The performance of scintillation detectors with the advanced scintillator material /sup 6/Li /sup 158/Gd (/sup 11/BO/sub 3/)/sub 3/ was compared with conventional /sup 3/He proportional counters at the IPNS spallation source at the Argonne National Laboratory, Argonne, IL. The complex neutron and gamma flux was measured with both detector types simultaneously in time-of-flight mode. Initial experiments demonstrated that both detectors have a sensitivity of about 60% for thermal neutrons. In addition, both detectors exhibited the same low gamma sensitivity.