis-acryl composite resin (P < .05). Before and after thermal cycling, increase in mean hardness values were observed only in 3D printed composite resin (P < .05) and the highest ΔE00 value were observed in PMMA resin for all materials (P < .05). 3D printing and CAD-CAM milled interim materials showed better fracture strength. After the coffee thermal cycle, the highest surface hardness value was again found in 3D printing and CAD-CAM milled interim samples and the color change of the bis-acryl resin-based samples and the additive production technique was higher than the PMMA resin and CAD-CAM milled resin samples.

Konvansiyonel, Eksiltmeli ve Eklemeli İmalat Tekniklerinde Kullanılan Geçici Kron Materyallerinin Yüzey Pürüzlülüğüne Diş Fırçalama ve Yüzey İşlemlerinin Etkisi: İn Vitro Çalışma

Background: This study aimed to compare the effect of the surface treatment and toothbrushing abrasion on the surface roughness of interim crown material specimens manufactured using conventional, subtractive, and additive processing techniques.&#x0D; Material and methods: 80 disk-shaped specimens were prepared from 4 different interim crown materials; one auto-polymerized polymethyl methacrylate resin (PMMA);(IM) and one bis-acryl composite resin;(AC) for conventional technique, one computer-aided design/computer-aided manufacturing (CAD-CAM) PMMA block;(TC) for subtractive process, one 3-dimensionally (3D) printed resin;(CB) for additive process. Specimens of each interim crown material were divided into two subgroups according to applied surface treatments; conventional polishing or surface sealant agent coupling (n=10). The surface roughness values of specimens before (Ra0) and after 10,000 cycles of toothbrushing (Ra1) were measured with a profilometer. Data were statistically analyzed.&#x0D; Results: The polished groups of all interim crown materials showed significantly higher Ra0 values compared to the sealant groups before toothbrushing (p˂0.05). While the polished IM groups exhibited the highest Ra0 value (0.44±0.08), the sealed TC groups exhibited the lowest Ra0 value (0.23±0.06). The Ra values of all material groups increased after simulated 1-year toothbrushing. While the polished IM group exhibited the highest Ra1 value (0.45±0.14), the sealed CB group had the lowest Ra1 value (0.31±0.09).&#x0D; Conclusion: It was observed that toothbrushing caused an increase in the surface roughness of all interim materials. The application of a surface sealant agent to these materials is more effective than polishing to reduce surface roughness. Sealed 3D printed resin for additive process exhibited the lowest mean roughness value after toothbrushing.&#x0D; Keywords: Additive Manufactured, Interim Crown Material, Roughness, Subtractive Manufactured, Toothbrushing Abrasion

Effect of different surface treatments on the retention force of additively manufactured interim implant-supported crowns.

To compare the effect of different pre-cementation surface treatments and bonding protocols on the retention force of additively manufactured (AM) implant-supported interim crowns. A total of 50 AM interim crowns (Temporary CB resin) were cemented on implant abutments. Five groups (n = 10) were established based on the different surface pre-treatments performed in the intaglio surface of the specimens: no surface pre-treatment (Group C or control), air-abraded with 50-μm aluminium oxide particles (Group AP), air-abraded with 50-μm aluminium oxide particles followed by the application of silane (Group AMP), silane (Group MP), and air-abraded with 30μm silica-coated aluminum oxide particles followed by the application of silane (Group CMP). Each specimen was cemented into an implant abutment using a composite resin cement (Rely X Unicem2). Afterward, the specimens underwent retention testing with a Universal Instron machine. Pull-off forces (N) and modes of failure were registered. Statistical analysis was performed using Mann-Whitney U tests with Bonferroni corrections for multiple tests (α = 0.05). The median retention force values were 233.27 ±79.28 N for Group Control, 398.59 ±68.59 N for Group MP, 303.21 ±116.80 N for Group AMP, 349.31 ±167.73 N for Group CMP, and 219.85 ± 55.88 N for Group AP. The pull-off forces were significantly greater for Group MP, while the differences between the remaining groups were not statistically significant (P > 0.05). Group AP showed the lowest retention force values among all the groups. Failure modes after the pull-off testing were predominantly adhesive and substrate failure of the AM interim material. The surface treatment of the intaglio AM crown tested significantly influenced the retention force values measured. Pre-treatment with an MDP-containing silane improved the retentive force values computed, whereas pre-treatment with 50-μm Al2O3 air-particle abrasion alone is not recommended prior to cementation on a titanium-based implant abutment.

Comparative Analysis of the Fracture Resistance of a Polymeric Material for 3D Printing and a Milled Polymethylmethacrylate Material as Interim Material for Fixed Partial Dentures: New Material Updated

The aim of this study was to evaluate and compare the fracture resistance of a temporary three-unit fixed dental prosthesis (FDP) made of a new polymeric material obtained by an additive technique (3DPP) using a computer-aided design and manufacturing (CAD/CAM) system, comparing the prosthesis to the respective outcomes of temporary polymethylmethacrylate (PMMA) FDPs obtained by a subtractive technique (milling). Methods: Three-unit FDPs were 3D printed using a polymeric material (n = 20) or milled using polymethylmethacrylate (n = 20). After thermocycling at 5000 cycles at extreme temperatures of 5 °C and 55 °C in distilled water, each specimen was subjected to a compression test on a universal testing machine at a rate of 0.5 mm/min until failure occurred, recording the value in newtons (N). Results: There were statistically significant differences (p-value &lt; 0.005) between the PMMA material (2104.7 N; SD = 178.97 N) and 3DPP (1000.8 N; SD = 196.4 N). Conclusions: The fracture resistance of the PDFs manufactured from milled PMMA showed higher values for fracture resistance. However, the resistance of the 3DPP showed acceptable values under mechanical load; this notable advance in the resistance of printed materials consolidates them as an important alternative to use in interim indirect restorations.

Konvansiyonel, CAD/CAM frezeleme ve 3D baskı yöntemleriyle üretilmiş geçici materyallerin yüzey özelliklerinin Streptococcus mutans ve Candida albicans tutunumuna etkileri

Objectives: The purpose of this in vitro study was to compare conventionally manufactured, CAD/CAM milled, and 3D-printed interim materials based on their susceptibility to adherence of Streptococcus mutans and Candida albicans, and examine the influence of surface roughness and hydrophobicity. Materials and Methods: Eighty disc-shaped specimens fabricated from autopolymerized polymethyl methacrylate (A-PMMA), bis-acryl composite (Bis-acrylate), CAD/CAM PMMA-based polymer (Milled-PMMA), and 3D-printed resin (Printed) were subjected to 10,000 thermal cycles (5-55 °C) and divided into two groups (n=10) according to microbial suspension used: Streptococcus mutans and Candida albicans. Surface roughness (Ra) and hydrophobicity (WCA) of specimens were measured. An adhesion test was performed by incubating the specimens in Streptococcus mutans and Candida albicans suspensions at 37 °C for 24 hours, and the adherent cells were evaluated by counting colony-forming units (CFU/ml). Scanning electron microscopy (SEM) was performed to analyze the surfaces (n=2). Data were analyzed with Kruskal-Wallis and Mann-Whitney U tests. Spearman’s correlation analysis was used to determine correlation among the measurements (α=.05). Results: Type of restorative material significantly influenced Ra and WCA. The highest adhesion of Streptococcus mutans was observed in Printed, followed by Bis-acrylate, A-PMMA, and Milled-PMMA (p=.001). The highest adhesion of Candida albicans was noted on A-PMMA, followed by Printed, Bis-acrylate, and Milled-PMMA (r=.001). The adhesion of Streptococcus mutans (r=.660) and Candida albicans (r=.413) showed a positive correlation with Ra. A negative correlation was found between WCA of the materials and Streptococcus mutans adhesion (r=-.373). Conclusions: Surface roughness plays an important role in the adherence of microorganisms. CAD/CAM PMMA-based polymers may be a better choice to reduce microbial adhesion in long-term use.

Effect of hydrogen peroxide-based bleaching agents on the color dimensions and surface roughness of different milled restorative dental materials.

To compare the color dimensions, color discrepancies (ΔE00), and surface roughness of milled materials before and after the application of a bleaching agent. A total of 10 extracted molars were obtained. Each tooth was cut in transversal sections, to create discs (3 mm thick, 10 mm diameter) (control group). Disk specimens of 8 materials were fabricated: polymethyl methacrylate (PMMA) interim material (PMMA-Telio group), 2 resin nanoceramics: (RNC-Ultimate group) and (RNC-Cerasmart group), 2 hybrid ceramics: (HC-Shofu group) and (HC-Enamic group), lithium disilicate (LD-Emax group), zirconia reinforced glass ceramic (ZGC-Suprinity group), and zirconia (Zr group) (n=10). Color measurements were obtained using a spectrophotometer before and after applying 35% hydrogen peroxide-based bleaching agent. Pre- and post-bleaching surface roughness analysis were completed using a profilometer. Significant L*, a*, b*, and ΔE00 values differences were found (P < .05). Color discrepancies (ΔE00) ranged from 0.30 ± 0.14 to 4.82 ± 0.10. The highest color discrepancies were measured on the PMMA-Telio group, while the lowest color discrepancies were computed on the ZGC-Suprinity, RNC-Ultimate, and RNC-Cerasmart. Significant surface roughness differences were found (P <.05). The largest increase of surface roughness values between the pre- and post-bleaching measurements was obtained in the PMMA-Telio group with a mean ΔSa value of 4.73 ± 3.02, while the largest decrease of surface roughness values between the pre- and post-bleaching measurements was obtained in the Zr-InCeram group with a mean ΔSa value of -1.58 ± 0.10. The milled materials tested showed significant pre- and post-bleaching color and surface roughness discrepancies. Int J Prosthodont. doi: 10.11607/ijp.8359.

Mechanical properties of CAD/CAM polylactic acid as a material for interim restoration

Statement of problemBiomaterials, including polymethyl methacrylate (PMMA) and bisacrylate, have been widely used as conventional interim materials and may exhibit cytotoxicity or systemic toxicity. PurposeThis study was designed to compare the mechanical properties of polylactic acid (PLA) as an alternative to conventional dental polymers for computer-aided design and manufacturing (CAD/CAM). Material and methodsFour groups (n = 20 per group) of CAD/CAM polymers were assessed. Specimens of PLA (PLA Mill) and PMMA (PMMA Mill) for subtractive manufacturing, PLA for fused deposition modeling (PLA FDM), and bisphenol for additive manufacturing by stereolithography (Bisphenol SLA) were fabricated into 2-mm-wide, 2-mm-thick and 25-mm-long specimens using a milling machine, an FDM printer, and an SLA printer, respectively.The flexural strength (FS) and elastic modulus (EM) were calculated. The surface roughness and Shore D hardness were analyzed with a 3D optical surface roughness analyzer and a Shore durometer, respectively. ResultsPLA Mill showed the lowest FS (64.9 ± 8.28), followed by PLA FDM (104.27 ± 4.42 MPa), PMMA Mill (139.2 ± 20.95 MPa), and Bisphenol SLA (171.56 ± 15.38 MPa), with statistically significant differences. PLA FDM showed the highest EM, followed by PLA Mill, Bisphenol SLA, and PMMA Mill. Significant differences were observed not only between PMMA Mill and Bisphenol SLA but also between PLA FDM and PLA Mill. The lowest Shore D hardness was observed for PLA FDM, followed by PLA Mill, PMMA Mill, and Bisphenol SLA, which showed the highest value among the 4 groups, with significance. The highest values for the surface roughness parameters were observed for PLA Mill, and the lowest were observed for Bisphenol SLA. ConclusionsAmong the tested CAD/CAM polymers, Bisphenol SLA was the most durable material, and the mechanical properties of PLA FDM were within the clinically acceptable range.

Fracture load of 4-unit interim fixed partial dentures using 3D-printed and traditionally manufactured materials

Statement of problemHow the fracture strength of recently introduced 3-dimensionally (3D) printed interim materials compares with that of conventional materials is unclear. PurposeThe purpose of this in vitro study was to compare the fracture load of 4-unit interim fixed partial dentures made from 3 different materials before and after mastication simulation. Material and methodsBased on a master model of a 4-unit fixed partial denture with maxillary left first premolar and second molar abutment teeth, interim restorations were fabricated from 3 different materials (3D-printed, Temporary CB Resin, milled, PMMA for brain, and manually manufactured, Luxatemp Plus). The fixed partial dentures (n=30 for each material) were cemented on 3D-printed model abutment teeth that were connected via a thin latex layer to a polyurethane base block. The fracture load of 15 fixed partial dentures of each material was tested without aging. Another 15 fixed partial dentures of each material were tested after thermomechanical aging. ResultsThe mean fracture load was between 186 N and 661 N, and all materials showed significant lower fracture loads after aging. Before and after aging (before/after ±standard deviation) milled (661 ±59/568 ±52 N) achieved the highest loads before manually manufactured (621 ±100/478 ±96 N) and 3D-printed (294 ±83/186 ±70). ConclusionsThe 3D-printed interim restoration material and the inherent manufacturing process show significant lower fracture loads than the tested alternatives. However, as the influence of geometric differences could not be quantified, whether this remains true after correcting for geometric differences remains unclear. For the tested interim materials, thermocycling and mastication simulation significantly reduced fracture loads over time, even at loads as low as 50 N.

Influences of Toothbrushing and Different Toothpastes on the Surface Roughness and Color Stability of Interim Prosthodontic Materials.

The surface properties and color stability of interim crown materials may vary depending on the toothbrushing procedure. This study aimed to investigate the effects of toothbrushing and different toothpastes on the surface roughness (Ra) and color stability of different interim crown materials. Disc-shaped specimens were prepared from four interim crown materials (Tab 2000 (ChPM), Imident (LaPM), Protemp 4 (ChDM), and Telio-CAD (CadPM)). Specimens were divided into four subgroups for the control group (Cnt) and for simulated toothbrushing with distilled water (Dw) or with two different toothpastes (whitening toothpaste (WTp), activated charcoal toothpaste (ACTp)). The specimens’ Ra values were measured before and after 10,000 cycles of toothbrushing. The color parameters were measured and the color differences (ΔE00) were calculated. Data were statistically analyzed by two-way analysis of variance (ANOVA) and Tukey’s HSD tests. A significant increase in the Ra values was observed after toothbrushing, except for the LaPM_Dw, ChDM_Dw, and all the CadPM specimens (p < 0.05). Toothbrushing with toothpastes increased the ΔE00 values of all ChPM and ChDM interim materials (p < 0.05). Before and after all toothbrushing procedures, the CadPM specimens had smoother and ChPM specimens had rougher surfaces than the other interim materials. The two tested toothpastes had similar effects on the Ra of all interim materials. Non-perceivable color changes were seen only with the CadPM_Dw group.

Flexural strength of aged and nonaged interim materials fabricated by using milling, additive manufacturing, and a combination of subtractive and additive methods

Statement of problemInterim dental restorations can be fabricated from additively manufactured ingots. However, the flexural strength and surface roughness of restorations fabricated by using this technique are unknown. PurposeThe purpose of this in vitro study was to assess the influence of the manufacturing method (milling, additive manufacturing, or a combination of subtractive and additive methods) and accelerating aging on the flexural strength and surface roughness of interim dental materials. Material and methodsA bar design (25×2×2 mm) was used to fabricate the specimens by using 3 methods: milling (M group), additive manufacturing (AM group), and a combination of subtractive and additive methods (AM+M group). In the M group, an interim material (CopraTemp PMMA) was used to fabricate the milled (350i imes-icore) specimens. In the AM group, specimens were fabricated by using a printer (Form3B+) and an interim resin (Temporary CB) according to the manufacturer’s protocol. In the AM+M group, specimens were milled from AM ingots (Temporary CB) and with the same milling machine as in the M group. Two subgroups were created based on the artificial aging (thermocycling): nonaged and aged (n=10). Flexural strength was calculated by using a universal testing machine, followed by determination of the Weibull distribution. Surface roughness was measured by using a digital microscope. The Shapiro-Wilk test revealed that the flexural strength and surface roughness (Ra) data were normally distributed (P>.05). Two-way ANOVA followed by post hoc multiple comparison Tukey tests were used to examine the data (α=.05). The Shapiro-Wilk test revealed that the surface roughness area data were not normally distributed (P<.05). Therefore, the Kruskal-Wallis followed by pairwise multiple comparisons tests were selected (α=.05). ResultsManufacturing methods (P<.001) and artificial aging (P=.043) were significant factors in the flexural strength measured. The M group had the highest flexural strength mean values (180 MPa), while the AM group showed the lowest flexural strength mean values (77 MPa). Additionally, nonaged specimens (128 MPa) had significantly higher flexural strength values than aged specimens (117 MPa). Manufacturing method (P<.001) was a significant factor in the surface roughness measured. The M group had the highest linear surface roughness mean values (0.86 μm), while the AM group showed the lowest linear surface roughness mean values (0.49 μm). ConclusionsManufacturing method and thermocycling influenced the flexural strength and surface roughness of the groups tested.

Color and surface stainability of additively and subtractively manufactured interim restorative materials against mouth rinses

Statement of problemInterim restorations are often used along with mouth rinses during the healing period following surgical procedures. However, evidence regarding the color and surface properties of digitally fabricated interim restorations after oral rinsing is lacking. PurposeThe purpose of this in vitro study was to evaluate whether different mouth rinses could affect the color and surface roughness of milled and printed interim restorations after simulated oral rinsing. Material and methodsDisk-shaped specimens (Ø15×2 mm; N=180) were fabricated by using conventional (Jet Tooth Shade), milled (Yamahachi PMMA Disk), and printed (NextDent C&B) resin materials. All resin specimens were divided into 3 different groups according to the rinsing material: distilled water, whitening mouth rinse (Listerine Healthy White), and conventional mouth rinse (Listerine Cool Mint). The specimens were further allocated into short- and long-term subgroups, and oral rinsing simulation was performed (n=10). Short-term rinsing simulated the conditions in a usual interim restoration period, and long-term rinsing was performed to evaluate the properties of the interim materials. The color differences (CIEDE2000, ΔE00) between the baseline and each time point were determined by using a spectrophotometer. The surface roughness of the tested specimens was measured by using a confocal laser scanning microscope. Kruskal-Wallis and Friedman tests with nonparametric pairwise comparisons were used to analyze the data (α=.05). ResultsOn simulation of a 6-month use of the mouth rinse, the color change in the milled resin did not differ from that in the conventional resin (P>.334), but the printed resin showed a significantly greater color change than the other resins (P<.007). The greatest color change with the printed resin was observed when a conventional mouth rinse was used. However, all color changes were below a perceptible threshold of 1.30. When daily rinsing for 14 years was simulated, all resin groups showed a perceptible color change when conventional mouth rinse was used, and the printed resin showed the greatest median ±interquartile range ΔE00 (2.24 ±0.2). In both short- and long-term simulations, the printed resin rinsed with the conventional mouth rinse showed significantly greater roughness than that rinsed with distilled water (P<.009). ConclusionsThe printed resin showed higher stainability than the conventional resin, and the color change was greatest with the conventional mouth rinse. However, in 6 months of daily mouth rinse simulation, all the tested resin materials exhibited imperceptible color change and clinically acceptable surface roughness.

Influence of postprocessing rinsing solutions and duration on flexural strength of aged and nonaged additively manufactured interim dental material

Statement of problemAdditive manufacturing procedures for fabricating interim restorations include rinsing postprocessing procedures. However, the impact of different rinsing solutions and times on flexural strength is unknown. PurposeThe purpose of this in vitro study was to assess the influence of the rinsing solutions and duration, as well as accelerated aging (thermocycling) procedures, on the flexural strength and Weibull characteristics of an additively manufactured interim dental material. Material and methodsA bar design (25×2×2 mm) file was used to fabricate all the specimens with 3D printing and an interim material (Nextdent C&B MFH). Five groups were created based on the rinsing solution used during the postprocessing procedures: 91% isopropyl alcohol (IPA) (control or IPA-91), 99% IPA (IPA-99 group), bio-ethyl alcohol 100% (BE group), tripropylene glycol monomethyl ether (TPM) 100% (TPM group), and water miscible formula (Resinaway) (RA group). Each group was divided into 4 subgroups depending on the total rinsing time: 5, 6, 7, and 8 minutes (5, 6, 7, and 8 subgroups). Additionally, each subgroup was distributed between nonaged and aged thermocycling procedures (n=10). Flexural strength measurements were made by using a universal testing machine. Two-parameter Weibull distribution values, including the Weibull modulus, scale (m), and shape (0), were calculated. Three-way ANOVA and pairwise multiple comparison Tukey tests were used to analyze the data (α=.05). ResultsThree-way ANOVA showed that the rinsing solution (P<.001), rinsing time (P=.004), and thermocycling procedures (P<.001) were significant predictors of the flexural strength values obtained. The IPA-91 and IPA-99 groups obtained the highest flexural strength, while the RA, TPM, and BE groups obtained the lowest flexural strength. The 7- and 8-minute subgroups obtained the highest flexural strength, while the 5-minute subgroup obtained the lowest flexural strength. The nonaged specimens obtained significantly higher mean flexural strength values than the aged specimens. ConclusionsThe vat-polymerized additively manufactured interim dental material tested with differing rinsing solutions and times demonstrated significant differences in the flexural strength values measured. Accelerated artificial aging procedures significantly decreased the flexural strength of the vat-polymerized interim dental material tested.

Influence of definitive and interim restorative materials and surface finishing on the scanning accuracy of an intraoral scanner

PurposeTo analyze the influence of the restorative material type (definitive and interim) and its surface treatment (polished or glazed) on the scanning accuracy of an intraoral scanner. Material and methodsA mandibular dental typodont containing 3 typodont teeth (left second premolar and left first and second molars) was used for testing. Ten groups were created based on the crown material: typodont tooth (control group), gold (G group), zirconia (Z group), lithium disilicate (LD group), hybrid ceramic (HC group), composite resin (CR group), conventional PMMA (CNV-PMMA group), bis-acryl composite resin (CNV-BA group), milled PMMA (M-PMMA group), and additively manufactured bis-acryl-based polymer (AM-BA group). Except the G group, groups were subdivided into polished (P subgroups) or glazed (G subgroups). Each specimen was digitized by using an extraoral scanner (D1000; 3Shape A/G) and an intraoral scanner (TRIOS 4; 3Shape). Each reference scan was used to measure the discrepancy with the corresponding 15 intraoral scans by calculating the root mean square (RMS) error (Geomagic; 3D Systems). The Welch ANOVA and Games-Howell tests were selected to examine trueness (α=0.05). The F-test with Bonferroni correction was used to evaluate precision. ResultsSignificant trueness and precision differences were found (P<.001). The G-P subgroup had the lowest trueness values, while the CNV-PMMA-P, M-PMMA-P, and AM-BA-P subgroups had the highest trueness values. Significant RMS mean discrepancies were computed when comparing polished and glazed specimens fabricated with the same material (P<.001). The CNV-PMMA-G subgroup had the lowest precision values, while the CNV-BA-P subgroup had the highest precision values (P<.001). ConclusionsThe type and surface finishing of the restorative materials tested influenced the scanning accuracy of the IOS tested. The lowest trueness values were found in the high noble alloy specimens, while the highest trueness values were measured in conventional and milled PMMA and additively manufactured bis-acryl-based polymer polished specimens. Except for zirconia crowns, higher trueness values were found in polished specimens when compared with glazed crowns. The CNV-PMMA-G subgroup had the lowest precision values, while the highest precision values were measured in the CNV-BA-P subgroup. CLINICAL SIGNIFICANCEDefinitive and interim materials tested decrease intraoral scanning accuracy. Furthermore, polishing instead of glazing definitive and interim material assessed might be preferable to maximize intraoral scanning accuracy.