Various methods have been developed for the preparation of MgO nanomaterials. However, they often suffer from limitations such as high cost, lengthy synthesis times, and excessive power consumption. In response, a direct heating (DH) method has been developed to address these challenges, enabling rapid (< 10 min) and cost-effective production of MgO nanomaterials. In this study, the DH process was optimized by investigating the influence of precursor solution concentrations (0.01 M to 0.10 M) on the growth of MgO nanomaterials on wire surfaces. Analyses utilizing Fourier Transform Infrared Spectroscopy (FTIR), Energy Dispersive X-ray Spectroscopy (EDX), and X-ray Photoelectron Spectroscopy (XPS) confirmed the formation of MgO. Field Emission Scanning Electron Microscopy (FESEM) revealed that the nanomaterials predominantly nano-walls and particles. The optimized synthesis conditions for MgO nanomaterials requires the heating of 0.10 M Mg(NO3)2·6H2O precursor at 50 W.h. for 10 min. Under this specific condition, a favourable surface coverage of 81.54% was achieved where the MgO nanowalls produced has demonstrated promising capability to remove Methylene Blue (MB) dye under UV irradiation. In conclusion, DH technique is a favourable alternative route to synthesize MgO nanomaterial in a simple, cost-and -time efficient and environmentally friendly way.
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