Granite Types Research Articles

Natural Radioactivity, Radiological Hazard and Petrographical Studies on Aswan Granites Used as Building Materials in Egypt

The present study was carried out on commercial types of Aswan granite used as building and decorative materials. Nearly 29 granitic rocks samples from 11 classes (black Aswan, red Aswan, dark Rosa, light Rosa, yellow Verdi, grey Shirka, Gandolla, Forsan, red Nefertiti, Royal, and white Halayeb) were collected from three stations near Aswan city for petrographical description and assessment of natural radioactivity. The petrographical study of granites was conducted by polarized-light microscope in order to determine their mineralogical composition and investigate their texture; the activity of the natural radionuclides 238U, Ra226, 232Th, and 40K was measured by gamma-ray spectrometry with a NaI(Tl) detector. The average values of the activities, 52.2 Bq kg−1, 57.8 Bq kg−1, 31.2 Bq kg−1, and 1055.7 Bq kg−1 of U-238, Th-232, Ra-226, and K-40, respectively, were higher than that the world average values of 35 Bq kg−1, 30 Bq kg−1 and 400 Bq kg−1 for 226Ra, 232Th, and 40K, respectively, according to the recommended levels from UNSCEAR reports. The minimum and maximum values obtained were compared with the value ranges from other locations in the Eastern Desert, highlighting the fact that that the maximum values obtained in this work are higher than those in other areas. According to the radiological hazards indices results, most samples lie in the permissible level ranges, suggesting their favorability for use as building materials. In contrast to that, some samples have some environmental parameters higher than the international levels, indicating their unsuitability as building materials.

A laboratory approach on the combined effects of granite bioreceptivity and parameters modified by climate change on the development of subaerial biofilms on cultural heritage

Conservation of cultural heritage buildings and monuments may be negatively affected by the impact of climate change on substrates and colonizing microorganisms. In this study, four types of commercial granite, in which the bioreceptivity ranged from very low to very high, were inoculated with a multispecies microbial culture and exposed to different temperatures (18 and 24 °C) and levels of water availability (1 day, 3 days and 7 days of water availability/week) to simulate different climatic conditions. The effects on biofilm formation of the interactions between the substrate bioreceptivity and the environmental parameters were investigated. Biofilm growth and photosynthetic efficiency were monitored over 42 days by pulse-amplitude modulated (PAM) fluorometry and spectrophotometric colour measurement. The primary bioreceptivity of the granite was a determining factor in the organisms' capacity to attach to the substrate and interacted through the experiment with the climatic conditions by modifying the development of the microorganisms. Water availability was a limiting factor for the colonizing microorganisms, in terms of both growth and photosynthetic efficiency. At the higher temperature, metabolic reactions were enhanced under water restriction (but not under maximum water availability) and the microbial ecology was altered, leading to a higher proportion of cyanobacteria relative to algae.

Geochemical behavior of rare metals and high field strength elements during granitic magma differentiation: A record from the Borong and Malashan Gneiss Domes, Tethyan Himalaya, southern Tibet

In the Borong Gneiss Dome and Malashan Gneiss Dome within the Tethyan Himalaya, zircon UPb ages and whole-rock geochemical data demonstrate that at least two episodes of leucogranite formed at 19.8–19.4 Ma and 18.6–18.5 Ma, respectively. Each of them contains at least two suites of granite: two-mica granite and garnet-bearing leucogranite. Although the two types of granites are characterized by distinct element geochemistry and mineral compositions, they show similar Sr-Nd-Hf isotope ratios and regular variations in the compositions of whole-rock elements. From two-mica granite to garnet-bearing leucogranite, SiO2, Na2O, Rb, Nb, and Ta contents and Rb/Sr ratios increase; in contrast, Al2O3, CaO, MgO, FeO, TiO2, Sr, Ba, Eu, Zr, U, Th, light rare earth elements (LREEs) and Sc contents, as well as Zr/Hf and Nb/Ta ratios, decrease. Such systematic variations imply that two-mica granite and garnet-bearing leucogranite are cogenetic and that two-mica granite represents the more primary melt, whereas garnet-bearing leucogranite is a more evolved melt. During granitic magma evolution, fractional crystallization induces substantial changes in the melt structure and in turn major changes in the dissolution behavior of accessory phases (e.g., zircon, monazite, and apatite) and the geochemistry of key trace elements. Such changes might be the key factors that resulted in the subordinate W-Sn-Nb-Ta-Be anomalies in the more evolved granites, which implies that the Himalayan Cenozoic leucogranites have high potential to produce economic rare metal deposits.

Origin of S-, A- and I-Type Granites: Petrogenetic Evidence from Whole Rock Th/U Ratio Variations

The origin and evolution of granites remain a matter of debate and several approaches have been made to distinguish between different granite types. Overall, granite classification schemes based on element concentrations and ratios, tectonic settings or the source rocks (I-, A-, S-type) are widely used, but so far, no systematic large-scale study on Th/U ratio variations in granites based on their source or tectonic setting has been carried out, even though these elements show very similar behavior during melting and subsequent processes. We therefore present a compiled study, demonstrating an easy approach to differentiate between S-, A- and I-type granites using Th and U concentrations and ratios measured with a portable gamma ray spectrometer. Th and U concentrations from 472 measurements in S- and I-type granites from the Variscan West-Bohemian Massif, Germany, and 78 measurements from Neoproterozoic A-type Malani granites, India, are evaluated. Our compendium shows significant differences in the average Th/U ratios of A-, I- and S-type granites and thus gives information about the source rock and can be used as an easy classification scheme. Considering all data from the studied A-, I- and S-type granites, Th/U ratios increase with rising Th concentrations. A-type granites have the highest Th/U ratios and high Th concentrations, followed by I-type granites. Th/U ratios in S- to I-type granites are lower than in A-type and I-type granites, but higher than in S-type granites. The variation of Th/U ratios in all three types of granite cannot be explained by fractional crystallization of monazite, zircon and other Th and U bearing minerals alone, but are mainly due to source heterogeneities and uranium mobilization processes.

Density heterogeneity of the Earth’s crust of Ukraine and adjacent territories from three-dimensional gravity modelling

The work was performed to study the density heterogeneity of the crust of Ukraine and adjacent regions analyzing detailed 3D gravity models of the following tectonic regions and separate structures: Dnieper-Donets Basin and Donbas, Ingulsky megablock, Golovanivska suture zone, latitudinal zones of fractures of the Ukrainian Shield, Black Sea megadepression and surrounding areas. The models are constructed on the basis of geological, petrophysical and seismic data along geotravers, DSS profiles, the modern WARR methodsand are calculated using the automated software complex for interpretation of potential fields GMT-Auto. As a result, new information was obtained for the density distribution in the whole Earth’s crust.The density distributions construct for the entire crust of Ukraine and adjacent regions at certain depths (surface of the basement, 10, 20, 30 km, Moho discontinuity). The thickness was determined for conditionally distinguished «granite», «diorite», «basalt» layers of the Earth’s crust and crust-mantle mixture within the whole region of the study. Its values are graphically represented by isolines on the respective schematical maps. The resulting density inhomogeneity became the basis for constructing, for the first time in a three-dimensional version, a scheme for the predictive composition of the Earth’s crust with typification according to the power ratios of its constituent layers. The heterogeneity of the present-day consolidated crust of the whole study area is characterized by granitic, granitic-dioritic, dioritic and basaltoid types. To clearly identify the dismemberment of the lower layer of the crust which is considered inseparable by the classification of the DSS method the basaltoid type is divided into 3 subtypes. The subtype 1 with a content of 40—70 % of basalt, subtype 2, where concent-ration of basalt increases to 70—90 % and subtype 3, which is composed only of basalt.It has been established that the basicity of the Earth’s crust of the USh changes from west to east, respectively, from basalt to diorite type. Decrease in crustal basicity is also observed in suture zones, namely from diorite and basaltoid typein Golovanivskii suture to basaltoid and diorite type in the Inguletsko-Kryvorizckii suture and diorite type in the Orikhivsko-Pavlogradskii suture. In the DDB the crustal basicity increases from northwest to southeast in accordance with the segmentation of this feature. The basaltoid type of the crust is predominant in the Black Sea megadepression and adjacent territories. For the first time, a type of crust was identified that does not coincide with the known ones and is characterized by the presence in the section of the «basalt» and «granite» layers (with a zero or very low «diorite» thickness). A similar type of bark is present in the Ingul megablock of the USh, in the northern side zone of the DDB, as well as in the Black Sea megadepression.

Effect of particle size and composition of granitic sands on the radiological behaviour of mortars

Although primarily deemed to be an ornamental stone, granite may also be ground into fines for use in cement mortars, where it exhibits high strength and durability. Both the 40K present in the stone and the natural decay series of its uranium, thorium and actinium components exhibit high activity concentrations. An understanding is therefore needed of the correlation among the different particle sizes in granite aggregate to assess their contribution to a mortar's activity concentration index (ACI). This study analyses the variation in ACI with particle size in three types of granite based on the chemical, mineralogical and radiological characterisation of five size fractions. The activity concentrations of the thorium and uranium natural decay series were highest in the finest fractions. A correlation was observed between thorium and the MgO and Fe2O3 normally present in mica group phyllosilicates. In two of the three granites, the mortars prepared with the smallest size particles had ACI values >1.

Statherian (ca. 1714–1680 Ma) Extension-Related Magmatism and Deformation in the Southwestern Korean Peninsula and Its Geological Significance: Constraints from the Petrological, Structural, Geochemical and Geochronological Studies of Newly Identified Granitoids

In this study, petrological, structural, geochemical, and geochronological analyses of the Statherian alkali feldspar granite and porphyritic alkali feldspar granite in the southwestern part of the Korean Peninsula were conducted to examine petrogenesis of the granitoids and their tectonic setting. Zircon U-Pb dating revealed that the two granites formed around 1.71 Ga and 1.70–1.68 Ga, respectively. The results of the geochemical analyses showed that both of the granites have a high content of K2O, Nb, Ta, and Y, as well as high FeOt/MgO and Ga/Al ratios. Both granites have alkali-calcic characteristics with a ferroan composition, indicating an A-type affinity. Zircon Lu-Hf isotopic compositions yielded negative εHf(t) values (−3.5 to −10.6), indicating a derivation from ancient crustal materials. Both granite types underwent ductile deformation and exhibited a dextral sense of shear with a minor extension component. Based on field relationships and zircon U-Pb dating, it was considered that the deformation event postdated the emplacement of the alkali feldspar granite and terminated soon after the emplacement of the porphyritic alkali feldspar granite in an extensional setting. These data indicated that there were extension-related magmatic activities accompanying ductile deformation in the southwestern part of the Korean Peninsula during 1.71–1.68 Ga. The Statherian extension-related events are well correlated with those in the midwestern part of the Korean and eastern parts of the North China Craton.

Geochemistry, origin and anatexis temperature of monzogranite formation in Mount Khalaj (Mashhad, Iran)

Geochemistry, origin and anatexis temperature of monzogranite formation in Mount Khalaj (Mashhad, Iran)

Rare Earth Element and Incompatible Trace Element Abundances in Emeralds Reveal Their Formation Environments

Emeralds require the unusual association of typically compatible elements (Cr, V), with incompatible Be to form, and occur in complex tectonic settings associated with sediments (type IIB; Colombia) or, more commonly, with magmatism and regional metamorphism (IA). Precise rare earth element (REE) and incompatible trace element abundances are reported for a global suite of emeralds, enabling the identification of the environments in which they formed. Type IIB emeralds have nearly flat continental crust normalized REE patterns (La/YbCC = ~2), consistent with a sedimentary source origin. Type IA emerald REE patterns have upturns in the heavy REE (La/YbCC = ~0.3), a feature also shared with South African emeralds occurring in Archaean host rocks. Modeling of type IA emerald compositions indicates that they form from magmatic fluids of sedimentary (S)-type granite melts interacting with Cr, V-rich mafic–ultramafic crustal protoliths. This geochemical signature links emerald formation with continental suture zones. Diamonds, rubies, and sapphires have been considered as ‘plate tectonic gemstones’ based on mineral inclusions within them, or associations with plate tectonic indicators. Emeralds are distinct plate tectonic gemstones, recording geochemical evidence for origin within their mineral structure, and indicating that plate tectonic processes have led to emerald deposit formation since at least the Archaean.

Age, origin and tectonic implications of Late Carboniferous-Early Permian felsic magmatic rocks from central Inner Mongolia, south-eastern Central Asian Orogenic Belt

ABSTRACT Permo-Carboniferous felsic magmatic rocks are widely exposed on the northern half of the south-eastern Central Asian Orogenic Belt. However, their origin and spatiotemporal distribution are unknown. Herein, zircon U-Pb-Hf isotopic data, major and trace element compositions of the whole-rock, and Sr-Nd isotopic data derived for felsic volcanic rocks and granites of the Chaganaobao and Baiyinaobao areas in central Inner Mongolia are combined with the data from previous studies. The integration of these results reveals that the Uliastai Continental Margin, Erenhot-Hegenshan Ophiolite Belt, and Northern Orogenic Belt have coeval magmatic lull or trough at c. 307 Ma, which overlap with the closure timing of the Hegenshan Ocean. The Latest Carboniferous−Early Permian (c. 303−295 Ma) felsic volcanic rocks in the Chaganaobao area of the Uliastai Continental Margin comprise dacite, trachydacite, and rhyolite, while demonstrating positive whole-rock εNd(t) (+2.9 to +4.7) and zircon εHf(t) values (+7.65 to +13.78). Early Permian granites of the Baiyinaobao area located within the Northern Orogenic Belt show positive εHf(t) values (+ 2.70 to +11.33) and low TFe2O3 + MgO + TiO2 contents. The geochemical composition reveals that those felsic magmatic rocks mainly originate from the partial melting of juvenile crustal components with subordinate input of mantle-derived melts. Those c. 305−275 Ma felsic magmatic rocks from the north of the south-eastern Central Asian Orogenic Belt exhibit affinities of post-collision type granites in geochemical nature. Therefore, the flare-up of the Early Permian magmatism surrounding the Erenhot-Hegenshan Ophiolite Belt could be related to the extension after the final closure of the Hegenshan Ocean.

Geochemistry of apatites from Mesozoic granitoids in the northeastern North China Craton and their petrogenetic implications

We report geochemical data of apatites from Mesozoic granitoids in the northeastern North China Craton (NCC), and discuss the relationship between apatite and whole-rock compositions with the aim of using apatite geochemical data to constrain granitoid petrogenesis. Measured Sr contents and Sr/Y ratios of apatites exhibit positive correlations with those of their host rocks, and εNd(t) values of apatites display a strong linear relationship with εHf(t) values of zircons in the granitoids. In addition, apatites exhibit similar rare-earth element (REE) distribution patterns with their host rocks, although apatites have much higher REE contents. Sr/Y–Y variation diagram for apatite is proposed to distinguish adakitic rock from non-adakitic. The REE patterns of apatites, together with other geochemical indexes, can also be used to discriminate highly fractionated granitoids from unfractionated I-type granite or other type granite. The geochemical and Nd isotopic compositions of apatites have well revealed the magma source of Mesozoic granitoids in the northeastern NCC. In conclusion, we highlight that apatite geochemistry reflects the whole-rock geochemical characteristics of granitoids and has the potential to track granite detritus.

Zircon U–Pb geochronology, Hf isotope composition, and petrochemical characteristics of Paleocene granitoids in the western Gangdese Belt, Tibet

Abstract —The research team studied the petrology, whole-rock geochemistry, zircon U–Pb age, and stable isotopic characteristics of the Rongguo Longba and Garongcuo granites of the Nuocang area to understand better the impact of Neo-Tethys ocean subduction and In-dia–Eurasia continental collision on Paleocene tectonomagmatic processes along the southern margin of the Gangdese Belt. The Rongguo Longba granite and Garongcuo granite porphyry formed at 61.86 and 62.17 Ma, respectively. The Nuocang granitoids are characterized by (1) high SiO2, NaO2, and Al2O3 contents and low FeOtot, MgO, and TiO2 contents; (2) LREE and LILE enrichment and HREE and HFSE (Nb, P, and Ti) depletion; and (3) obvious negative Eu anomalies. These features indicate that the Nuocang granites are of the high-K calc-alkaline and peraluminous granite types. Furthermore, their zircon Hf isotope characteristics suggest that the magma source region has an ancient crystalline basement. The basaltic andesitic crystal tuff is the product of garnet–peridotite partial melting and crust contamination from rising magma emplacement.

Discovery of multi-crustal rejuvenations for the formation of the Lincang granitic batholith, Southwest China: magmatism relating to Changning–Menglian Paleo–Tethyan termination

ABSTRACT The consumption of the Changning–Menglian Palaeo-Tethys ocean in the Triassic formed the Lincang granitic batholith in the southwestern China, once the oceanic supra-subduction zone. The batholith provides us a critical window to understand the nature of the crustal basements and the process of Palaeo-Tethyan termination. Here we report zircon U-Pb ages and Hf isotopes, and whole-rock elements and Sr-Nd isotopes of granitic samples from the central part of the Lincang batholith. The geochemical results reveal two genetic types of granites indicated by low-K and high-K affinities, respectively. The Group 1 low-K granitoids dated at 237–229 Ma are low-K calc-alkaline and metaluminous to peraluminous (A/CNK = 0.75–1.29), with K2O contents of 0.13–1.33 wt%, K2O/Na2O ratios of 0.03–0.30, Rb/Sr ratios < 0.18, and initial 87Sr/86Sr = 0.71693 and εNd(t) = −10.8. In contrast, the Group 2 high-K granitoids dated at 239–200 Ma are calc-alkaline and peraluminous (A/CNK = 1.02–1.20), with higher K2O contents (3.15–4.7 wt%), K2O/Na2O ratios (1.15–2.00) and Rb/Sr ratios (0.77–2.62), and more enriched isotopic compositions (initial 87Sr/86Sr = 0.73129 to 0.74037, εNd(t) = −13.1 to −11.0) as well as highly negative zircon εHf(t) values of −16.8 to −6.7. The formation time of these granitoids is compatible with that of the post-collision of the Palaeo-Tethys, subsequently to the magmatic gap (250–240 Ma) coupling with the syn-collision stage. The magmatic source discriminations suggest that the low-K granitoids were derived from partial melting of the dehydrated low-K amphibolite source and the high-K granitoids were dominantly from the psammitic source with minor mantle-derived magma involvement. Using the geochemical variations of the granitic rocks related to the Palaeo-Tethyan closure, we reveal melting of multiple crustal sources rather than a sole source to construct the Lincang batholith.

Petrogenesis of highly fractionated leucogranite in the Himalayas: The Early Miocene Cuonadong example

There has been considerable debate concerning the petrogenesis of Cenozoic highly felsic, strongly peraluminous, leucogranites within the Himalayan–Tibetan orogen, with two contrasting viewpoints regarding their origin, either as primary melts from parting melting or magmatic differentiation. This debate hampers our understanding of the tectono‐magmatic evolution and associated uplift and exhumation processes during Himalayan orogenesis. This study attempts to resolve this debate by means of an integrated petrographic, geochronological, and geochemical study on the Cenozoic Cuonadong leucogranites (including two‐mica granites, garnet‐bearing granites, and tourmaline‐bearing granites) in the eastern part of the south Himalayan–Tibetan orogen. One SHIRIMP zircon U–Pb dating of two‐mica granites and four LA–ICP–MS monazite U–Th–Pb dating of all three types of granites yield ages of ca. 21.9–19.7 Ma. Combined with previous published continuous U–Th–Pb zircon/monazite ages varying from 16.5 to 21.8 Ma, indicating that Cuonadong leucogranites have experienced continuously multiple episodes of intrusion and long‐term crystallization from ca.16 to 22 Ma, and lasted for ca. 6 Myrs. Major and trace element geochemistry combined with whole‐rock Sr–Nd isotope data suggest that the Cuonadong's three types of leucogranites are highly fractionated and garnet‐ and tourmaline‐bearing granites are more evolved. The Cuonadong leucogranite melts are mainly derived from metapelites within the High Himalayan Crystalline Sequence, and underwent fractional crystallization of biotite, monazite, and plagioclase during melt migration. This study indicates Cuonadong leucogranites are Cenozoic highly fractionated strongly peraluminous leucogranites, which, combined with previous intermittent documentations of fractionated leucogranites, point to an increasing maturation of the continental crust composition during continental orogenesis.

Impact of mine pit lake on metal mobility in groundwater

Open pit mines are potential source of metal contamination. Three types of open pit mines, i.e. copper, quartzite and granite were selected to understand the mobility and behaviour of metals. Metal contamination due to abandoned open pit copper mines (Average Cu = 64.57 ± 90 µg/L) is observed more comparative to quartzite (Average Cu = 20.42 ± 34.39 µg/L) and granite mines (Average Cu = 9.67 ± 7.94 µg/L). Acid mine drainage (AMD) from copper mines result in dissolution of metals and contaminates groundwater in the downstream direction. Correlation used for source assessment confirms the influence of anthropogenic or abandoned pit mine on metal concentration in groundwater. It is observed that the impact of abandoned pit mine is more compared to tailings and overburden dumps. Dissolution and precipitation process control the metal abundance in downstream groundwater. Precipitation dominates dissolution process with distance and results in decrease in metal concentration. It also confirms the self-neutralisation and self-attenuation capacity of the aquifer. The study recommends restoration of abandoned open pit mines to their natural conditions to avoid metal contamination in downstream.

Petrogenesis of Archaean granites in the Barberton region of South Africa as a guide to early crustal evolution

ABSTRACT The Barberton region of South Africa is characterized by a broad variety of granite types that range in age from ca. 3.5 Ga to 2.7 Ga and reflect the processes involved in the formation of Archaean continental crust on the Kaapvaal Craton. These granites are subdivided into three groups, as follows: A tonalite-trondhjemite-granodiorite (TTG) suite diapirically emplaced at 3 450 Ma and 3 250 Ma into pre-existing metamorphosed greenstone belt material. TTG melts were derived from melting amphibolite in the lower crust, with individual plutons being emplaced at various crustal levels. The dome-and-keel geometry that characterizes the TTG-greenstone dominated crust at this time is inconsistent with a plate tectonic domain and reworking was likely controlled by gravity inversion or ‘sagduction’; Regionally extensive potassic batholiths (the GMS suite) were emplaced at 3 110 Ma during a period of crustal thickening and melting of a TTG-dominated lower crust. Subsequent to emplacement of the voluminous GMS granites, the thickened continental crust had stabilized sufficiently for large sedimentary basins to form; Late granite plutons were emplaced along two distinct linear and sub-parallel arrays close to what might have been the edge of a Kaapvaal continent at 2 800 to 2 700 Ma. They are subdivided into high-Ca and low-Ca granites that resemble the I- and S-type granites of younger orogenic episodes. The high-Ca granites are consistent with derivation from older granitoids in the lower crust, whereas the low-Ca granites may have been derived by melting metasedimentary precursors in the lower-mid crust. Granites with similar characteristics are associated with a subduction zone in younger terranes, although the recognition of such a feature at Barberton remains unclear. The petrogenesis of granites in the Barberton region between 3.5 Ga and 2.7 Ga provides a record of the processes of Archaean crustal evolution and contributes to discussions related to the onset of plate tectonics.

Microstructural evolution of granitic stones exposed to different thermal regimes analysed by infrared thermography.

Detailed knowledge of the behaviour of rocks under thermal stress is essential in a variety of fields such as the exploitation of oil and mineral resources, the geothermal sector, the storage of radioactive liquid waste, or even CO 2 capture and storage. Granites are widely studied and exploited in these fields, and they show different reactions to high-temperature and thermal cycles due mainly to their high mineralogical and textural heterogeneity. One of the features that influences the most the thermal response is the porosity. The objective of this study is to evaluate the influence of porosity when these rocks are exposed to different thermal treatments. For that purpose, experiments were carried out on four granitoids selected by their similar crystal size, but with variable mineral proportion and porosity values, ranging from 1 to 6%. Two kinds of tests were performed: i) progressive heating cycles from 90 °C to 130 °C to determine the critical threshold for thermal damage; ii) thermal fatigue with cycles of heating-cooling up to 200 °C. The porosity and the water transport phenomena of the samples were characterised before and after each cycle by the monitoring of capillary water uptake coupled with infrared thermography. This technique allowed to follow the capillary fringe migration during the test and the evolution of the cooling rate index. The direct assessment of the damage was carried out by mercury injection porosimetry, optical polarising microscopy, and scanning electron microscopy. The combination of all the results permitted to establish a link between the evolution of temperature and the modification of porous networks in granitoids. Microcracks appeared distinctly at a temperature between 90 °C to 130 °C for high porosity granitoids whose Quartz/Feldspar ratio was close to 1. For higher temperatures, the low porosity granitoids develop microcracks from the first heating cycle. The porosity then showed a stronger impact on thermal behaviour than the effect of the mineralogy. The results obtained from infrared thermography allowed to detect the strong variations in the microstructure. • The initial heterogeneity of a granite generates a different cracking threshold for the same type of granite. • Repeated heating leads to increasing damage to rocks • The initial porosity and the quartz/feldspar ratio play a role in the thermal behaviour of granite. • Infrared thermography is a promising tool to detect microcracking.

The importance of sequential partial melting and fractional crystallization in the generation of syn-D3 Variscan two-mica granites from the Carrazeda de Ansiães area, northern Portugal

In the Carrazeda de Ansiães region, northern Portugal, a mesozonal granitic suite intruded Precambrian to Ordovician metasedimentary rocks during the late kinematic stages of the Variscan orogeny. In this multiphase granitic complex, consisting of ten granite types, the youngest group of two-mica granites (G7–G10) was emplaced between 318 ± 1 Ma and 316.2 ± 0.7 Ma, as determined by ID-TIMS U–Pb on zircon and monazite. Granite types G7–G9 were affected by the third phase of deformation (D3) before they were completely crystallized, as indicated by their internal NW–SE magmatic foliation concordant with the regional structures. The granite type G10 shows some distinctive textural features, showing a strong brittle deformation, probably due to its preferential emplacement in late NNE-SSW fault zones. Granites G7–G9 have equal or higher amounts of muscovite than biotite and contain surmicaceous enclaves, xenoliths, “schlieren”, and, more rarely, microgranular enclaves. The muscovite-dominant granite G10 does not contain enclaves. These Variscan granites are peraluminous, with ASI ranging between 1.22 and 1.39 and normative corundum of 2.79–4.39%, having the characteristics of S-type granites. In fact, the enrichment in LREE relatively to HREE, the negative Eu anomalies, and similar mean values of (87Sr/86Sr)i, εNdt and δ18O for G7 (0.7156 ± 0.0005; − 8.5; 11.49 ‰) and G8 (0.7155 ± 0.0007; − 8.4; 11.39 ‰) show that these two granite types resulted from sequential partial melting of the same metasedimentary material, where granite G8 would have derived from a higher degree of partial melting than G7. Granites G8–G10 and their minerals show a fractionation trend that is confirmed by modeling of major and trace elements. The subparallel REE patterns and the decreasing REE contents within the differentiation series, the Rb–Sr isochron for G8, G9 and G10 (315.5 ± 5.4 Ma; MSWD = 1.3) and the relatively uniform εNdt and δ18O data suggest that fractional crystallization was the main mechanism, which would have lasted less than 1 Ma. The tin-bearing granites G7 and G10 have ≥ 20 ppm Sn, but the main quartz veins containing cassiterite and wolframite cut granite G10, which contains 31 ppm Sn. Fractional crystallization was responsible for the increase in Sn content in granites from the G8–G10 series and their micas.

An Experimental Investigation of the Influence of Loading Rate on Rock Tensile Strength and Split Fracture Surface Morphology

To investigate the effect of the loading rate on the tensile strength of rock material and the morphology of the resulting split fracture surfaces, three types of rock specimens, namely, granite, basalt and limestone, were collected and tested with Brazilian testing under different loading rates. The tensile strength was measured, and the effect of the loading rate on the tensile strength of the rock material was studied. Digital terrain map models of the split fracture surface were obtained with an optical 3D scanning technique, and the effects of the loading rate on the geometry and morphology of the fracture surface were studied. The influence of the loading rate and tensile strength on the roughness was studied quantitatively by calculating the roughness indices of a fracture surface for all three kinds of rock. The research results show that the rock tensile strength increases with the loading rate. A linear relationship was established in double-logarithmic coordinates to describe the relationship between the tensile strength and the loading rate. Four different roughness indices were used to describe the morphology of the split fracture surface. The analysis results show that the magnitudes of all the roughness indices increase with the loading rate. Additionally, the roughness indices for all three types of rock linearly increase with the tensile strength. This linear trend indicates that it is possible to utilize fracture surface roughness indices to estimate rock tensile strength. The current study may motivate further research on the relationship between the morphology indices of rock fractures and mechanical parameters of the rock.

Fresh and hardened properties of high-strength concrete incorporating byproduct fine crushed aggregate as partial replacement of natural sand

This paper presents the fresh and hardened properties of high-strength concrete comprising byproduct fine crushed aggregates (FCAs) sourced from the crushing of three different types of rocks, namely granophyre, basalt, and granite. The lowest void contents of the combined fine aggregates were observed when 40% to 60% of natural sand is replaced by the FCAs. By the replacement of 40% FCAs, the slump and bleeding of concrete with a water-to-cement ratio of 0.45 decreased by approximately 15% and 50%, respectively, owing to the relatively high fines content of the FCAs. The 28 d compressive strength of concrete was 50 MPa when 40% FCAs were used. The slight decrease in tensile strength from the FCAs is attributed to the flakiness of the particles. The correlations between the splitting tensile and compressive strengths of normal concrete provided in the AS 3600 and ACI 318 design standards are applicable for concrete using the FCAs as partial replacement of sand. The maximum 56 d drying shrinkage is 520 microstrains, which is significantly less than the recommended limit of 1000 microstrains by AS 3600 for concrete. Therefore, the use of these byproduct FCAs can be considered as a sustainable alternative option for the production of high-strength green concrete.