Compacted Specimens Research Articles

Experimental bilayer zirconia systems after aging: Mechanical, optical, and microstructural characterization.

To characterize two experimental zirconia bilayer materials compared to their monolithic controls, before and after hydrothermal aging. Commercial zirconia powders were utilized to fabricate two bilayer materials: 3Y-TZP+ 5Y-PSZ (3Y+5Y/BI) and 4Y-PSZ+ 5Y-PSZ (4Y+5Y/BI), alongside control groups 3Y-TZP (3Y/C), 4Y-PSZ (4Y/C), and 5Y-PSZ (5Y/C). Compacted specimens were sintered (1550 °C- 2 h, 3 °C/min), and half of them underwent hydrothermal aging (134 °C-20h, 2.2 bar). Characterizations were performed through scanning-electron microscopy (SEM), X-ray diffraction (XRD), Raman spectroscopy, reflectance tests and biaxial flexural strength test (ISO:6872). Weibull statistics were applied to determine the characteristic strength and Weibull modulus. Grain size and optical properties were analyzed using two-way ANOVA followed by the Tukey test. Degradation regions and monoclinic phase were observed at aged 3Y-TZP and 4Y-PSZ surfaces. Significant differences were observed in the evaluation of optical properties between the bilayer and control groups. The bilayer materials presented intermediate characteristic strength values compared to their controls and aging significantly increased the strength of some groups. Experimental bilayer materials presented lower mechanical properties than monolithic controls, 3Y/C and 4Y/C. Hydrothermal aging increased the characteristic strength of bilayered and monolithic controls, except for 5Y-PSZ. Both experimental bilayer systems, as well as monolithic controls, met the ISO 6872:2015 requirements for single-unit crowns (100 MPa), 3-unit fixed dental prostheses (FDPs) up to premolars (300 MPa), and 3-unit FDPs involving molars (500 MPa). However, for FDPs with four or more units, only monolithic 3Y-TZP and 4Y-PSZ, and bilayered 3Y+5Y met the required minimum flexural strength (≥800 MPa).

Developing eco-friendly lightweight concrete mixes using recycled EPS beads for structural and non-structural applications

In this study, several concrete mixes were developed by partially replacing all concrete mix components with recycled expanded polystyrene (EPS) beads. The replacement ratios ranged from 10% to 60% of the total mix volume. The impact of compaction was also studied by casting half of the specimens without compaction and the other half with compaction. Evaluations included thermal conductivity, density, compressive, flexural, and splitting tensile strengths. Results showed that EPS replacement improved thermal insulation but reduced density and all mechanical properties. Density decreased by 8% to 46% for compacted and 14% to 60% for uncompacted specimens. Thermal conductivity dropped by 38% to 74% for compacted and 58% to 85% for uncompacted specimens. The compressive strength of compacted specimens decreased exponentially, but those with up to 40% EPS were suitable for load-bearing blocks. Specimens containing 50% EPS exhibited a compressive strength of 7.2 MPa, making them suitable for non-structural applications requiring good thermal insulation properties. Although the EPS substitution lowered the strength-to-density ratio, it is expected to produce a more eco-friendly LWC due to reduced cement, water, and aggregate consumption.

Evaluation of Different Blending Methods to Obtain Copper Composites with Graphene Oxide

This study evaluated mixing methods for producing graphene oxide-reinforced copper matrix composites aiming for a better dispersion of graphene oxide in the composite, using powder metallurgy techniques. The compacted specimens were prepared by four different mixing processes that employed either a mechanical stirrer, rotary evaporator, tip ultrasound, or ultrasound process followed by mechanical stirring. Characterizations were performed using optical microscopy, scanning electron microscopy, X-ray diffraction, Raman spectroscopy, transmission electron microscopy, compression tests, Vickers microhardness, and electrical conductivity measurements. The results indicate that the combined method yields a more homogeneous microstructure and superior mechanical properties, while electrical conductivity was maintained at a level higher than that achieved by the other methods.

Evaluation of asphalt mixtures modified with low-density polyethylene and high-density polyethylene using experimental results and machine learning models

The widespread use of low-density polyethylene (LDPE) and high-density polyethylene (HDPE) plastics has resulted in a large amount of waste plastic that requires appropriate disposal or reuse. One potential solution is to use them in the modification of asphalt concrete (AC) mixtures for more sustainable highways. To study this possibility, permanent deformation and dynamic modulus (DM) of the LDPE and HDPE modified AC mixtures was investigated by conducting flow number (FN), flow time (FT) and DM tests on Superpave gyratory compacted specimens. Machine learning models; multi-layer perceptron (MLP), radial basis function neural network (RBFNN), generalized regression neural network (GRNN) and support vector machine (SVM) were used to predict the DM on the basis of frequency and temperature parameters. The model’s performance was gauged by analyzing the root mean square error, mean relative error, and coefficient of determination. The study findings revealed that the LDPE and HDPE modified AC mixtures provide 2.07 times and 1.27 times better resistance to permanent deformation, respectively, than their counterpart. It was also found that the LDPE and HDPE modified AC mixtures have 2.1 times and 1.4 times higher DM values, respectively, than the Control AC mixtures. Among the machine learning models, MLP (R2 = 0.98) showed best accuracy in predicting DM and thus is recommended to be used in similar studies due to its robustness. Additionally, the feature importance analysis revealed that frequency has the highest impact on DM predictions, followed by temperature and the inclusion of the LDPE.

The effect of specimen size on the unconfined compressive strength of cement-stabilized granular mixtures made of natural and recycled aggregates

The cement-stabilization technique is employed on natural and recycled granular materials to improve their mechanical properties. The strength of these materials is assessed by the unconfined compressive strength on laboratory compacted specimens, typically after 7 days of curing. Standards and technical specifications specify different values of specimen height and diameter and different loading modes of testing. This makes the comparison between different materials and with the acceptance limits of technical specifications difficult. The research investigates the effect of specimen size and loading mode on the unconfined compressive strength of both natural and recycled cement-stabilized granular materials. The results revealed significant differences in strength due to variations in specimen size and loading mode. As expected, an increase in specimen slenderness resulted in a decrease in compressive strength. A linear regression model was developed to quantify the effect of the experimental variables on the compressive strength of the two cement-stabilized materials.

Shear strength characteristics of unsaturated compacted GMZ bentonite considering anisotropy

Anisotropic microstructure would be generated in the bentonite block during unidirectional compactions. Working as buffer materials, the compacted bentonite will inevitably experience shearing processes during the long-term operation of geological repositories. In this paper, high-pressure triaxial tests were conducted on unsaturated compacted GMZ bentonite specimens with different water contents, dry densities and confining stresses, with the compaction surface of the specimens oriented in both horizontally (H-type) and vertically (V-type) configurations. Results demonstrate that an increase in water content leads to a reduction in both peak strength and residual strength, while higher confining stresses enhance these strength parameters. Normally consolidated and lightly over-consolidated bentonite specimens display substantial shear deformation, whereas heavily over-consolidated specimens tend to experience brittle failure. Water content plays a significant role in shaping both the critical state line (CSL) and the Hvorslev surface (HS), with increasing water content resulting in decreased slope parameters for both and an increased intercept parameter for the HS. Generally, V-type specimens demonstrate a steeper CSL and an outwardly extended HS in contrast to that of H-type specimens. The critical state ratio for V-type specimens is about 10 % higher, and the friction angle is 2.8° greater, than that of the H-type ones. Moreover, this difference appears to increase with increasing water content. The difference of the HS slope parameter between the two specimens is minor, while the intercept parameter is higher for the V-type specimens.

Assessing cracking resistance and threshold limits of bituminous mixtures with IDEAL-CT and predictive modeling techniques

This paper presents a comprehensive study to establish the threshold limit of CTIndex for the Marshall mixes. The study also aims to assess the impact of different design factors on the cracking resistance of bituminous mixtures using the Indirect Tensile Asphalt Cracking Test (IDEAL-CT) test. This study considers 2 different aggregate sources, 2 different gradations, 5 different types of Design Aggregate Gradation (DAG), 3 binder types, and 5 levels of compactive effort. The test results show that higher cracking resistance can be achieved using a smaller nominal maximum size of the aggregate (NMAS), finer gradation, modified binder, and decreased compactive effort with aggregates having low abrasion and absorptive characteristics. This study also comprehends the influence of volumetric parameters of the bituminous mixes on fracture resistance. It was found that at a particular Optimum Binder Content (OBC), higher bulk specific gravity of the compacted specimen (Gmb) and voids filled with asphalt (VFA) result in reduced CTIndex, specifying poor cracking performance. While higher air voids (AV) and voids in mineral aggregate (VMA) lead to increased CTIndex, indicating better-cracking resistance. Statistical analysis tools were used to evaluate the significance of the influential factors that are affecting the cracking potential of the mix. Different Machine learning models were also developed to predict CTIndex based on the design factors considered in the study. The random forest (RFR) model showed strong accuracy, reflected by low Mean Absolute Error (MAE=3.16), Mean Absolute Percentage Error (MAPE=9.57), Root Mean Square Error (RMSE=4.23), and a high coefficient of determination (R²=0.95) value, notifying a precise fit and reliable predictions. Additionally, a GUI has been also developed to enhance the practical usability of the model for wider usage. Further, the present study proposes the threshold value of CTIndex for the selection of crack-resistant bituminous mixtures. Moreover, the study investigated the correlation between laboratory and field compaction methods and validated the initial threshold specification of CTIndex for the Marshall mixes. Despite of the variations in different compaction methodologies and specimen thickness, a strong positive correlation (R² > 0.76) between laboratory and field cores of BC-1 and DBM-2 indicates that the performance criteria are adequate and justified.

Improving Shear Strength and Microstructural Behavior of Black Cotton Soil Treated with Construction Demolished Waste

With its expansive character and low bearing capacity, black cotton soil presents considerable obstacles to construction projects. These challenges can be difficult to overcome. There is a tendency for it to rise and compress in response to variations in the amount of moisture present, and it also has weak strength properties, which makes construction activities more difficult. This study explores the possibility of stabilizing black cotton soil with recycled construction and demolition (C&D) waste in order to address these issues. Various C&D waste materials, like concrete, bricks, mortar, and other debris, are examined for their potential to enhance the shear strength of black cotton soil. The paper assesses the effectiveness of incorporating C&D waste blends ranging from 5% to 25% to mitigate soil swelling and shrinkage with improve shear strength. Previous to determining the soil's shear strength, index properties were assessed. Unconfined compression strength tests (UCS) are carried out on compacted specimens handled with C&D waste blends, with curing periods of 1 day, 7 days, and 28 days at room temperature. A comparison investigation showed that there was a comparable increase in UCS and a decrease in axial strain at failure as the amount of C&D waste in the soil rose. Micro-analyses displayed that the main factors prompting the interacting behavior of soil amended with C&D waste include changes in the gradation, cohesiveness, and the interplay between the particles, the mineralogical makeup, and the elemental, chemical, and microstructural components. The research aims to offer insights into sustainable methods for strengthening the performance of black cotton soil while reducing waste generation in construction activities.

Effect of Production and Curing Methods on the Properties of Roller-Compacted Concrete: A Review

Roller Compacted Concrete (RCC) exhibits many characteristics of both asphalt and rigid pavements, but their use is restricted. Many reasons led to this decision, including the fact that RCC is a type of concrete mixture that requires a specific consistency. It should be firm enough to be compacted by a roller compactor but also have enough moisture to ensure even distribution. The lab-field performance difference of RCC is another reason for decreasing its use. The laboratory RCC mixes are prepared using the modified Proctor compaction method. Subsequently, specimens are fabricated utilizing a vibratory hammer (VH) to evaluate their strength properties. Nevertheless, in the construction industry, pavement is built utilizing static, pneumatic, and vibratory rollers. Consequently, quality control is carried out by acquiring pavement samples and comparing them to laboratory samples. Each of these procedures employs different processes and energies, resulting in variations in field and laboratory behavior. In this investigation, some studies will be discussed about the RCC behavior under field and lab conditions using various design methods, such as the vibrating table (VH), vibratory table (VT), gyratory compactor (GC), and modified proctor (MP). These studies showed a difference in RCC mechanical and macroscale properties between laboratory compaction methods. For instance, VH specimens led to a higher evaluation, while GY specimens produced a less favorable estimation of the hardened properties observed in the field. While the MP and VT compacted specimens had a comparable structural arrangement to the field, they exhibited notable differences in terms of porosity and strength. Other studies revealed the essence of the curing stage in terms of RCC mechanical properties and indicated that some curing processes, like compound curing, may improve RCC performance.

Research on the migration law of aggregate particles in the compaction process of asphalt mixture based on discrete element method

Asphalt mixture compaction is among the key technologies in asphalt pavement construction, but the effect of asphalt mixture mixing quality on mixture compaction performance is still unclear. This research aimed to develop an asphalt mixture compaction model by discrete element simulation and verify it by compaction degree. Asphalt mixture compaction process was simulated and the effect of asphalt mixture workability on the stress, migration law and void distribution properties of aggregate particles during compaction process was investigated. The obtained results showed that the developed asphalt mixture compaction model was reasonable and correct. The more uniform the asphalt mixture is mixed, the smaller the average force on the aggregates, the aggregate particle migration velocity, and the aggregate particle displacement during the compaction of the asphalt mixture. Under the same conditions, increasing the mixing temperature from 140℃ to 180℃ increased the average velocity of the aggregates in the asphalt mixture by 92 %. It also decreased the voids in the compacted mixture specimens. At the same time, under the action of edge effect, void distribution at the center of compacted specimen was small, void distribution around the specimen was high, and void distribution along specimen compaction force direction was also high.

An alternative approach for increasing the visibility of roads

Visibility problems occur on highways that are not sufficiently illuminated at night, endangering traffic safety. Phosphor material, which has a natural glow feature under ultraviolet (UV) light, is planned to increase road visibility in areas with inadequate lighting. Phosphor powder (PP) was used in four different percentages (25%, 50%, 75%, and 100%) as fillers in hot mix asphalt (HMA), reduced to filler size. Asphalt specimens were prepared using a super pave gyratory compactor and super pave volumetric mixture design. Compacted specimens were exposed to artificial 12V UV light for 10-minute intervals in a dark room, and UV light absorption was observed. Visibility analyses were performed on the specimens by taking high-resolution photos with long exposure from a distance of approximately 30 cm from the asphalt specimen using a professional camera. According to the analysis results, the visibility values increased by 200.4%, 378.5%, 538.1%, and 728.5% compared to the reference specimen for substitution rates of 25%, 50%, 75%, and 100%, respectively. Experiments were conducted to determine the behavior of the specimens prepared as phosphorus substitutes in the mixture. After selecting the optimum binder contents, the modified Lottman test procedure was applied to measure the specimens' strength values and moisture sensitivity prepared at optimum ratios. The indirect tensile test results show that the 25% PP-substituted specimen had a better strength value. The tensile strength ratio (TSR) value, the ratio of dry and wet tensile stresses, was determined to have minor moisture sensitivity in the 50% PP-substituted specimen. HWTT was applied to the specimen containing 50% PP content, which exhibited the best TSR ratio, resulting in improved rutting performance compared to the reference specimen.

Advancing Field Aging Simulation Methods for Cantabro Abrasion Loss Testing

Over the past several years, the asphalt industry has progressively increased efforts to evaluate mixtures after laboratory conditioning for the purpose of simulating field aging, and has also increased reliance on mixture testing. AASHTO T 401-22 describes Cantabro Mass Loss testing and has an appendix of field aging simulation protocols that can be used to estimate field aging by making use of compacted specimens. T 401-22 is one of the few methods to contain both a field aging simulation protocol and a mixture property index test. This paper uses roughly 1,000 tested specimens from forty-nine mixes (mostly dense-graded asphalt with minor amounts of stone-matrix asphalt) evaluated for up to four years of field aging in a hot and non-freeze climate alongside twenty-five different laboratory conditioning protocols. This paper’s objective is to provide information to improve T 401-22 by way of recommendations to update the appendix of conditioning protocols with more comprehensive assessments of their effectiveness in simulating field aging in a hot, non-freeze climate. The overarching recommendation of this work culminates with four protocols. Two of these protocols use only oven conditioning, whereas the remaining two protocols use a combination of stages exposing specimens to oxidation in ovens, moisture effects in hot water baths, and freeze–thaw cycling. The time required to administer the recommended protocols varies from approximately 6 to 28 days and they simulate between 1 and 5 years of field aging depending on the protocol selected.

Effect of hybrid ratio and sintering temperature on hardness properties of hybrid AMCs

The present research work is aimed toward fabrication of hybrid Aluminium matrix composites (AMCs) of different hybrid ratios of Alumina (Al2O3) and Silicon Carbide (SiC) followed by investigation of their microstructure and hardness properties. Hybrid AMCs were fabricated through powder metallurgy process by adding 5 wt% and 10 wt% mixture of Al2O3 and SiC reinforcements of various hybrid ratios (0:1, 1:3, 1:2, 1:1, 3:1, 2:1 and 1:0) with the pure Aluminium powder. The mixture powder were properly mixed by ball milling arrangements for 6 h. The mixture powder were preheated at 500 °C for 2 h in a high temperature programmable tube furnace followed by immediate compaction under a closed die at 1500 psi pressure through automatic hydraulic press. The compacted specimens were then sintered at 350 °C, 500 °C and 650 °C for 2 h in the same furnace. Hardness test of the fabricated hybrid AMCs were carried out by Vickers Micro-hardness testers and hardness values were measured by the integrated software. The hardness properties of hybrid AMCs also were compared with the hardness properties of pure Aluminium specimens fabricated through the same process route and process parameters. It is interestingly observed that hardness of hybrid AMC is more when pure Aluminium powder is reinforced with only SiC of same wt.% for both the cases (5 wt% and 10 wt% reinforce AMCs) and it decreases with decrease of weight fraction of SiC and simultaneously increase of weight fraction of Al2O3 keeping total weight fraction of mixture as constant.

Influence of the curing stress effect on the stiffness degradation curve of a silt stabilized with lime and cement

This study investigated the shear modulus degradation curves of reconstituted stabilized soil specimens and their evolution during curing up to 270 days. An experimental protocol is proposed to get as close as possible to the in situ curing conditions of a chemically (lime and hydraulic binder) and mechanically (compaction) improved soil placed in a high-rise geotechnical structure. Innovative solutions now make it possible to build high embankments (> 10 m) in stabilized soil. In the laboratory, a silty soil stabilized with 1% lime and 5% hydraulic binder, which is a classic treatment for linear projects, was cured with a pressure of 300 and 500 kPa, corresponding to a depth in the embankment of 15 and 25 m. These structures are expected to have high mechanical performance and must be able to withstand very small deformations (earthquakes, traffic loads). Experimental campaigns are performed in laboratory using torsion tests with a resonant column apparatus (RCA) to obtain the shear modulus G as a function of distortion. A comparison was made between normalized curing conditions (temperature of 20 °C and atmospheric pressure) and curing with confining pressure (temperature of 20 °C and 300 or 500 kPa pressure). For this aim, 74 torsional RCA tests were conducted on 16 compacted soil specimens. These showed that the curing pressure, applied just after compaction, brings the expected properties more quickly and confers superior properties of around 15% in the long term. A power law was proposed to estimate the Gmax of a stabilized silt specimen as a function of time, based on the Gmax measured during the first two days of curing. This empirical law gives the Gmax over the long term (270 days) for curing with or without confining pressure. Pioneering a combined curing-testing RCA approach, this study elucidates the short and long-term behavior of stabilized silts under realistic curing conditions.

Feasibility of compacted attapulgite/diatomite amended clayey soils as gas barrier materials

Compacted clay liners are extensively used as barriers to control the upward diffusion of vapors of volatile or semi-volatile organic contaminants released from unsaturated contaminated soils at industry-contaminated sites. This study aimed to investigate the gas diffusion barrier performance of compacted clayey soils amended with three agents including attapulgite and diatomite individually, and attapulgite/diatomite mixture. The properties including water retention, volumetric shrinkage, gas diffusion, and unconfined compressive strength were evaluated through a series of laboratory tests of amended compacted clayey soils. The results demonstrate that the decrease in volume proportions of inter-aggregate pores leads to an increase in unconfined compressive strength (qu). Both hydrophilic groups and microstructures of attapulgite and diatomite result in an increase in water retention percent (Wt) of compacted clayey soil specimens after amendment regardless of the type of agent or initial water content (w0). Furthermore, the ratio of the gas diffusion coefficient (De) to the gas diffusion coefficient in the air (Da) was significantly reduced owing to a decrease in volume proportions of inter-aggregate pores, hydrophilic group, and microstructures of attapulgite and diatomite. Scanning electron microscope analyses revealed that rod-shaped attapulgite filled the inter-aggregate pores formed by clay particles, whereas the disc-shaped diatomite particles, characterized by micropores, failed to obstruct the inter-aggregate pores due to their larger particle size. Mercury intrusion porosimetry (MIP) analyses showed a reduction in pore volume in the inter-aggregate pores, leading to a reduction in the total pore volume for both the attapulgite and attapulgite/diatomite mixture amended clays, which is in accordance with the scanning electron microscope (SEM) results. The findings are pertinent to the practical application of compacted clay liners as gas barriers against the upward migration of volatile or semi-volatile organic contaminants at contaminated sites.

EXAMINING THE APPLICABILITY OF ALKALI ACTIVATED BINDERS (AABS) AS A LANDFILL LINER AND COVER

Landfill liner is a containment system used between landfill waste and the ground soil to prevent the migration of leachate into the soil and groundwater. Clay is typically used as a liner in the landfill barrier system due to efficiency and low permeability. Over the last decade, different types of binders such as cement, fly ash, and slag have been used with clay to improve the mechanical characteristics and reduce hydraulic conductivity of natural clay liners. This study introduced a new sustainable technique where treated dune sand mixed with alkali activated binder (AAB) made with fly ash (FA), ground-granulated blast-furnace slag (GGBFS), and alkali activated solutions are used as a landfill liner system, due to the unavailability of natural clay in most countries. Therefore, lab-scale compacted specimens with different mixing ratios of AABs treated desert sand were prepared and cured for 7 days to conduct a series of compressive strength. The results showed that the 20% binder mixed with 30% FA, 70% slag, and alkali solution of 0.5 have a high compressive strength with 12 MPa compared with other mixing ratios. However, a 10% binder with same precursors ratio of FA and slag has shown a less strength regardless of alkali solution with around 3 MPa. Finally, all mixing ratios have shown that the strength met the requirements of landfill liner system which were greater than 200 kPa.

EXAMINING THE APPLICABILITY OF ALKALI ACTIVATED BINDERS (AABS) AS A LANDFILL LINER AND COVER

Landfill liner is a containment system used between landfill waste and the ground soil to prevent the migration of leachate into the soil and groundwater. Clay is typically used as a liner in the landfill barrier system due to efficiency and low permeability. Over the last decade, different types of binders such as cement, fly ash, and slag have been used with clay to improve the mechanical characteristics and reduce hydraulic conductivity of natural clay liners. This study introduced a new sustainable technique where treated dune sand mixed with alkali activated binder (AAB) made with fly ash (FA), ground-granulated blast-furnace slag (GGBFS), and alkali activated solutions are used as a landfill liner system, due to the unavailability of natural clay in most countries. Therefore, lab-scale compacted specimens with different mixing ratios of AABs treated desert sand were prepared and cured for 7 days to conduct a series of compressive strength. The results showed that the 20% binder mixed with 30% FA, 70% slag, and alkali solution of 0.5 have a high compressive strength with 12 MPa compared with other mixing ratios. However, a 10% binder with same precursors ratio of FA and slag has shown a less strength regardless of alkali solution with around 3 MPa. Finally, all mixing ratios have shown that the strength met the requirements of landfill liner system which were greater than 200 kPa.

Micro-destructive assessment of subgrade compaction quality using ultrasonic pulse velocity

The ultrasonic pulse velocity (UPV) correlates significantly with the density and pore size of subgrade filling materials. This research conducts numerous Proctor and UPV tests to examine how moisture and rock content affect compaction quality. The study measures the changes in UPV across dry density and compaction characteristics. The compacted specimens exhibit distinct microstructures and mechanical properties along the dry and wet sides of the compaction curve, primarily influenced by internal water molecules. The maximum dry density exhibits a positive correlation with the rock content, while the optimal moisture content demonstrates an inverse relationship. As the rock content increases, the relative error of UPV measurement rises. The UPV follows a hump-shaped pattern with the initial moisture content. Three intelligent models are established to forecast dry density. The measure of UPV and PSO-BP-NN model quickly assesses compaction quality.

NMR-based pore water distribution characteristics of silty clay during the soil compaction, saturation, and drying processes

The pore water distribution (PWD) of soil provides key information about soil shear strength, hydraulic conductivity, and water-retention ability. The PWD characteristics of the soil depend on the specimen preparation conditions (i.e., the variations in initial water content or compaction degree) and drying-wetting processes, which were investigated by using the nuclear magnetic resonance (NMR) technique. The NMR T2 spectrum is mathematically transformed into the PWD curve to more accurately quantify the variations in pore water content stored with pores of different radii. The pore water in silty clay can be categorized into strongly bound water, intra-aggregate pore water, and inter-aggregate pore water, which are identified by the pore radius of <0.05 μm, 0.05-1.0 μm and >1.0 μm, respectively. The effects of compaction degree and initial water content on the PWD of the soil exhibit distinctions. For unsaturated compacted specimens, the PWDs remain unaffected by changes in compaction degree, while an increase in initial water content promotes the formation of clay aggregates, thereby increasing the maximum water-holding pore radius and the intra-aggregate pore water content. For saturated compacted specimens, the inter-aggregate and intra-aggregate pore water content increases with a decrease in the compaction degree, while the changes in the PWD shape from unimodal to bimodal with an increase in the initial water content. During the soil drying process, inter-aggregate pore water is rapidly drained, the intra-aggregate dominant pore water content increases first and then decreases, and the strongly bound water content remains constant. The relationship between the cumulative pore water distribution curve and the soil-water characteristic curve (SWCC) can be established through the Young-Laplace theory. The SWCC can be well predicted by using the envelope of the cumulative pore water distribution curves during soil drying.

Compaction Delay and Temperature Effects on Early-Age Properties of Roller-Compacted Concrete

The lower water content of roller-compacted concrete (RCC) coupled with climatic conditions (e.g., higher air temperature, increased wind speed, and lower relative humidity) and compaction delay factors (e.g., traffic delay, plant location, and paving speed) can significantly affect the in situ density and hardened properties of RCC pavements. In this study, a control RCC mix was batched and maintained at standard (21°C) and elevated (35°C) temperatures and then compacted at increasing delay times for up to 180 min. The elevated mix temperature and compaction delay times greater than 90 min prevented the RCC mix from achieving 98% of the initial wet density from the modified Proctor test. Two additional RCC mixes were batched to determine if they could maintain a longer compaction window, one containing a rheology-modifying and retarding admixture and the other incorporating saturated fine lightweight aggregates. The RCC with admixture was the most effective at maintaining moisture content, density, compressive strength, and fracture properties at all compaction delay times. For example, at 180 min of delay, the RCC mixture with admixture still maintained 98.2% of the initial wet density, 81% of the compressive strength, and approximately the same fracture toughness and energy. The addition of fine lightweight aggregates did not extend the compaction window relative to standard RCC mix. The gyratory compacted specimens were more sensitive to the effects of temperature and compaction delay on RCC mixes than the vibratory hammer prepared specimens.