Thermo-acoustic investigations require reliable measurement techniques in hot environments for pressure, density fluctuations with a high dynamic range and acoustic particle velocity. This paper presents recent developments of optical measurement techniques in combustion diagnostics. A fibre-optic microphone based on the interferometric detection of membrane deflections was designed to measure acoustic pressure oscillations. Due to the heat resistant design, the sensor has an upper temperature limitation of approximately 970 K. Rayleigh-Scattering measurements, using the density dependent intensity of scattered light were performed in an unconfined flame with approximately 1600 K to study amplitude and phase distribution of the flame pulsation. Acoustic particle velocity can be determined applying acoustic PIV (particle image velocimetry) technique. This paper shows a way to measure simultaneously the acoustic particle velocity and the locally resolved mean flow velocity of a turbulent flow. Together these non-invasive techniques are applicable to study thermo-acoustic processes and sound generation in combustion chambers or turbines.