Conventional Powder Metallurgy Research Articles

Manufacturing Oxide Dispersion Strengthened (ODS) steel plate via cold spray and friction stir processing

Oxide dispersion strengthened (ODS) steels, traditionally fabricated by ball milling and conventional powder metallurgy techniques to achieve bulk form, followed by intricate rolling and thermal treatment steps to achieve plate or sheet form. Here, we present a novel processing route that combines cold spray (CS) with friction stir processing (FSP) to manufacture ODS steel plate directly from gas atomization reaction synthesis (GARS)-prepared powder, thus no rolling steps involved. Microstructural and mechanical characterizations were performed to assess the quality and properties of the resulting ODS steel plate. Our findings demonstrate that the slightly porous CS deposited layer was fully consolidated after FSP, yielding a fully dense ODS steel plate that exhibited a favorable tradeoff between strength and ductility upon extraction from the substrate. Furthermore, through microstructural analysis, we revealed the presence of an appreciable density (∼1022/m3) of nano-sized oxide particles, with the majority being smaller than 5 nm via the combined CS + FSP fabrication route. This work serves as a first proof-of-concept demonstration of the manufacturing approach described herein, offering a possible alternative route for producing ODS steel plates.

Role of Cr in Mn-rich precipitates for Al–Mn–Cr–Zr-based alloys tailored for additive manufacturing

Novel alloy concepts enabled via additive manufacturing processes have opened up the possibility of tailoring properties beyond the scope of conventional casting and powder metallurgy processes. The authors have previously presented a novel Al–Mn–Cr–Zr-based alloy system containing three times the equilibrium amounts of Mn and Zr. The alloys were produced via a powder bed fusion-laser beam (PBF-LB) process taking advantage of rapid cooling and solidification characteristics of the process. This supersaturation can then be leveraged to provide high precipitation hardening via direct ageing heat treatments. The hardening is enabled with Zr-rich and Mn-rich precipitates. Literature study confirms that Mn-rich precipitates have a notable solubility of Cr, for example, the Al12Mn precipitate. This study aims to clarify the effect of Cr solubility in the thermodynamics and kinetics simulation and compare the precipitation simulations with samples subject to >1000 h isothermal heat treatment, thus creating an equilibrium-like state. The results show that Cr addition to the precipitates stabilizes the Al12Mn precipitate while slowing the precipitation kinetics thus producing a favourable hardening response. Such observations could be insightful while designing such alloys and optimising heat treatments of the current or even a future alloy system.

Biomechanical behavior of a new design of dental implant: Influence of the porosity and location in the maxilla

The biomechanical performance of dental implants determines their clinical success. In this work, the stress and deformation distribution of a new implant design (dense and porous) was evaluated by the Finite Element Method. Furthermore, the effect of the location of the dental implant in the maxillary zone, as well as the mechanical response in the peri-implant maxillary tissue (cortical and trabecular) is discussed in detail. Before carrying out the computational study of the dental implant, Ti6Al4V cylindrical preforms obtained by conventional powder metallurgy and space-holder technique were characterized, to choose the most appropriate porosity (percentage and size) to achieve the biomechanical and biofunctional balance of the dental implant investigated. The novel porous dental implant under investigation exhibits 40% porosity in the region in contact with the trabecular bone, featuring inclined pores at 60 and 120° with a diameter of 200 μm. Our findings revealed that the cortical bone experienced the highest stress values, whereas the trabecular bone exhibited the highest levels of strain. Notably, the location of dental implants in the maxilla highlighted as the most influential factor affecting the maximum values of von Mises equivalent stress and strain. Furthermore, in the second molar location, the stress and strain levels exceeded the recommended thresholds for maintaining peri-implant bone density. Additionally, the porous implants generated significantly higher levels of stress and strain in the peri-implant trabecular bone than dense implants.

Role of process control agent in the production of Al2O3-reinforced titanium matrix composites

Metal Matrix Composites (MMCs) have recently been preferred over traditional materials in many engineering applications. Titanium matrix composites (TMCs) are used in the automotive, aerospace and defence industries thanks to their exceptional strength, high fatigue strength, good corrosion resistance and high elastic modulus. Some of the most used reinforcement materials for TMCs are SiC, Zr2O3, Al2O3, graphene, carbon nanotube (CNT) and TiC. In this study, TMCs reinforced Al2O3 were produced via conventional powder metallurgy (PM) and ultrasonic-assisted mixing. An Al2O3 in varying amounts (5 and 10 wt%) was incorporated into the TMCs via mechanical alloying (MA) for 5 h in a high-energy ball mill and using different process control agents (PCA, Stearic acid (SA), Polyvinyl Alcohol (PVA), Ethanol). The mechanically alloyed (MA'ed) powders were compacted by a hydraulic press under uniaxial pressure of 450 MPa and sintered at 1200 °C for 2 h in an argon atmosphere. The microstructural, mechanical and tribological properties of Ti-xAl2O3 powders and bulk samples were investigated. The highest hardness and the lowest specific wear rate were found in specimens reinforced with 5 wt% Al2O3, using ethanol as PCA, and produced by ultrasonic-assisted mixing, but the same specimen had the lowest compressive strength.

Supreme tensile properties in precipitation-hardened 316L stainless steel fabricated through powder cold-consolidation and annealing

One of the key goals of processing 316L stainless steel by powder metallurgy (PM) techniques is to achieve industrial-viable tensile properties without structural defects like poor densification, undesired phase transitions, and oxidation during high-temperature sintering. To address this, this study adopts high-pressure torsion to fabricate a fully dense structure at ambient temperature through cold consolidation. The samples fabricated by the present PM-based technique exhibits considerably enhanced tensile properties compared to counterparts processed by conventional PM techniques, with a remarkable yield strength of 1 GPa and total elongation of 46%. Additionally, the segregation of certain elements during subsequent annealing results in a unique microstructure with nano-scale sigma precipitates which induces dislocation pile-up, leading to improved yield strength and retarded dislocation motion. The results indicate that the present PM-based route is an applicable technique to achieve the strength-ductility synergy in 316L stainless steel.

Improving the properties of TiC steel bonded cemented carbides by optimizing the slurry rheology, printing path and shape design of 3D gel printing

TiC steel bonded cemented carbide was modeled by an extrusion-based 3D gel printing(3DGP) method. The rheological behavior of slurry was studied to control the slurry extrusion and modeling. The effects of printing parameters, printing path and modeling complexity were researched to get a printed sample without defects. The results indicated that the slurry with a solid loading of 50 vol% (85 wt%) was prepared, and its viscosity change is very little during 24 h in case of a higher shear rate like a nozzle. The viscosity of the slurry decreases with increasing the extrusion pressure and nozzle diameter. The skewed pattern of filaments eliminated pores in printed samples in comparison with the rectangular pattern under the condition of straight lines of the printing path. Pores at the corners of a model can be eliminated by changing the printing path from concentric lines to zigzag lines or two sets of slanted parallel lines. The modeling complexity without a support structure can be revealed by printing tilt cylinders with different angles, and the local parts on a model with a tilt angle of <45° can be printed accurately without designing a support structure. Improving the 3DGP procedure based on these experiences, the TiC steel bonded cemented carbide samples had properties similar to those prepared by conventional powder metallurgy methods.

Hot-Pressing Deformation Yields Fine-Grained, Highly Dense and (002) Textured Ru Targets.

Ruthenium (Ru) is a refractory metal that has applications in the semiconductor industry as a sputtering target material. However, conventional powder metallurgy methods cannot produce dense and fine-grained Ru targets with preferred orientation. Here, we present a novel method of hot-pressing deformation to fabricate Ru targets with high relative density (98.8%), small grain size (~4.4 μm) and strong (002) texture. We demonstrate that applying pressures of 30-40 MPa at 1400 °C transforms cylindrical Ru samples into disk-shaped targets with nearly full densification in the central region. We also show that the hardness and the (002)/(101) peak intensity ratio of the targets increase with the pressure, indicating enhanced mechanical and crystallographic properties. Our study reveals the mechanisms of densification and texture formation of Ru targets by hot-pressing deformation.

The Effect of the Surface Topography of High-Speed Steel Cutting Blades Made Using Various Methods on Their Technological and Functional Properties.

Indication of the proper scope of application of high-speed steels (HSS) produced by conventional methods and powder metallurgy for cutting tool blades requires a thorough assessment of their properties in various cutting conditions. According to common knowledge, the properties of tools made of both types of steel are largely determined by the arrangement of carbide phases. It turns out, however, that the surface morphology of the cutting blades is at least as important for their operational properties. This was already indicated by the preliminary research of the authors of the article, in which it was found that the surface topography significantly affects their durability depending on the applied value of the cutting speed in dry machining conditions and in the presence of a cooling lubricant. As it turned out, contrary to the literature data, blades made of sintered HSS do not have better service properties in all cutting conditions than blades made by conventional methods (e.g., in forging and hot rolling processes). Hence, it was necessary to determine the justified range of use of both types of steel for cutting blades. Cutting blades with a similar chemical composition from conventional high-speed steel and those produced in the powder metallurgy process were tested. Wear curves were determined on the basis of the tests. On this basis, for the assumed value of the blunting index, the tool life of the cutting edges was determined during the cutting of selected structural steel, commonly used for high-strength machine parts. Tests of the cutting ability of the blades were carried out without and with the use of a cooling--lubricating liquid. In order to correctly interpret the obtained results of the wear and durability tests of the cutting edges, verification tests were carried out. A detailed analysis of the research material made it possible to determine the recommended range of applicability of conventional and sintered HSS for the tested case.

Production and Characterization of Aluminum Reinforced with SiC Nanoparticles

Aluminum matrix nanocomposites have been the subject of much attention due to their extraordinary mechanical properties and thermal stability. This research focuses on producing and characterizing an aluminum matrix reinforced with silicon carbide (SiC) nanometric particles. The conventional powder metallurgy route was used to produce the nanocomposites, and the dispersion and mixing process was carried out by ultrasonication. The conditions of the dispersion and the volume fraction of the SiC were evaluated in the production of the nanocomposites. Microstructural characterization was carried out using optical microscopy (OM), scanning electron microscopy (SEM), energy dispersive X-ray spectroscopy (EDS), and electron backscatter diffraction (EBSD). Mechanical characterization was carried out using hardness and tensile tests. The dispersion agent was investigated, and isopropanol leads to better dispersion with fewer agglomerates. Increasing the volume fraction of the reinforcement improves the hardness of the nanocomposites. However, greater agglomeration of the reinforcement is observed for larger volume fractions. The greatest increase in hardness (77% increase compared to the hardness of the Al matrix) is obtained with 1.0 vol. % of SiC, corresponding to the sample with the best dispersion. The mechanical characterization through tensile tests attests to the effect of the reinforcement on the Al matrix. The main strengthening mechanisms identified were the load transfer, the texture hardening, Orowan strengthening, and the increase in the density of dislocations in the nanocomposites.

Constructing process maps for pulsed wave laser additive manufacturing with interpretable machine learning

Oxide dispersion strengthened (ODS) steels have found increasing applications in advanced fission and fusion reactors due to their excellent strength and resistance to radiation damage. The traditional powder metallurgy (PM) methods for fabricating ODS steels are costly and time-consuming. To address these limitations, attempts have been made to fabricate ODS steels with emerging additive manufacturing (AM) technology, such as laser powder bed fusion (L-PBF). However, up to now, the AM-fabricated ODS steels have not been able to match the quality of those from the conventional PM processes. In this work, we explore pulsed wave (PW) laser AM, as opposed to the conventional single mode continuous wave (CW) laser AM, for ODS steel fabrication. In particular, based on available experimental data of PW laser fabricated ODS steel parts, we construct a two-dimensional (2D) process map using two PW features (engineered using operating parameters) to define and visualize the parameter space that is directly linked to the quality assessment of the parts. Additional process maps are constructed to quantitatively model the density and nano-hardness of the parts. These process maps are constructed through rational feature engineering, supervised feature selection, and interpretable machine learning techniques. The constructed process maps for quality classification, density and nano-hardness regression analyses are validated by experiments. The process maps help us further understand the physical phenomena that produce good or bad quality parts.

Microstructure and mechanical properties of Ti-TiBw-x%Cu composites by powder metallurgy using atomized Ti-TiBw powder as raw materials

Titanium matrix composites (TMCs) reinforced with titanium boride whisker (TiBw) prepared by conventional smelting or powder metallurgy via in-situ techniques are inevitable to cause TiBw coarsening by high-temperature thermal history, which feasibly leads to stress concentration and results in seriously inverse relationship between strength and toughness. This paper developed a novel strategy using Ti-TiBw composite powder as raw powder which is produced by the plasma rotating electrode atomization method (PREP), to control TiBw to nanoscale size by taking advantage of the rapid cooling rate of PREP. On this basis, the fast eutectic element Cu was proposed as alloying element and introduced into Ti-TiBw composite system using powder metallurgy, to investigate the influence rules of Cu content on TiBw scale characteristic parameters (diameter and aspect ratio, etc.) as well as the microstructure and mechanical properties of Ti-TiBw composites. The hardness of the specimen was increased by 61.9%, while its tensile strength and yield strength were increased to 823 ± 12 MPa and 602 ± 11 MPa, respectively. Its elongation retained the same level at 10.8 ± 1.9% as that of Ti-TiBw composites.

Microstructure and Mechanical Properties of Low-Cost SiC-Reinforced Aluminum and Al4Cu Matrix Composites Produced by Sintering in Vacuum.

Composite materials based on Al and Al4Cu with the addition of SiC particles (2.5; 5; 7.5; 10 wt.%) were produced in low-cost conventional powder metallurgy processes involving mixing, compacting with a pressure of 300 MPa, and sintering at 600 °C in a vacuum atmosphere. An attempt was made to create a relationship between the vacuum sintering and the microstructure and mechanical properties of Al/SiC composites. The strength of the matrix-reinforcing interface depends on the chemical composition of the components; therefore, the influence of 4 wt.% copper in the aluminum matrix was investigated. Comprehensive microstructural and mechanical properties (including Brinell hardness, compressive and flexural strength measurements) of the produced composites were measured. The addition of 2.5 wt.% SiC to the Al4Cu matrix improved the mechanical properties of the composites compared to the matrix. In the composite with the addition of 2.5 wt.% of SiC, while the addition of the reinforcement did not affect the hardness and compressive strength and caused a rapid decrease in the flexural strength compared to the aluminum matrix, the addition of Cu to the matrix of this composite improved hardness (from 25 to 49 HB), compressive strength (from 423 to 618 MPa), and flexural strength (from 52 to 355 MPa).

In Vitro and In Vivo Bone Regeneration Assessment of Titanium-Doped Waste Eggshell-Derived Hydroxyapatite in the Animal Model.

In this work, a titanium-doped hydroxyapatite (HAp) scaffold was produced from two different sources (natural eggshell and laboratory-grade reagents) to compare the efficacy of natural and synthetic resources of HAp materials on new bone regeneration. This comparative study also reports the effect of Ti doping on the physical, mechanical, and in vitro as well as in vivo biological properties of the HAp scaffold. Pellets were prepared in the conventional powder metallurgy route, compacted, and sintered at 900 °C, showing sufficient porosity for bony ingrowth. The physical-mechanical characterizations were performed by density, porosity evaluation, XRD, FTIR, SEM analysis, and hardness measurement. In vitro interactions were evaluated by bactericidal assay, hemolysis, MTT assay, and interaction with simulated body fluid. All categories of pellets showed absolute nonhemolytic and nontoxic character. Furthermore, significant apatite formation was observed on the Ti-doped HAp samples in the simulated body fluid immersion study. The developed porous pellets were implanted to assess the bone defect healing in the femoral condyle of healthy rabbits. A 2 month study after implantation showed no marked inflammatory reaction for any samples. Radiological analysis, histological analysis, SEM analysis, and oxytetracycline labeling studies depicted better invasion of mature osseous tissue in the pores of doped eggshell-derived HAp scaffolds as compared to the undoped HAp, and laboratory-made samples. Quantification using oxytetracycline labeling depicted 59.31 ± 1.89% new bone formation for Ti-doped eggshell HAp as compared to Ti-doped pure HAp (54.41 ± 1.93) and other undoped samples. Histological studies showed the presence of abundant osteoblastic and osteoclastic cells in Ti-doped eggshell HAp in contrast to other samples. Radiological and SEM data also showed similar results. The results indicated that Ti-doped biosourced HAp samples have good biocompatibility, new bone-forming ability, and could be used as a bone grafting material in orthopedic surgery.

Micropillar compression of Ti(C,N)-FeNi cermets: Microstructural, processing, and scale effects

The influence of microstructure and processing route on the small-scale mechanical response as well as on the deformation and failure mechanisms of Ti(C,N)-FeNi cermets were investigated by uniaxial compression of micropillars milled by focused ion beam with different sizes. Stress-strain curves were determined and associated deformation mechanisms were observed in-situ using scanning electron microscopy. The appropriate micropillars dimension was assessed, based on the microstructural characteristics of studied cermets, to overcome scale effect issues. A direct relationship was observed between yield strength and ceramic/metal ratio for colloidal samples. Meanwhile, deformation of metallic binder and glide between Ti(C,N)/Ti(C,N) particles were evidenced as dominant mechanisms during the compression for colloidal cermets with 70 and 80 vol% of ceramic phase, respectively. The obtained results illustrate that samples processed from powder attained by colloidal route provide superior mechanical behavior, as compared to that exhibited by specimens shaped following a conventional powder metallurgy one (wet ball-milling/drying).

Investigation on compaction pressure and sintering temperature suitable for Nimonic 90 superalloy

Fabrication of high strength, high temperature and corrosion resistant materials provide much assistance in aerospace, automotive, chemical and oil industries, as they have to withstand severe operating conditions. Traditionally, superalloys are widely used under these conditions that are prepared by casting method. Nowadays, powder metallurgy technique is gaining importance for preparing superalloys because of its capability of making homogeneous microstructure with near-net-shape. In this significant context, the processing of Nimonic 90 superalloy sample using conventional powder metallurgy route is discussed. Desired amount of metallic powders by weight percent are blended, uni-axially pressed and sintered in tubular vacuum furnace at different sintering temperatures. The influence of compaction pressure and sintering temperature on density, hardness, surface roughness and electrical resistivity is determined. Surface porosity and the effect of sintering temperature on the microstructural features are analyzed noticeably. It is found that the compaction pressure of 700 MPa and the sintering temperature of 1365℃ are the most desirable process parameters, essentially required for synthesizing the Nimonic 90 superalloy. Sample prepared under these conditions has achieved the desired density and hardness, as that of the standard Nimonic 90 alloy. Thus, the study paves the way for future researchers to appropriately identify the conditions suitable for preparing the superalloys as per the application needed.

Comparative Study of Corrosion Behaviors of WC-NiMo and WC-Co Cemented Carbides.

In this paper, the influence of a nickel binder metal and molybdenum carbide as an additional alloying element on the microstructure and corrosion behavior of WC-based cemented carbides, processed by conventional powder metallurgy, was studied, and a comparison with conventional cemented carbide (WC-Co) was carried out. The sintered alloys were characterized, before and after corrosive tests, by analyses using optical microscopy, scanning electron microscopy, energy dispersive X-ray spectroscopy, and X-ray diffraction. The corrosion resistance of the cemented carbides was investigated by open circuit potential, potentiodynamic polarization, and electrochemical impedance spectroscopy in a 3.5 wt.% NaCl solution. The WC-NiMo cemented carbides showed microstructures similar to those of WC-Co; however, pores and binder islands were observed in the microstructures. The corrosion tests showed promising results, the WC-NiMo cemented carbide showed superior corrosion resistance and higher passivation capacity than the WC-Co cemented carbide. The WC-NiMo alloy showed a higher EOC ≈-0.18 V vs. Ag|AgCl|KCl3mol/L than the WC-Co (EOC≈-0.45 V vs. Ag|AgCl|KCl3mol/L). The potentiodynamic polarization curves showed lower current density values throughout the potential range for the WC-NiMo alloy, and it was observed that Ecorr was less negative (≈-0.416 V vs. Ag|AgCl|KCl3mol/L) than for WC-Co (≈-0.543 V vs. V vs. Ag|AgCl|KCl3mol/L). The EIS analysis confirmed low rate corrosion of WC-NiMo associated with the formation of a passive thin layer. This alloy showed a higher Rct (1970.70 Ω).

Mechanical, wear and corrosion behavior of Ti–6Al–xNb (x = 3.5–21 wt%) alloys manufactured by powder metallurgy

In this study, Ti–6Al–xNb alloys with different Nb percentages (x = 3.5–21 wt%) were produced by the conventional powder metallurgy technique. After mixing and pressing the alloy powders in appropriate proportions, the green samples were sintered in a tube furnace under a vacuum atmosphere at 1200 °C for 2 h. The X-ray diffraction analysis (XRD) showed that all the alloys consist of α–Ti, TiNb (β–Ti) and AlNb2 phases. The results showed that the Ti–6Al–14Nb alloy among all alloys has the best mechanical properties, and the microhardness, tensile and flexural strength are 276.4 Vickers hardness (Hv0.2), 453 MPa and 1682 MPa, respectively. Tribological tests were carried out in both dry and wet conditions with Hanks' Balanced Salt Solution. While generally, the specific wear rates of the samples increased with Nb content up to 17.5 wt% under dry conditions, on the other hand, they increased with increasing Nb content under wet conditions. On the other hand, the specific wear rate increased with increasing the sliding distance. The best corrosion resistance alloy among all the samples was Ti–6Al–7Nb with −0.0968 V corrosion potential (Ecorr), 0.015 μA/cm2 corrosion current density (Icorr) values.

Fabrication of tailored Ti6Al4V-based materials by conventional powder metallurgy for bone implant applications

ABSTRACT This works proposes a methodology for fabricating materials with specific characteristics mimicking human bones. A Ti64 alloy powder was used as the base material and it was mixed with Ag, Ta, TiN and salt particles to obtain different features. A hip-bone like component was fabricated, including a highly porous core of Ti64/25Ta/5Ag and a compact outer shell of Ti64/5Ag that is supposed to improve corrosion and osseointegration. Besides, a harder cover surface in Ti64/10TiN composite should increase the wear resistance. The green component was sintered at 1260°C in argon. Its Young’s modulus was close to the one of bones due to the added porosity, which also provided a permeability close to the one reported for trabecular bones. Tribocorrosion behaviour in simulated body fluid was improved by TiN addition. In conclusion, the proposed processing route was able to produce complex components fulfilling specific features required for human bone replacement.

PRODUCTION OF OXIDE DISPERSION STRENGTHENED INCONEL 718 ALLOYS USING CONVENTIONAL POWDER METALLURGY AND ADDITIVE MANUFACTURING METHODS

Oxide dispersion strengthened (ODS) Ni-based alloys having a high density of nano-oxides (NOs) (&amp;lt;10 nm) are considered to be good candidates for extreme environments, such as high temperature, radiation, and corrosion. In this study, ODS IN718 alloys have been produced using conventional powder metallurgy (PM) and novel selective laser melting (SLM) additive manufacturing. The effect of processing routes on the microstructure, in particular on the nano-oxide formation and structure has been investigated. It has been found that the powder metallurgy method that consists of compressing followed by sintering at 1250 and 1500 °C results in a nano-granular structure with homogenously distributed fine nano-oxides having a high number density. Similarly, SLM results in a high number density of fine nano-oxides; however, the particles exist in groups with the grains/cells. The nano-oxides are determined to be Y2Ti2O7, Y2TiO5 or YTiO3 and Y-Al-O. The deviation in the lattice parameters of Y2Ti2O7 infers the existence of some Al in the structure. This study sheds light on producing ODS IN718 alloys with high-density nano-oxides using powder metallurgy and additive manufacturing methods.

Limits of powder metallurgy to fabricate porous Ti35Nb7Zr5Ta samples for cortical bone replacements

The use of β-Titanium alloys to fabricate metal implants with Young's modulus that resembles bone tissues is presented as an alternative to commercially pure titanium or α-Titanium alloys, although it is still necessary to introduce proper implant porosity to reach the Young's modulus of cortical bones. In this work, porous samples were fabricated by loose sintering (0 MPa) and compared to samples manufactured at 1000 MPa, both sintered under the same conditions. Raw powders and sintered samples of the β-Titanium alloy, Ti35Nb7Zr5Ta, were characterized in detail in terms of both physicochemical and microstructural properties. Moreover, the tribo-mechanical behavior of sintered samples was evaluated by performing ultrasound technique, instrumented micro-indentation (P-h curves), and scratch tests. The bio-functional behavior was studied by impedance spectroscopy and contact angle measurements. The results allowed the evaluation of the limits of conventional powder metallurgy (percentage of porosity, size, and morphology of pores), as well as the influence of the porosity and chemical composition to achieve a better biomechanical and bio-functional behavior that would guarantee bone requirements. The Ti35Nb7Zr5Ta alloy showed relatively high electrical impedance values compared to commercially pure titanium, indicating an improved bio-corrosion behavior. Furthermore, wettability measurements indicated that porous disks fabricated by loose sintering exhibit higher hydrophilicity, often associated with a better antibacterial response.