Bulk-fill Resin Composites Research Articles

Microleakage of Class II Bulk-Fill Resin Composite Restorations Cured with Light-Emitting Diode versus Quartz Tungsten-Halogen Light: An In Vitro Study in Human Teeth

Background: Resin composites undergo a certain degree of shrinkage when light-cured with different light sources available on the market, resulting in microleakage of dental restorations. The aim of the present study was to assess microleakage of class II restorations with bulk-fill resin composites cured with LED (light-emitting diode) and QTH (quartz tungsten-halogen light) units, both in cervical and occlusal areas of cavity preparations. Materials and Methods: In the present in vitro experimental study, a total of 30 human molar teeth were used, in which 60 class II cavities were prepared (mesial and distal) and restored with Filtek bulk fill resin composite. Restorations were equally distributed in 3 groups according to type of curing light: A, QTH (Litex 680A Dentamerica®); B, LED (Bluephase N® 3rd generation); and C, LED (Valo® 3rd generation). Each group was further subdivided into subgroups 1 and 2 according to IV-A or IV-B resin composite color. Restored teeth were subjected to 20,000 thermal cycles between 5° and 55 °C, then immersed in 1M silver nitrate solution for 24 h. Subsequently, the teeth were sectioned mesiodistally to obtain samples for observation under stereomicroscope in order to determine microleakage degree. Kruskal-Wallis H and Mann-Whitney U statistical tests were applied with a significance level of 5% (p < 0.05). Results: No statistically significant differences were found in the degree of microleakage of bulk-fill resin composites light-cured with LED and QTH units for both occlusal (p > 0.05) and cervical areas (p > 0.05). Additionally, no significant differences were found when comparing microleakage between occlusal and cervical areas (p > 0.05), regardless of lamp type. In addition, significant differences in microleakage degree were found between bulk-fill resins with IV-A and IV-B shades when they were light-cured with QTH at cervical level (p = 0.023). However, there were no significant differences when comparing these bulk-fill resin composite shades at occlusal level with LED (p > 0.05) and QTH (p > 0.05) units. Conclusions: Class II restorations with bulk-fill resin composite in IV-A and IV-B shades light-cured with third generation LED lamp and QTH showed no significant differences in microleakage when compared in both occlusal and cervical areas. On the other hand, significantly more microleakage was found at the cervical level when a darker shade of resin composite was used and light-cured with the QTH unit.

Colour Stability Of Bulk Fill Composites: A Systematic Review

Background: The introduction of Bulk-Fill (BF) composite materials, among other new preparations, was one of the most recent innovations in operative dentistry. All bulk composites' colour stability is a source of concern. There has been a lot of research on the effects of different drinking solutions on the colour consistency of conventional resin-based composites, but little has been written about the colour changes of BF composite resins, which have been developed for the placement of somewhat thicker layers.&#x0D; Aim: Thus, the objective of this systematic review was to assess the colour consistency of various bulk-filled composites.&#x0D; Methods and Materials: A massive exploration of preexisting literature was done in order to locate all relevant research that addressed the sustainability of colour of BF composites under the effect of various. According to PRISMA standards, the current systematic evaluation was carried out. A thorough search for non-controversial existing literature on the websites like PubMed portal, MEDLINE portal, and Scopus portal was done in December 2022. There were no comparable articles in Cochrane online library. To make sure that all pertinent studies were found, search keywords were applied. Furthermore, all appropriate scientific papers from Jan 2010 to December 2022 on the effect of various beverages, polishing techniques, storage media, and oral fluids, bleaching protocols on the colour longevity of bulk-filled composite samples were included.&#x0D; Results: 18 studies were evaluated in this systematic review. 9 studies focused on the effect of different drinks and beverages like tea, coffee, wine, and acidic beverages over the changes in the colour of bulk-filled composites. There were 4 studies that evaluated the impact of different polishing mechanisms. There were 2 researches that described the influence of different bleaching techniques over the change in colour of bulk-filled composites. One study discussed the effect of reinforcement of glass fibers and polythene fibers in bulk-filled composites, the presence of different dentin substitutes and water solubility and water sorption impact over the change in colour. The number of specimens evaluated ranged from n=20 to n=800 across all the included studies. There was the use of two to ten composite materials across all the included studies.&#x0D; Conclusion: When there was an analysis of the effect of different beverages and drinks over the changes in colour then there were mixed results. Some studies found that colour changes in bulk-filled composites are lesser than in customary composites. While some studies revealed that alteration in colour is greater in bulk-filled composites when compared to customary composites. Some studies found no significant difference in colour change in conventional composite and bulk-filled composite. The polishing operations can have a serious influence on the staining impedance of bulk-fill composite resins.

In-vitro pulpal temperature increases when photo-curing bulk-fill resin-based composites using laser or light-emitting diode light curing units.

To evaluate the in vitro pulpal temperature rise (ΔT) within the pulp chamber when low- and high-viscosity bulk-fill resin composites are photo-cured using laser or contemporary light curing units (LCUs). The light output from five LCUs was measured. Non-retentive Class I and V cavities were prepared in one upper molar. Two T-type thermocouples were inserted into the pulp chamber. After the PT values reached 32°C under simulated pulp flow (0.026 mL/min), both cavities were restored with: Filtek One Bulk Fill (3M), Filtek Bulk Fill Flow (3M), Tetric PowerFill (Ivoclar Vivadent), or Tetric PowerFlow (Ivoclar Vivadent). The tooth was exposed as follows: Monet Laser (1 and 3s), PowerCure (3 and 20 s), PinkWave (3 and 20 s), Valo X (5 and 20 s) and SmartLite Pro (20 s). The ΔT data were subjected to one-way ANOVA followed by Scheffe's post hoc test. Monet 1s (1.9J) and PinkWave 20 s (30.1J) delivered the least and the highest amount of energy, respectively. Valo X and PinkWave used for 20 s produced the highest ΔT values (3.4-4.1°C). Monet 1s, PinkWave 3s, PowerCure 3s (except FB-Flow) and Monet 3s for FB-One and TP-Fill produced the lowest ΔT values (0.9-1.7°C). No significant differences were found among composites. Short 1- to 3-s exposures produced acceptable temperature rises, regardless of the composite. The energy delivered to the tooth by the LCUs affects the temperature rise inside the pulp. The short 1-3s exposure times used in this study delivered the least amount of energy and produced a lower temperature rise. However, the RBC may not have received sufficient energy to be adequately photo-cured.

The Influence of Chlorhexidine Gluconate Dentine Pre-Treatment on Adhesive Interface and Marginal Sealing.

Background and Objectives: The aim of this in vitro study was to evaluate the combined effect of a 2% chlorhexidine aqueous solution and a universal adhesive system applied in self-etch and etch-and-rinse strategies on the composite resin-dentin interface. Materials and Methods: Class V cavities were prepared on the facial and lingual surfaces of forty caries-free molars extracted for orthodontic reasons. The samples were randomly divided into two groups corresponding to the used etching protocol: I-etch-and-rinse; II-self-etch. In each tooth, one cavity was assigned for the control subgroups -IA (n = 20) and IIA (n = 20)-adhesive only, and the opposite cavity was pretreated with a 2% chlorhexidine solution-Gluco CHeX Cerkamed-subgroups IB (n = 20) and IIB (n = 20). Both sets of groups were restored using a universal adhesive system (Single Bond Universal Adhesive, 3M-ESPE) and a bulk-fill composite resin (Filtek One Bulk Fill Restorative, 3M-ESPE). The roots and the pulp tissue were then removed, and a needle connected to a perfusor with 100 mL saline solution was used for pulp pressure simulation with a hydrostatic pressure of 20 cm H2O. Cariogenic attack was simulated using a demineralizing solution for 3 days at a constant temperature of 25 °C. The teeth were then sectioned in a facial-lingual direction and the microleakages at the occlusal and cervical margins were registered and scored using an optical Carl-Zeiss AXIO Imager A1m microscope (Carl-Zeiss). The composite resin-dentin interface was analyzed using a SEM Vega Tescan LMH II. Statistical analysis was performed using the Kruskal-Wallis test with a significance level of p < 0.05. Results: Microleakage evaluation showed no significant differences among the study groups (p > 0.05). In subgroup IA, significant differences were recorded between occlusal and cervical margins (p < 0.05). Conclusions: Application of chlorhexidine on tooth substrate before using a universal bonding system in total etch or self-etch mode has no influence on the adhesive interface in the condition of cariogenic attack. The thickness of the adhesive resin layer seems to be less uniform when using chlorhexidine, but the morphological differences at the adhesive interface have no influence on the sealing capacity of the universal bonding system, regardless of the etching strategy.

Detection of Leachable Components from Conventional and Dental Bulk-Fill Resin Composites (High and Low Viscosity) Using Liquid Chromatography-Tandem Mass Spectrometry (LC-MS/MS) Method.

The aim of this study was to investigate leachable components (monomers) in high and low viscosity dental bulk-fill resin composites and conventional resin composite materials after polymerization. Six bulk-fill and six conventional dental resin composite materials were used in this study. The samples of each material (three sets of triplicates) were cured for 20 s with irradiance of 1200 mW/cm2 with a LED curing unit and immersed in a 75% ethanol solution at 37 °C. The eluates from each triplicate set were analyzed after 24 h, 7 days or 28 days using liquid chromatography coupled with triple quadrupole tandem mass spectrometry (LC-MS/MS). Detectable amounts of 2-Hydroxyethyl methacrylate (HEMA) were found in both Gradia materials and the amount observed across different time points was statistically different (p ˂ 0.05), with the amount in solution increasing for Gradia and decreasing for Gradia Direct flo. Bisphenol A diglycidildimethacrylate (BIS GMA) was found in Filtek and Tetric materials. Triethylene glycol dimethacrylate (TEGDMA) was detected in all materials. On the other hand, there were no statistically significant differences in the amounts of TEGDMA detected across different time points in either of the tested materials. Monomers HEMA, TEGDMA, 4-dimethylaminobenzoic acid ethyl ester (DMA BEE) and BIS GMA in bulk-fill and conventional composites (high and low viscosity) can be eluted after polymerization. The good selection of composite material and proper handling, the following of the manufacturer's instructions for polymerization and the use of finishing and polishing procedures may reduce the elution of the unpolymerized monomers> responsible for the possible allergic and genotoxic potential of dental resin composites.

Effect of low temperature and room temperature on the depth of cure of bulk-fill composite resins

The study analyzed the influence of temperature on the depth of cure of bulk-fill composite resins. Three discs (ISO 4049/2000) from each group were made, and four restorative materials were investigated: Opus Bulk-Fill Flow, Opus Bulk-Fill APS, Filtek™ One Bulk-Fill, and Filtek™ Bulk-Fill Flow. They were light-cured (Gnatus ± 1,200 mW/cm2) for 20 seconds, varying the temperature (23°C and 5°C) and simulating the use of the product both at room temperature and under refrigeration. The materials were inserted in aluminum matrices with 10 mm in depth and 4 mm in diameter. A clear film strip and a glass microscope slide were positioned at the top and bottom surfaces. The material was condensed and light-cured with the tip of the light source in close contact, for 20 seconds on the top surface. Immediately after irradiation, the samples were removed from the mold, and the uncured part was removed with a plastic spatula. The measurement was performed with a micrometer ± 0.1 mm, and the value was divided by 2. The data were analyzed with two-way ANOVA at a significance of 0.05. There was a statistical difference in the temperature between the results obtained in Opus Bulk-Fill APS (p &lt;0.001) and Filtek™ Bulk-Fill Flow (p = 0.018) resins. For the temperature of 5°C, Filtek™ Bulk-Fill Flow showed a statistical difference compared to the other resins, while Opus Bulk-Fill Flow and Opus Bulk-Fill APS did not. For the temperature of 23°C, Filtek™ Bulk-Fill Flow maintained the statistical difference from the others, but Filtek™ One Bulk-Fill and Opus Bulk-Fill APS did not present statistical differences. Storing the Filtek™ Bulk-Fill Flow composite resin in the refrigerator caused a greater depth of cure than the other resins, and the depth of cure decreased at room temperature. As for Opus Bulk-Fill APS, the depth of cure decreased proportionally to the temperature decrease. The temperature may affect the depth of cure of some composite resins.

Fracture Load of Molars Restored with Bulk-fill, Flowable Bulk-fill, and Conventional Resin Composite After Simulated Chewing.

This study aimed to compare the fracture toughness of molars with wide mesio-occlusal-distal (MOD) cavities restored with regular and flowable bulk-fill resin composite and a conventional resin composite after 250,000 mechanical cycles of chewing simulation. Thirty-two extracted mandibular third molars were selected and class II MOD cavities involving 2/3 of the intercuspal width and 4 mm depth were prepared. Teeth were divided into four groups based on resin composite type and insertion technique (n=8): (1) CT, unprepared teeth (control); (2) CV, conventional resin composite (Tetric N-Ceram, Ivoclar Vivadent) with incremental technique; (3) R-BF, regular bulk-fill resin composite (Tetric N-Ceram Bulk Fill, Ivoclar Vivadent) with a single increment; and (4) F-BF, flowable bulk-fill resin composite (Tetric N-Flow Bulk Fill, Ivoclar Vivadent) with a single increment, except for a 1-mm-thick layer at the occlusal surface, restored with conventional resin composite (Tetric N-Ceram). All specimens were evaluated to detect the presence and propagation of enamel cracks using a LED transilluminator before and after 250,000 mechanical cycles (SD Mechatronic GmbH). After a chewing simulation, they were subjected to a compressive force in a universal testing machine (DL-2000, EMIC) until fracture. The maximum fracture load of the specimens was measured (N) and the fracture patterns were classified based on the fracture site (above or below the cementoenamel junction [CEJ]). Data were statistically analyzed with one-way ANOVA. All specimens survived after 250,000 mechanical cycles, and no statistically significant differences among groups were observed regarding the fracture toughness (p<0.05). The fracture analysis demonstrated that failures below the CEJ were more common in CV (75%), while CT, R-BF, and F-BF showed this type of failure in 38%, 63%, and 63% of the specimens, respectively. The results of the crack analysis showed that the occurrence of new cracks and crack propagation was also higher in CV (33.3%), followed by R-BF, F-BF, and CT (14%, 14%, and 11% of the specimens, respectively). Teeth restored with regular and flowable bulk-fill composites showed similar fracture toughness after the chewing simulation compared to those restored with the conventional resin composite and unprepared teeth. Furthermore, teeth restored with both regular and flowable bulk-fill composites showed a lower incidence of enamel cracks and fractures below the CEJ compared to those restored with the conventional resin composite.

Microleakage Study of a Bulk Fill over an Uncured Adhesive System

This study aimed to evaluate and compare the microleakage of composite resin restorations under a total-etch adhesive system applied with two different techniques, with and without cure. Cavities were made on the buccal surface of twenty-six intact teeth and subsequently restored with bulk-fill flow composite resin (SDR®® flow+) and conventional resin (Spectra™ ST HV). Two experimental groups were created, one where the total-etch adhesive (Prime &amp; Bond Active®) was cured and another where the adhesive was not cured before placing the flowable resin. Two control groups were also created, negative and positive. After the restorations were finished the, teeth were submerged in a solution of sodium pertechnetate (99mTcNaO4) for 3 h to evaluate the microleakage. The results showed more infiltration of radioisotopes characterized by the highest total count values of microleakage in group 1 (cured adhesive) and in the positive control. Group 2 (noncured adhesive) and the negative control showed lower values. We therefore considered that these groups were similar since their p-value was less than 0.05, with no statistically significant difference. Group 4 showed a statistically significant increase in relation to group 3 (p = 0.027). We concluded that the method of bulk-fill composite resins with noncured adhesive agents can have a positive effect on the longevity of bond strengths, with reduced microleakage.

Blue Laser for Polymerization of Bulk-Fill Composites: Influence on Polymerization Kinetics.

The objective of this study was to compare the polymerization kinetics of bulk-fill resin composites cured with a LED-curing device and a diode laser (449 nm). Three bulk-fill composites were light-cured with constant radiation exposure at 10 J/cm2 by varying radiant exitance and curing time. The following three light-curing protocols were used: (I) 3300 mW/cm2 for 3 s; (II) 2000 mW/cm2 for 5 s; and (III) 1000 mW/cm2 for 10 s. The degree of conversion (DC) was monitored in real time at a data acquisition rate of 2 spectra/s over a 5-min period and again after seven days using Fourier transform infrared spectroscopy. DC amounted to 30.9-61.7% at 4-mm depth after 5 min. DC values of two sculptable composites were significantly higher with the laser, regardless of the curing protocol used, but not for the flowable composite. The maximum polymerization rate (2.0-22.1%/s) was less affected by the type of curing device for one of the composites, while the other two composites achieved significantly higher values when cured with the laser. Laser curing generally increased the DC and the maximum polymerization rate while it shortened the onset of the maximum reaction rate. New handheld laser devices with adjustable power have the potential to be used as a photopolymerization light source for new generations of bulk-fill composites.

Effect of topical fluoride applications on residual monomer release from resin-based restorative materials

BackgroundThe effects of topical fluoride applications on the release of monomer ingredients from resin-based dental materials by immersion in various extraction solutions are unclear. The aim of this study was to determine the effect of topical fluorides (APF and NaF) on the elution of residual monomers (Bis-GMA, TEGDMA, UDMA, and HEMA) from resin-based materials.MethodsNinety specimens were prepared, 30 bulk-fill composite resin, 30 nanohybrid universal composite resin, and 30 polyacid-modified composite resin (compomer). These were randomly divided into three groups based on fluoride application procedures. Each specimen was kept in 75% ethanol solution, and residual monomers released from materials were analyzed using high-performance liquid chromatography (HPLC) after 10 min, 1 h, 24 h, and 30 days. The groups were compared using the Mann Whitney U and Kruskal Wallis tests. Measurements were analyzed using the Friedman and Wilcoxon signed-rank tests.ResultsFluoride applications generally had no considerable effect on the amount of residual monomer released from resin-based restorative materials. The amount of monomer release after topical APF application was similar to the release in the control group and was lower than the release in the NaF group. The release of monomers from the resin-based material used in the study did not approach toxic levels at the applied time intervals. The compomer released lower amounts of monomer than other resin-based materials.ConclusionsFluoride applications do not increase monomer release from resin-based restorative materials. However, compomers should be employed by clinicians due to their lower monomer release compared to other resin restorative materials. The release of monomers from all the resin-based materials did not approach toxic levels at the applied time intervals.

The Effect of Pre-Heating on Fracture Toughness in Three Distinct Composite Resin Systems at Two Different Temperatures: A Protocol for an In-vitro Study

Introduction: Composite resins are considered the pinnacle of esthetic restorations, but they have their own disadvantages, such as polymerization shrinkage, low fracture toughness, and the formation of microcracks, all of which eventually results in failure of the restoration. Fracture toughness is an important factor for failure. Warming the same composites to certain temperatures will show drastic improvements in the abovementioned flaws, especially the fracture toughness. Need for the study: Therefore, the objective of this study is to evaluate and compare the fracture toughness of three different types of composite resin systems at two different pre-heating temperatures. The study aims to provide valuable information to clinicians in choosing the most appropriate restorative material for posterior composite restorations, which can ultimately improve the treatment's success rate and reduce the risk of complications such as secondary caries, postoperative sensitivity and ultimately restoration failure. Objective: In summary, this study will compare and evaluate the fracture toughness of nanohybrid, micro-hybrid, and bulkfill composite resins pre-heated at 50 degrees Celsius and 60 degrees Celsius. Methodology: The methodology involves dividing 72 freshly extracted premolars with intact occlusal anatomy and fully developed apical foramina into three main groups based on three different composites and further dividing each group into two sub-groups based on two different pre-heating temperatures, with 12 teeth in each group. Each tooth will then be prepared with a Class-II Mesio-Occlusal-Distal (MOD) cavity and receive pre-heated composite restoration according to its assigned group and sub-group. The prepared samples will be tested for fracture toughness using a universal testing machine.

Characterization of whitening toothpastes and their effect on the physical properties of bulk-fill composites

To characterize activated charcoal and 2% hydrogen peroxide-based toothpastes and investigate their effects on roughness, color change, and gloss of bulk-fill composite resin. Composite resin specimens (Aura Bulk Fill, SDI) were subjected to 5,000 brushing cycles with regular toothpaste (Colgate Total 12, [RT]), activated charcoal toothpaste (Bianco Dental Carbon, [AC]), or hydrogen peroxide-containing toothpaste (Colgate Luminous White Advanced, [HP]), with or without coffee exposure. The pH, particle characterization by scanning electron microscopy (SEM), and weight% of solid particles in the toothpaste were assessed. Roughness (Ra) was evaluated using a surface profile-measuring device, color change (∆Eab/∆E00) by reflectance spectrophotometer, and gloss unit (GU) by glossmeter. Kruskal-Wallis, Dunn, Friedman, and Nemenyi tests were used, and the correlation coefficient test was performed between Ra and GU (α=0.05). RT presented a higher Ra after brushing and did not change after staining with coffee; moreover, the ∆Eab/∆E00 values were higher for RT than HP. Regarding gloss, AC and HP obtained higher values compared to RT. A significant negative correlation between gloss and Ra was found for RT exposed to coffee. All toothpastes had a neutral pH; however, RT had the largest percentage of solids by weight. SEM images showed particles of many sizes: irregular shape (RT), more regular particles (AC), and spherical clusters (HP). Although surface roughness, color change, and gloss may compromise the longevity of restorations, the whitening toothpastes tested did not promote more morphology changes than regular toothpastes.

Effects of ceramic thickness, ceramic translucency, and light transmission on light-cured bulk-fill resin composites as luting cement of lithium disilicate based-ceramics.

To assess the effects of ceramic thickness, ceramic translucency, and light transmission on restorative composites used as luting cement for lithium disilicate-based ceramics. Four luting types of cement were tested (n=8); a dual-cured resin cement (Multilink N), a light-cured conventional flowable composite (Tetric N-Flow), and two light-cured bulk-fill flowable composites (Tetric N-Flow Bulk Fill and X-tra base). The 20 s- or 40 s-light (1000 mW/cm2) was transmitted through 1- or 2-mm-thick high- or low-translucency (HT- or LT-) ceramic discs (IPS e.Max press) to reach the 1-mm-thick luting cement. Light transmitted to cement without ceramic served as a control. Vickers hardness number (VHN), flexural strength (FS), fractography, and degree of conversion (DC) were evaluated. One-way and multi-way analysis of variance was conducted to determine the effects of factors on VHN and FS. Ceramic thickness, light transmission time, and cement type significantly affected the VHN of the luting cement (P < .000). Only Multilink N (LT- and HT-1mm) and Tetric N-Flow (HT-1mm) reached 90% VHN of corresponding control by 20 s-light transmissions, but Tetric N-Flow exhibited lowest VHN and approximately 1/3-1/2 VHN of Multilink N (P < 0.05). X-tra base expressed superior physicochemical properties to Tetric N-Flow Bulk Fill (P < 0.05) and reached >90% VHN of control in all conditions with 40 s-light transmissions except for LT-2 mm. DC, FS, and fractography supported these findings. The light-cured bulk-fill composite served as a luting cement for lithium-disilicate-based ceramics in a product-dependent manner. Light transmission time is crucial to ensure sufficient luting cement polymerization.

Clinical Evaluation of Class I Posterior Restorations Restored with Smart Dentin Replacement Flowable Bulk-fill Composite Material in Bulk-fill and Incremental Technique – One-year Randomized Clinical Trial

ABSTRACT Aim and Objective: The aim and objective of this in vivo study are to evaluate the clinical performance of smart dentin replacement (SDR) flowable bulk-fill composite in class I restorations with incremental technique and bulk-fill technique. Materials and Methods Fifty patients with at least two class 1 cavities in the age group of 18–40 years were recruited. In all cavities, Xeno Vplus self-etch adhesive was applied. In one of the cavities, SDR was placed in bulk increments up to 4 mm as needed to fill the cavity 2-mm short of the occlusal surface. The occlusal part was placed with SureFil nanohybrid composite, and the other cavity was placed by incremental technique. The restorations were evaluated using FDI criteria. Results: Data were subjected to statistical analysis and analyzed using Chi-square test. After 1 year, all restorations received clinically excellent and clinically good scorings for each criterion. Conclusion: There is no statistically significant difference between the bulk-fill technique and the incremental technique using SDR after 1-year follow-up. CLINICAL RELEVANCE TO INTERDISCIPLINARY DENTISTRY The smart dentin replacement bulk-fill resin composites demonstrated good clinical durability as equal as conventional composites. It provides an advantage of less clinical time for placement in deep posterior cavities.

The effect of different herbal teas on the color stability of nanohybrid and bulk-fill composites

Aim: The aim of this study is to investigate the effects of green tea and rosehip tea, on the color stability of nanohybrid and bulk-fill composite resins. Methodology: A total of 60 disc-shaped samples were made from two types of A2 resin with nanohybrid (Tetric N Ceram, Ivoclar Vivadent, Schaan, Liechtenstein) and bulk-fill (Filtek Bulk-Fill, 3M ESPE, MN, USA) structure with the help of 10 mm diameter and 2 mm thick Teflon molds in this study. All samples were finished and polished with 4-stage (thick, medium, fine, superfine) polishing discs (Sof-lex, 3M ESPE, MN, USA) and kept in an oven at 37 °C for 24 hours. The samples, whose initial color measurements were made by spectrophotometer, were divided into subgroups for the control group and two different herbal teas (Green tea, Rosehip) (n=10). Color measurements were repeated, and ΔE values were calculated. Wilcoxon, Kruskal-Wallis, and Bonferroni tests were used to analyze the data (p &lt; 0.05). Results: There was no statistically significant difference in color change between the composite resins (p &gt; 0.05). No significant color change was found for either the Tetric N-Ceram or Filtek Bulk-Fill composite resin samples immersed in distilled water (p &gt; 0.05, ΔE&lt;3.3). Conclusion: Rosehip and green tea affect the color stability of composite resin restorations. Whereas the color change caused by green tea is at a clinically acceptable level, that stemming from rosehip tea falls within clinically unacceptable levels. How to cite this article: Tunçdemir MT, Dereli Z, Bahar A. The effect of different herbal teas on the color stability of nanohybrid and bulk-fill composites. Int Dent Res 2022;12(Suppl.1):103-7. https://doi.org/10.5577/intdentres.445 Linguistic Revision: The English in this manuscript has been checked by at least two professional editors, both native speakers of English.

Micro-computed tomography assesment of structural microporosity and marginal gaps in different flowable composites placed with different instruments

Objectives: The aim of this study was to evaluate the structural microporosity (MP) and marginal gap (MG) of different flowable composite resins placed with different instruments using micro-computed tomography (μCT). &#x0D; Materials and Methods: Standard Class II MOD cavities were prepared on 108 lower third molar teeth. Three different flowable composite resins; Filtek Bulk-fill, SDR Bulk-fill and I-Flow conventional flowable composite resin were applied to the cavities using a sharp explorer, a microbrush or an injector. After they were covered with a paste-like nanohybrid composite resin, μCT images were examined in terms of MP and MG. Statistical analysis of the data was performed using two-way ANOVA and Tukey’s post hoc tests. &#x0D; Results: MP was observed less in explorer group than microbrush and injector groups (p &lt; 0.05). There was no significant difference between microbrush and injector groups (p &gt; 0.05). i-FLOW flowable composite resin showed the highest MP rate compared to the other two groups (p &lt; 0.05). There was no significant difference between SDR and Filtek Bulk-fill in MP (p &gt; 0.05). In terms of MG, i-FLOW presented higher MG values than other two materials (p &lt; 0.05), while the instruments showed similar results (p &gt; 0.05). &#x0D; Conclusions: Additional occluso-gingivally vibration of flowable materials with an explorer may be useful in the placement. Bulk-fill composite resins are better than conventional flowable composite resin in terms of MP and MG.

Bond strength of bulk fill composite to teeth prepared with Er

Aim: The present in vitro study aimed to evaluate the bond strength of a bulk fill composite on dentin surfaces prepared with the Er: YAG laser. Methods: Twenty-four permanent third molars were selected and divided into 2 groups: CP - Conventional preparation with high-speed handpiece (control) and LA (laser) - Preparation with Er: YAG laser. The occlusal surface was removed to expose coronal dentin, which was subsequently prepared with a high-speed handpiece or Er: YAG laser (350mJ, 4Hz, 1.5 ml/min water flow). Both groups were restored with Filtek One Bulk Fill (3M ESPE) composite resin. After 24 hours, the samples were evaluated for microtensile bond strength (μTBS), fracture pattern, and scanning electron microscopy (SEM). Results: The data obtained in the μTBS test were submitted to t-test (α=0.05). The results showed no difference in μTBS when the different types of cavity preparation were compared (ρ=0.091). Fracture patterns revealed the prevalence of cohesive fracture in composite resin in CP (83.3%) and adhesive fracture in LA (92.1%). In the SEM analysis, the LA group demonstrated the presence of gaps between the composite resin and the irradiated dentin surface. The hybrid layer exhibited more regularity with the presence of longer and uniform resin tags in the CP group. Conclusion: The type of cavity preparation did not influence the values of bulk fill composite resin μTBS to dentin. Fracture patterns and scanning electron microscopy analyses suggested less interference at the adhesive interface in preparations performed using CP.

Periodontopathic bacterial adhesion to different restorative materials used to elevate proximal subgingival margins.

This study compared the periodontopathic bacterial adhesion to four restorative materials used for deep margin elevation at 2, 24, and 48-h after incubation. Discs were produced from four restorative materials: resin modified glass ionomer, glass hybrid, flowable bulk fill resin composite, and bioactive ionic resin. Root dentin was used as control. Specimens were coated with saliva and used to culture a biofilm comprised of three strains of periodontopathic bacteria; Porphyromonas gingivalis, Prevotella intermedia, and Aggregatibacter actinomycetemcomitans. Bacterial adherence was assessed by colony count assay, crystal violet staining, and visualized using confocal laser scanning microscopy. Data were analyzed by two-way ANOVA followed by Tukey's post hoc tests. The adhesion values for the control specimens were significantly higher than for other materials, while those for the flowable bulk fill were significantly lower than for any other material within all evaluation assays. The 2-h incubation period showed the lowest adhesion values regardless of the group. The 48-h adhesion values were higher than the 24-h results in all groups except the flowable bulk fill. Microscopic imaging partially supported the findings of the measurements. In terms of periodontopathic bacterial adhesion, the tested flowable bulk fill may be preferable for subgingival use over other tested materials.

Effect of vibration during bulk and incremental filling on adaptation of a bulk-fill composite resin

This study evaluated the effect of vibration on adaptation of bulk-fill composite resin. A scanning laser doppler vibrometer measured the frequency and amplitude of a vibratory device (COMO; B&L Biotech) used for resin placement and visualized its effect on the resin according to depth. A bulk-fill composite resin (Filtek Bulk Fill; 3M ESPE) was placed in simulated cavities (4 mm diameter, 4 mm depth) by different layering methods (incremental filling with two 2-mm-thick layers vs. bulk filling with a single 4-mm-thick layer). The groups were further divided based on the application of vibration during restoration (no vibration vs. vibration). In addition to the surface void area at the cavity floor, the overall void volume and the void volumes of the bottom, middle, and top thirds were obtained for micro-computed tomography analysis. The frequency and amplitude of the COMO were approximately 149 Hz and between 26 and 51 µm, respectively. When vibration was not applied, incremental filling had a lower void volume in the bottom third of the cavity than did bulk filling (p < 0.05). Vibration applied with a 4-mm-thick bulk fill had no significant effect on the adaptation of composite resin (p > 0.05). In contrast, vibration reduced the amount of void formation in the bottom third of the cavity during incremental filling (p < 0.05). Application of vibration to resin with a 2-mm incremental-layering technique formed a smaller void at the interface between the cavity and resin and within the bulk-fill composite resin.

In vitro surface and color changes of tooth-colored restorative materials after sport and energy drink cyclic immersions.

There has not been any research conducted on surface properties and color changes from sport and energy drinks on bulk-fill resin composite, nanohybrid resin composite and glass ionomer restorative material. The aim of this in vitro study was to investigate the effect of sport and energy drinks on surface hardness, roughness and color changes of bulk-fill resin composite, nanohybrid resin composite and glass ionomer restorative material, and to also evaluate the acidity and titratable acidity of the drinks. One hundred and forty-seven specimens of each tooth-colored restorative material were prepared in a polytetrafluoroethylene mold (10mm. in diameter and 2mm. in thickness). Before immersion, baseline data of hardness, roughness, and color value were recorded. Each material was divided into 3 groups for sport drink, energy drink, and deionized water (serving as a control). The specimens were immersed in a storage agent for 5s, then in artificial saliva for 5s alternately for 24 cycles, and then stored in artificial saliva for 24h. The immersion cycle was repeated for 14days and hardness, roughness and color values were measured at 7 and 14days. After immersion, the glass ionomer restorative material had statistically less hardness, more roughness and more color changes than the others (P < 0.05). Energy drink groups statistically caused more surface and color changes than sport drink groups (P < 0.05). Sport and energy drinks affected hardness, roughness, and color changes in all the tooth-colored restorative materials evaluated.